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The revolutionary impetus of the NMR methods in organic chemistry
has parallels in the field of boron chemistry. lIB NMR spectroscopy
provided a basis for the elucida tion of structures and reactions
of the boron hydrides. However, although many studies have been
carried out with the higher boranes, carboranes, metalloboranes,
etc., and although certain patterns have emerged, the correlation
between the observed chemical shift and the assigned structural
unit is still not fully understood. Therefore, predictions in this
area are still rather limited, and semiquantitative interpretations
are not yet pos sible. Several years ago Eaton and Lipscomb
sUpImarized the status in this field in their book "NMR Studies of
Boron Hydrides and Related Compounds" and a plethora of new data
has accumulated since then. The book also contained material on
simple bo rane derivatives, but they were not discussed in any
detail. On the other hand many systematic studies, both synthetic
and spectroscopic, have been conducted on these simple boron
materials in the last decade. Thus a large amount of NMR
information is available, not only on lIB but also on 1 H, 1 3 C,
and 14 N. However, this information is widely scattered in the
literature, and often the data are not discussed at all. It see med
appropriate, therefore, to collect these data and to present them
in one volume."
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