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Advances in Chemistry Research - Volume 50 (Hardcover)
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Advances in Chemistry Research - Volume 50 (Hardcover)
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This volume opens with a discussion of the analytical chemistry of
amlodipine from the perspective of drug purity control and
stability indicating assays for quality assurance purposes. The
synthesis and stability of the heterocycle is examined in
conjunction with the determination impurities in different
scenarios. Other specific aspects such as phase transitions, the
determination of genotoxic impurities, and the enantiomers of the
drug are also discussed.The following chapter focuses on the
numerical investigation of the trends in the flow patterns and the
corresponding characteristics of the chemical reactions that
develop for different flow path geometries incorporating features
typically found in engineering systems. These geometries include a
straight flow channel, a constricted channel, a channel with a
roughened surface, a channel with a junction, and then a channel
with an expansion and contraction including an open expansion, an
expansion with a filter, with baffles, a flow obstruction, and a
roughened surface.The authors go on to discuss carbonylation
reactions of important homogeneous and heterogeneous catalysts,
development of carbon monoxide surrogates and future aspects. The
carbon monoxide molecule has gained immense interest as one-carbon
source building block through CC bond formations in many catalytic
carbonylation reactions for producing fine and bulk chemicals.The
closing chapter discusses the most important aspects of
liquid-liquid extraction of ion-association complexes: association
and extraction equilibria, ion-association reagents, organic
solvents, side processes and their manifestation, and methods for
determining composition and equilibrium constants. It systematizes
information on the classical liquid-liquid extraction of
ion-association complexes which can help investigators take full
advantage of the high chemical-analytical potential of these
compounds.
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