Preparative Polar Organometallic Chemistry is a collection of
laboratory procedures for the synthesis and functionalization of
organoalkali and Grignard compounds. The second volume with methods
for generation and transformation of compounds bearing the metal at
an sp3 carbon complements the first in which the metal was bound to
an sp2 carbon atom in the reagent. Synthetically important
intermediates such as metallated S, S-acetales, imines, nitriles,
isonitriles and ketones are illustrated. All procedures have been
worked out in full detail and tested in the author's own
laboratory. Both books are intended to be practical bench-top
laboratory manuals for working organic chemists, from the student
to the advanced scientist.
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