This text is aimed at people who have some familiarity with
high-resolution NMR and who wish to deepen their understanding of
how NMR experiments actually 'work'. This revised and updated
edition takes the same approach as the highly-acclaimed first
edition. The text concentrates on the description of commonly-used
experiments and explains in detail the theory behind how such
experiments work. The quantum mechanical tools needed to analyse
pulse sequences are introduced set by step, but the approach is
relatively informal with the emphasis on obtaining a good
understanding of how the experiments actually work. The use of
two-colour printing and a new larger format improves the
readability of the text. In addition, a number of new topics have
been introduced:
How product operators can be extended to describe experiments in
AX2 and AX3 spin systems, thus making it possible to discuss the
important APT, INEPT and DEPT experiments often used in carbon-13
NMR.Spin system analysis i.e. how shifts and couplings can be
extracted from strongly-coupled (second-order) spectra.How the
presence of chemically equivalent spins leads to spectral features
which are somewhat unusual and possibly misleading, even at high
magnetic fields.A discussion of chemical exchange effects has been
introduced in order to help with the explanation of transverse
relaxation.The double-quantum spectroscopy of a three-spin system
is now considered in more detail.
Reviews of the First Edition
"For anyone wishing to know what really goes on in their NMR
experiments, I would highly recommend this book" - "Chemistry
World"
..".I warmly recommend for budding NMR spectroscopists, or
others who wish to deepen their understanding of elementary NMR
theory or theoretical tools" - "Magnetic Resonance in
Chemistry"
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