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This unique thesis discusses the development of conceptually novel
and synthetically valuable methods that use visible light
photocatalysis. Each chapter addresses a different topic in the
emerging field of photocatalysis, which has become an indispensable
tool for organic synthesis. Photocatalysis employs environmentally
harmless and abundant visible light in the presence of a
photosensitizer, and as such offers an attractive alternative to
harmful UV light in photo-mediated reactions. This book introduces
the novel concept of merging gold catalysis with visible light
photocatalysis in a dual catalytic fashion, which demonstrates
their compatibility with each other for first time and has inspired
the development of various reactions. Moreover, a novel
trifluoromethylation method, which combines radical addition
chemistry with a polar rearrangement to synthesize valuable
fluorinated compounds, is presented, since compounds featuring
fluorinated functionality are the subject of increasing attention
in pharmaceutical, agrochemical and material research. It also
develops an external photocatalyst-free photochemical method for
the synthesis of valuable indolizine heterocycles, where the
product mediates its own formation. Lastly, it describes the
synthesis and characterization of two novel highly porous
metal-organic frameworks (MOFs). The comprehensive text is rounded
out with illustrations and color figures.
This unique thesis discusses the development of conceptually novel
and synthetically valuable methods that use visible light
photocatalysis. Each chapter addresses a different topic in the
emerging field of photocatalysis, which has become an indispensable
tool for organic synthesis. Photocatalysis employs environmentally
harmless and abundant visible light in the presence of a
photosensitizer, and as such offers an attractive alternative to
harmful UV light in photo-mediated reactions. This book introduces
the novel concept of merging gold catalysis with visible light
photocatalysis in a dual catalytic fashion, which demonstrates
their compatibility with each other for first time and has inspired
the development of various reactions. Moreover, a novel
trifluoromethylation method, which combines radical addition
chemistry with a polar rearrangement to synthesize valuable
fluorinated compounds, is presented, since compounds featuring
fluorinated functionality are the subject of increasing attention
in pharmaceutical, agrochemical and material research. It also
develops an external photocatalyst-free photochemical method for
the synthesis of valuable indolizine heterocycles, where the
product mediates its own formation. Lastly, it describes the
synthesis and characterization of two novel highly porous
metal-organic frameworks (MOFs). The comprehensive text is rounded
out with illustrations and color figures.
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