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The Advancing Frontier in the Knowledge of the Structure of
Interphases.- Some Recent Spectroscopic Approaches to the
Solid-Solution Interface.- Application to Electrocatalysis of EMIRS
(Electrochemically Modulated Infrared Reflectance Spectroscopy) and
Related Techniques.- Photoacoustic Spectroscopy and the In-Situ
Characterization of the Electrochemical Interface.- Raman
Spectroscopic Techniques in Interfacial Electrochemistry.- Laser
Raman Spectroscopy in Studies of Corrosion and Electrocatalysis.-
UV-Visible Reflectance Spectroscopy in Electrochemistry.- Study of
Anodic Oxides by UV-Visible Potential-Modulated Reflectance
Spectroscopy.- Nonlinear Optical Techniques for Surface Studies.-
X-Ray Diffraction at the Electrode-Solution Interface.- X-Ray
Reflectivity and Surface Roughness.- Surface Structural
Investigations by Electron Diffraction Techniques.- Auger Electron
Spectroscopy and the Electrochemical Interface.- Photoelectron
Spectroscopy (XPS and UPS) of Electrode Surfaces.- Rutherford
Backscattering Spectroscopy of Electrode Surfaces.- Electrochemical
Applications of Scanning Tunneling Microscopy.
Electrochemistry is one of the oldest branches of Physical
Chemistry. Having its foundations in the work of Faraday, Arrhenius
and others, it evolved from the study of transport in electrolyte
solutions to that of electrode kinetics. Kinetic methods are
inherently unable to identify unequivocally the species involved in
a reaction. Therefore, beginning in the 70s many spectroscopic and
diffraction techniques were applied to the study of the
electrode-electrolyte interface, in order to identify intermediary
reaction species, and even the spatial arrangement of atoms or
molecules at the interface. In order to disseminate these
techniques, a NATO Advanced Sutdy Institute was held at Puerto de
la Cruz, Tenerife (Canary Islands, Spain) from July 2 to 15, 1988.
The Institute consisted of tutorial type lecutures, poster
sessions, and round-table discussions. It was attended by over 65
participants from NATO-member countries, and others from Argentina
and Japan. In the present volume most of the lectures presented at
the Institute have been collected. At least one chapter is devoted
to each technique. Emphasis has been made on case studies, rather
than theory, which can be found in textbooks and other
publications. Our purpose in this book is to help the
electrochemists uninitiated in spectroscopic methods to decide
which techniques would be suitable for application to their
particular problems. We thank all the lecturers who contributed to
this volume, and even those UHPs (Unrepentant Habitual
Procrastinators) who did not in spite of our urgings to do so.
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