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Solid-State NMR is a branch of Nuclear Magnetic Resonance which is
presently experiencing a phase of strongly increasing popularity.
The most striking evidence is the large number of contributions
from Solid-State Resonance at NMR meetings, approaching that
ofliquid state resonance. Important progress can be observed in the
areas of methodological developments and applications to organic
and inorganic matter. One volume devoted to more or less one of
each of these areas has been published in the preceding three
issues. This volume can be considered an addendum to this series.
Selected methods and applications of Solid-State NMR are featured
in three chapters. The first one treats the recoupling of dipolar
interactions in solids, which are averaged by fast sample rotation.
Following an introduction to effective Hamiltonians and Floquet
theory, different types of experiment such as rotary resonance,
dipolar chemical shift correlation spectroscopy, rotational
resonance and multipulse recoupling are treated in the powerful
Floquet formalism. In the second chapter, the different approaches
to line narrowing of quadrupolar nuclei are reviewed in a.
consistent formulation of double resonance (DaR) and dynamic angle
spinning (DAS). Practical aspects of probe design are considered as
well as advanced 2D experiments, sensitivity enhancement
techniques, and spinning sideband manipulations. The use of such
techniques dramatically increases the number of nuclei which can be
probed in high resolution NMR spectroscopy. The final chapter
describes new experimental approaches and results of structural
studies of noncrystalline solids."
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