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A comprehensive collection of robust methods for the detection of
pesticide compounds or their metabolites useful in food,
environmental, and biological monitoring, and in studies of
exposure via food, water, air, and the skin or lungs. The readily
reproducible methods range from gas and liquid chromatography
coupled to mass spectrometry detection and other classic detectors,
to capillary electrophoresis and immunochemical or radioimmunoassay
methods. The authors have focused on extraction and cleanup
procedures, in order to develop and optimize more fullyautomated
and miniaturized methods, including solid-phase extraction,
solid-phase microextraction, microwave-assisted extraction, and
on-line tandem liquid chromatography (LC/LC) trace enrichment,
among others. The protocols offer step-by-step laboratory
instructions, an introduction outlining the principles behind the
technique, lists of the necessary equipment and reagents, and tips
on troubleshooting and avoiding known pitfalls.
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