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Catalysis, which until recently had largely been limited to the production of large volume chemical, is now being increasingly used in the production of medium and small volume chemicals. Simultaneously, the role of process intensification in enhancing overall productivity is being increasingly recognised. This usually takes the form of reaction rate enhancement by extending known or emerging laboratory techniques to industrial scale production. Organic Synthesis Engineering describes the application of catalysis in its various forms in organic synthesis, and addresses both the chemical and engineering aspects of catalysts (particularly solid catalysts). It also outlines different techniques of reaction rate and/or selectivity enhancement - a feature not found in any existing books on reaction engineering.
Filling a longstanding gap for graduate courses in the field,
Chemical Reaction Engineering: Beyond the Fundamentals covers basic
concepts as well as complexities of chemical reaction engineering,
including novel techniques for process intensification. The book is
divided into three parts: Fundamentals Revisited, Building on
Fundamentals, and Beyond the Fundamentals. Part I: Fundamentals
Revisited reviews the salient features of an undergraduate course,
introducing concepts essential to reactor design, such as mixing,
unsteady-state operations, multiple steady states, and complex
reactions. Part II: Building on Fundamentals is devoted to "skill
building," particularly in the area of catalysis and catalytic
reactions. It covers chemical thermodynamics, emphasizing the
thermodynamics of adsorption and complex reactions; the
fundamentals of chemical kinetics, with special emphasis on
microkinetic analysis; and heat and mass transfer effects in
catalysis, including transport between phases, transfer across
interfaces, and effects of external heat and mass transfer. It also
contains a chapter that provides readers with tools for making
accurate kinetic measurements and analyzing the data obtained. Part
III: Beyond the Fundamentals presents material not commonly covered
in textbooks, addressing aspects of reactors involving more than
one phase. It discusses solid catalyzed fluid-phase reactions in
fixed-bed and fluidized-bed reactors, gas-solid noncatalytic
reactions, reactions involving at least one liquid phase
(gas-liquid and liquid-liquid), and multiphase reactions. This
section also describes membrane-assisted reactor engineering, combo
reactors, homogeneous catalysis, and phase-transfer catalysis. The
final chapter provides a perspective on future trends in reaction
engineering.
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