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Consider for a few moments the staggering magnitude of
technological advance which has occurred since the birth four
centuries ago of that early progenitor of the scientific method,
Galileo. Think also about the extent of scientific knowledge avail
able during the lifetime of Galileo and his associates; knowledge
increasing slowly through several centuries, accelerating rapidly
during the past twenty years, culminat ing at the present time in a
virtual impossibility that one person - one communit- possibly even
one nation - can hope to generate or use productively more than a
minute portion of the world's scientific knowledge. New
developments - expanded technological concepts - occur with
dazzling rapidity, often faster than they can be assimilated. At
the same time there are practical limitations to the extent of
formal education. Continuing education, upgrading of scientific
know-how, retraining to assure full utilization of existing
knowledge - these are urgent problems which today confront the
nation's scientific community. And there is never enough time. The
problem is compounded by the increasing burden of information
retrieval.
The papers presented in this volume of Advances in X-Ray Analysis
were chosen from those presented at the Fourteenth Annual
Conference on the Applications of X-Ray Analysis. This conference,
sponsored by the Metallurgy Division of the Denver Research
Institute, University of Denver, was held on August 24,25, and 26,
1965, at the Albany Hotel in Denver, Colorado. Of the 56 papers
presented at the conference, 46 are included in this volume; also
included is an open discussion held on the effects of chemical com
bination on X-ray spectra. The subjects presented represent a broad
scope of applications of X-rays to a variety of fields and
disciplines. These included such fields as electron-probe
microanalysis, the effect of chemical combination on X-ray spectra,
and the uses of soft and ultrasoft X-rays in emission analysis.
Also included were sessions on X-ray diffraction and fluor escence
analysis. There were several papers on special topics, including
X-ray topography and X-ray absorption fine-structure analysis.
William L. Baun contributed considerable effort toward the
conference by organizing the session on the effect of chemical
combination on X-ray spectra fine structure. A special session was
established through the excellent efforts of S. P. Ong on the uses
and applica tions of soft X-rays in fluorescent analysis. We offer
our sincere thanks to these men, for these two special sessions
contributed greatly to the success of the conference.
The torrential flow of technical information appearing in the world
sources of literature is creating concern and apprehension among
scientific people at all levels. It is extremely difficult to keep
abreast of information flowing into a specific field. It is nearly
impossible to transcend traditional confines of individual
disciplines and put to effective use all pertinent information
which stems from continuously increased trans disciplinary
research. At the same time the researcher is faced with problems of
in creasing complexity, with the requirement for new knowledge and
new techniques, and must frequently, with little time, bridge the
gap between his own sphere of experience and a sometimes apparently
unrelated new interest. This is readily observed with X-ray
analysis, where the chemist, physicist, metallurgist, and engineer
are each faced with the solution of problems peculiar to specific
disciplines but where solutions frequently correlate with the
particular needs of the others. The Annual Conference on
Applications of X-Ray Analysis and the subsequent Advances in X-Ray
Analysis contribute to better understanding of multidisciplinary
accomplishments; they are a ready source of information for the
researcher who must undertake an abrupt change in emphasis for new
objectives. The scope of this conference is broad--concerning
itself, as it does, with latest developments in high-temperature
and cryogenic techniques, phase equilibria, crystal structures,
polymers, microprobes, and new developments in instrumentation.
A real need exists for ways to bridge the gap between basic
research and prac tical application, for faster utilization of new
discoveries and new developments in the world of technology, and
for technical transfer of defense and space accomplish ments to the
civilian economy. The problem is compounded by the torrential flow
of technical information. Thirty million books are available on
technical subjects, the total increasing at the rate of six hundred
every day. There are one hundred thousand technical journals. More
scientific work has been published in the past ten years than in
all preceding recorded history. Scientists and engineers only a few
years beyond academic pursuits are already encountering a
continuing need for retraining and expansion of their own
knowledge. At the same time, the re searchers - scientists,
engineers, students - must exhibit bold creative thinking to evolve
new technology, to better understand nature's secrets, to conceive
new theories, and to reduce old theories to practical utilization.
Research in the physical sciences and the engineering sciences
provides the ever-flowing spring of knowledge for the investigation
of new ideas. Such research is sometimes hindered by classification
as "basic" or "applied. " There are many times when a research
program has no immediate or ultimate objective and is truly
contributing to our reservoir of knowledge - a reservoir which will
certainly be tapped in the future.
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