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NMR Spectroscopy of Polymers places emphasis on the practical
use of NMR spectroscopy in polymer chemistry rather than the
theoretical treatments. Based on the authors' extensive
experimental experience, topics covered include (1) experimental
problems such as preparation of sample solution, selection of
solvent, internal standard and tube, and contaminants in sample
solution, (2) accuracy and precision of NMR measurements required
in the analysis of polymer structure such as tacticity, copolymer
composition and chain end structures, (3) volume magnetic
susceptibility by NMR, (4) stereochemistry of polymer chains,
chemical composition and comonomer sequence distribution in
copolymers, and end groups and irregular linkages, (5) on-line
coupled size exclusion chromatography(SEC) and NMR
spectroscopy(SEC/NMR) in which an NMR spectrometer is set in the
SEC system as a detector.
NMR Spectroscopy of Polymers places emphasis on the practical
use of NMR spectroscopy in polymer chemistry rather than the
theoretical treatments. Based on the authors' extensive
experimental experience, topics covered include (1) experimental
problems such as preparation of sample solution, selection of
solvent, internal standard and tube, and contaminants in sample
solution, (2) accuracy and precision of NMR measurements required
in the analysis of polymer structure such as tacticity, copolymer
composition and chain end structures, (3) volume magnetic
susceptibility by NMR, (4) stereochemistry of polymer chains,
chemical composition and comonomer sequence distribution in
copolymers, and end groups and irregular linkages, (5) on-line
coupled size exclusion chromatography(SEC) and NMR
spectroscopy(SEC/NMR) in which an NMR spectrometer is set in the
SEC system as a detector.
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