This volume of Inorganic Syntheses spans the preparations of wide
range of important inorganic, organometallic and solid-state
compounds. The volume is divided into 6 chapters. The first chapter
contains the syntheses of some key early transition metal halide
clusters and the very useful mononuclear molybdenum(III) synthon,
MoCl3(THF)3. Chapter 2 covers the synthesis of a number of
cyclopentadienyl compounds, including a novel route to sodium and
potassium cyclopentadienide, MC5H5. Chapter 3 details synthetic
procedures for a range of metal-metal bonded compounds, including
several with metal-metal multiple bonds. Chapter 4 contains
procedures for a range of early and late transition metal
compounds, each a useful synthon for further synthetic elaboration.
Chapter 5 deals with the synthesis of a number of main group
compounds and ligands, while Chapter 6 covers teaching laboratory
experiments.
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