This book explains concepts of transmission electron microscopy (TEM) and x-ray diffractometry (XRD) that are important for the characterization of materials. The fourth edition adds important new techniques of TEM such as electron tomography, nanobeam diffraction, and geometric phase analysis. A new chapter on neutron scattering completes the trio of x-ray, electron and neutron diffraction. All chapters were updated and revised for clarity. The book explains the fundamentals of how waves and wavefunctions interact with atoms in solids, and the similarities and differences of using x-rays, electrons, or neutrons for diffraction measurements. Diffraction effects of crystalline order, defects, and disorder in materials are explained in detail. Both practical and theoretical issues are covered. The book can be used in an introductory-level or advanced-level course, since sections are identified by difficulty. Each chapter includes a set of problems to illustrate principles, and the extensive Appendix includes laboratory exercises.

This book explains concepts of transmission electron microscopy (TEM) and x-ray diffractometry (XRD) that are important for the characterization of materials. The fourth edition adds important new techniques of TEM such as electron tomography, nanobeam diffraction, and geometric phase analysis. A new chapter on neutron scattering completes the trio of x-ray, electron and neutron diffraction. All chapters were updated and revised for clarity. The book explains the fundamentals of how waves and wavefunctions interact with atoms in solids, and the similarities and differences of using x-rays, electrons, or neutrons for diffraction measurements. Diffraction effects of crystalline order, defects, and disorder in materials are explained in detail. Both practical and theoretical issues are covered. The book can be used in an introductory-level or advanced-level course, since sections are identified by difficulty. Each chapter includes a set of problems to illustrate principles, and the extensive Appendix includes laboratory exercises.

The new edition of this popular textbook provides a fundamental approach to phase transformations and thermodynamics of materials. Explanations are emphasised at the level of atoms and electrons, and it comprehensively covers the classical topics from classical metallurgy to nanoscience and magnetic phase transitions. The book has three parts, covering the fundamentals of phase transformations, the origins of the Gibbs free energy, and the major phase transformations in materials science. A fourth part on advanced topics is available online. Much of the content from the first edition has been expanded, notably precipitation transformations in solids, heterogeneous nucleation, and energy, entropy and pressure. Three new chapters have been added to cover interactions within microstructures, surfaces, and solidification. Containing over 170 end-of-chapter problems, it is a valuable companion for graduate students and researchers in materials science, engineering, and applied physics.