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Keeping mathematics to a minimum, this book introduces nuclear
properties, nuclear screening, chemical shift, spin-spin coupling,
and relaxation. It is one of the few books that provides the
student with the physical background to NMR spectroscopy from the
point of view of the whole of the periodic table rather than
concentrating on the narrow applications of 1H and 13C NMR
spectroscopy. Aids to structure determination, such as decoupling,
the nuclear Overhauser effect, INEPT, DEPT, and special editing,
and two dimensional NMR spectroscopy are discussed in detail with
examples, including the complete assignment of the 1H and 13C NMR
spectra of D-amygdain. The authors examine the requirements of a
modern spectrometer and the effects of pulses and discuss the
effects of dynamic processes as a function of temperature or
pressure on NMR spectra. The book concludes with chapters on some
of the applications of NMR spectroscopy to medical and non-medical
imaging techniques and solid state chemistry of both I = F1/2 and I
> F1/2 nuclei. Examples and problems, mainly from the recent
inorganic/organometallic chemistry literature support the text
throughout. Brief answers to all the problems are provided in the
text with full answers at the end of the book.
In recent years, there has been a major expansion of high pressure
research providing unique information about systems of interest to
a wide range of scientific disciplines. Since nuclear magnetic
resonance has been applied to a wide spec trum of problems in
chemistry, physics and biochemistry, it is not surprising to find
that high pressure NMR techniques have also had many applications
in these fields of science. Clearly, the high information content
of NMR experiments combined with high pressure provides a powerful
tool in modern chem istry. It is the aim of this monograph, in the
series on NMR Basic Principles and Progress, to illustrate the wide
range of prob lems which can be successfully studied by high
pressure NMR. Indeed, the various contributions in this volume
discuss studies of interest to physics, chemical physics,
biochemistry, and chemical reaction kinetics. In many different
ways, this monograph demonstrates the power of modern experimental
and theoretical techniques to investigate very complex systems. The
first contribution, by D. Brinkman, deals with NMR and NQR studies
of superionic conductors and high-Tc supercon ductors at high
pressure. Pressure effects on phase transitions, detection of new
phases, and pressure effects on diffusion and spin-lattice
relaxation, represent a few of the topics discussed in this
contribution of particular interest to solid state physics."
Keeping mathematics to a minimum, this book introduces nuclear
properties, nuclear screening, chemical shift, spin-spin coupling,
and relaxation. It is one of the few books that provides the
student with the physical background to NMR spectroscopy from the
point of view of the whole of the periodic table rather than
concentrating on the narrow applications of 1H and 13C NMR
spectroscopy. Aids to structure determination, such as decoupling,
the nuclear Overhauser effect, INEPT, DEPT, and special editing,
and two dimensional NMR spectroscopy are discussed in detail with
examples, including the complete assignment of the 1H and 13C NMR
spectra of D-amygdain. The authors examine the requirements of a
modern spectrometer and the effects of pulses and discuss the
effects of dynamic processes as a function of temperature or
pressure on NMR spectra. The book concludes with chapters on some
of the applications of NMR spectroscopy to medical and non-medical
imaging techniques and solid state chemistry of both I = F1/2 and I
> F1/2 nuclei. Examples and problems, mainly from the recent
inorganic/organometallic chemistry literature support the text
throughout. Brief answers to all the problems are provided in the
text with full answers at the end of the book.
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