The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential.  Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis.  Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment.

Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step.  These include:

• State-of-the-art extraction techniques for organic and inorganic analytes
• Sample preparation in biological measurements
• Sample pretreatment in microscopy
• Surface enhancement as a sample preparation tool in Raman and IR spectroscopy
• Sample concentration and clean-up methods
• Quality control steps

Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences.

Undergraduate students in environmental science need a foundation in instrumental analysis as much as traditional chemistry majors, but their needs may be quite different. Environmental Chemical Analysis provides an explanation of analytical instrumentation methods for students without a background in analytical chemistry. This second edition features expanded material on sample preparation and quality assurance and control. It also includes new chapters on biological analysis and analysis of environmental particulates. It brings together sampling, sample preparation, and analytical techniques necessary for environmental applications, demonstrated through case studies of actual environmental measurement protocols. Provides comprehensive coverage of all aspects of environmental chemical analysis Explains analytical instrumentation methods for students approaching the subject from a different angle Includes two new chapters on biological analysis and analysis of environmental particulates Expands material on sample preparation and quality assurance/quality control Winner of Choice 2019 Outstanding Academic Title Award

This book is an account of the manner in which the optical phenomena observed from solids relate to their fundamental properties. Written at the graduate level, it attempts a threefold purpose: an indication of the breadth of the subject, an in-depth examination of important areas, and a text for a two-semester course. The first two chapters present introductory theory as a foundation for subsequent reading. The following ten chapters broadly concern electronic properties associated with semiconductors ranging from narrow to wide energy gap materials. Lattice properties are examined in the remaining chap ters, in which effects governed by phonons in perfect crystals, point defects, their vibrational and electronic spectra, and electron-phonon interactions are stressed. Fun and hard work, both in considerable measure, have gone into the preparation of this volume. At the University of Freiburg, W. Germany, from August 7-20, 1966, the occasion of a NATO Advanced Study Institute on "The Optical Properties of Solids," the authors of these various chapters lectured for the Institute; this volume provides essentially the "Proceed ings" of that meeting. Many major revisions of original lectures (contrac tions and enlargements) were required for better organization and presentation of the subject matter. Several abbreviated chapters appear mainly to indicate the importance of their contents in optical properties research and to indicate recently published books that provide ample coverage. We are indebted to many people: the authors for their efforts and patience; our host at the University of Freiburg, the late Professor Dr.

In June 1978 the University of Rhode Island conducted a three-day short course on Recent Advances in Fiber Optics. followed by a two-day conference on the Physics of Fiber Optics. The course contained over a dozen lectures spanning a wide range of subject matter from fundamental theory to operational systems. presented by well-known scientists from industry. government and academic institutions. The conference. on the other hand. emphasized basic research on fiber optics and related subjects. This volume contains both papers presented at the conference. as well as the majority of the lectures from the course (the written versions were solicited on a voluntary basis for this volume). In some cases the papers in this volume represent expanded or otherwise modified versions of the original presentations. One of the principal aims of the conference was promulgation of novel and/or unconventional concepts. For this reason. the papers in this volume cover subjects such as bistable optical switches. fiber acoustic sensors. extruded infrared fibers. compressively coated glass fibers. and soliton propagation in fibers.

This book provides an account of modern aspects relating far infrared radiation to properties of solids; it encompasses both theoretical and experimental considerations. Written at the gradu ate level, it attempts a threefold purpose; an indication of the breadth of the subject, an in-depth examination of important areas, and reference material to complement a text for a course. The treatment and organization of material here is compatible with a preceding volume of this series on "Optical Properties of Solids." Chapters 1-6 present material concerned principally with experimental considerations necessary to the carrying out of meas urements in the far infrared spectral region. They also serve to provide considerable introductory material for the remaining chap ters which deal with various areas that offer theoretical treat ments utilizing and understanding far infrared properties of solids. Several lectures presented at the Institute could not be in cluded in this book for two reasons: (i) Final versions of the lecture notes suitable for publication never arrived from several lecturers; (ii) Some materials were deliberately left out fro~ this book as they were also presented at an earlier NATO Institute and form part of a preceding volume edited by us in this series. In particular, it is recommended that Chapters 14 and 15, viz., in frared and Raman spectra due to lattice vibrations by S. S. Mitra and impurity induced lattice absorption by L. Genzel in "Optical Properties of Solids'* be read concurrently with the present volume.

Undergraduate students in environmental science need a foundation in instrumental analysis as much as traditional chemistry majors, but their needs may be quite different. Environmental Chemical Analysis provides an explanation of analytical instrumentation methods for students without a background in analytical chemistry. This second edition features expanded material on sample preparation and quality assurance and control. It also includes new chapters on biological analysis and analysis of environmental particulates. It brings together sampling, sample preparation, and analytical techniques necessary for environmental applications, demonstrated through case studies of actual environmental measurement protocols. Provides comprehensive coverage of all aspects of environmental chemical analysis Explains analytical instrumentation methods for students approaching the subject from a different angle Includes two new chapters on biological analysis and analysis of environmental particulates Expands material on sample preparation and quality assurance/quality control Winner of Choice 2019 Outstanding Academic Title Award