Bringing together the leading European expertise in behaviour and design of silos, this important new book is an essential reference source for all concerned with current problems and developments in silo technology. Silos are used in an enormous range of industries and the handling characteristics of many industrial materials require different approaches for successful, economical installations. For the first time, the many approaches taken by specialists in different fields are brought together in a unified way so that common problems can be addressed. This book is the result of a four-year European project - Concerted Action - Silos - funded under the Brite Euram programme which has involved over 100 expert engineers and researchers from all over Europe, in seven working groups.

First published in 1999. Family homelessness is one of the most profound and disturbing social problems of the 1990's and will be one of the most important issues facing the United States in the twenty-first century. The main purpose of this study was to develop a transitional program framework that can assist homeless women with children to become self-sufficient. In order to create this framework; this study identified current program areas and components in transitional programs for homeless women with children, including education and employment training components; and determined which program areas and components of current programs have a relationship to programs with successful outcomes.

Particle technology is a term used to refer to the science and technology related to the handling and processing of particles and powders. The production of particulate materials, with controlled properties tailored to subsequent processing and applications, is of major interest to a wide range of industries, including chemical and process, food, pharmaceuticals, minerals and metals companies and the handling of particles in gas and liquid solutions is a key technological step in chemical engineering.

This textbook provides an excellent introduction to particle technology with worked examples and exercises. Based on feedback from students and practitioners worldwide, it has been newly edited and contains new chapters on slurry transport, colloids and fine particles, size enlargement and the health effects of fine powders. Topics covered include:

Characterization (Size Analysis)Processing (Granulation, Fluidization)Particle Formation (Granulation, Size Reduction)Storage and Transport (Hopper Design, Pneumatic Conveying, Standpipes, Slurry Flow)Separation (Filtration, Settling, Cyclones)Safety (Fire and Explosion Hazards, Health Hazards)Engineering the Properties of Particulate Systems (Colloids, Respirable Drugs, Slurry Rheology)

This book is essential reading for undergraduate students of chemical engineering on particle technology courses. It is also valuable supplementary reading for students in other branches of engineering, applied chemistry, physics, pharmaceutics, mineral processing and metallurgy. Practitioners in industries in which powders are handled and processed may find it a useful starting point for gaining an understanding of the behavior of particles and powders.

Review of the First Edition taken from "High Temperatures - High pressures" 1999 31 243 - 251

..""This is a modern textbook that presents clear-cut knowledge. It can be successfully used both for teaching particle technology at universities and for individual study of engineering problems in powder processing.""

Particle technology is a term used to refer to the science and technology related to the handling and processing of particles and powders. The production of particulate materials, with controlled properties tailored to subsequent processing and applications, is of major interest to a wide range of industries, including chemical and process, food, pharmaceuticals, minerals and metals companies and the handling of particles in gas and liquid solutions is a key technological step in chemical engineering.

This textbook provides an excellent introduction to particle technology with worked examples and exercises. Based on feedback from students and practitioners worldwide, it has been newly edited and contains new chapters on slurry transport, colloids and fine particles, size enlargement and the health effects of fine powders. Topics covered include:

Characterization (Size Analysis)Processing (Granulation, Fluidization)Particle Formation (Granulation, Size Reduction)Storage and Transport (Hopper Design, Pneumatic Conveying, Standpipes, Slurry Flow)Separation (Filtration, Settling, Cyclones)Safety (Fire and Explosion Hazards, Health Hazards)Engineering the Properties of Particulate Systems (Colloids, Respirable Drugs, Slurry Rheology)

This book is essential reading for undergraduate students of chemical engineering on particle technology courses. It is also valuable supplementary reading for students in other branches of engineering, applied chemistry, physics, pharmaceutics, mineral processing and metallurgy. Practitioners in industries in which powders are handled and processed may find it a useful starting point for gaining an understanding of the behavior of particles and powders.

Review of the First Edition taken from "High Temperatures - High pressures" 1999 31 243 - 251

..""This is a modern textbook that presents clear-cut knowledge. It can be successfully used both for teaching particle technology at universities and for individual study of engineering problems in powder processing.""

The Fourth Edition of Powder Technology Handbook continues to serve as the comprehensive guide to powder technology and the fundamental engineering processes of particulate technology, while incorporating significant advances in the field in the decade since publication of the previous edition. The handbook offers a well-rounded perspective on powder technologies in gas and liquid phases that extends from particles and powders to powder beds and from basic problems to actual applications. This new edition features fully updated and new chapters written by a team of internationally distinguished contributors. All content has been updated and new sections added on. Powder Technology Handbook provides methodologies of powder and particle handling technology essential to scientific researchers and practical industrial engineers. It contains contemporary and comprehensive information on powder and particle handling technology that is extremely useful not only to newcomers but also to experienced engineers and researchers in the field of powder and particle science and technology.

A state-of-the-art reference, Metal Nanoparticles offers the latest research on the synthesis, characterization, and applications of nanoparticles. Following an introduction of structural, optical, electronic, and electrochemical properties of nanoparticles, the book elaborates on nanoclusters, hyper-Raleigh scattering, nanoarrays, and several applications including single electron devices, chemical sensors, biomolecule sensors, and DNA detection. The text emphasizes how size, shape, and surface chemistry affect particle performance throughout.
Topics include synthesis and formation of nanoclusters, nanosphere lithography, modeling of nanoparticle optical properties, and biomolecule sensors.

The topics discussed in this text range from quasi-static problems to dynamic problems, and are divided into 15 groups, such as: cohesion/cracking; wave propagation; and quasi-static behaviour. Each group contains theoretical, experimental and computational approaches by researchers.

This is the first comprehensive book on fine particle synthesis that ranges from fundamental principles to the most advanced concepts, highlighting monodispersed particles from nanometers to micrometers. Describes mechanisms of formation and specific characteristics of each family of compounds while identifying problems and proposing solutions Offering a systematically organized review of the subject and including recent remarkable developments, Fine Particles contains subsections that analyze growth processes, characterize products, and delineate physical and chemical results based on causality arranges organic and inorganic materials according to their chemical composition covers forced hydrolysis and hydrolysis of metal and silicon alkoxides in homogeneous solutions details controlled double jet and Ostwald ripening processes examines emulsion and dispersion polymerization discusses surface modification of polymer and inorganic particles considers the formation of magnetic particles, fine composites, and nanocrystalline luminous materials and more Replete with 1700 references and over 600 photographs, drawings, tables, and equations, Fine Particles is useful for physical, surface, colloid, inorganic, organic, polymer, medicinal, and analytical chemists; chemical engineers; ceramicists; materials scientists; metallurgists; pharmacists; biochemists; biophysicists; biotechnologists; biomaterials specialists; and graduate students in these disciplines.

This unique reference examines the modern pharmaceutical compacting techniques used to form tablets out of powders-describing the physical structure of pharmaceutical compacts, the bonding phenomena that occur during powder compaction, and the compression mechanisms of pharmaceutical particles.

Addressing key issues in the instrumentation of powder handling processes, this up-to-date volumeserves as an excellent source of new ideas for designing on-line instruments, as well as a helpfulguide for understanding and applying measurement principles.Describing physical and chemical principles in clear, simple language, Powder and BulkSolids Handling Processes provides substantial background material that lists related industrialfields and the physical representation of powder properties . . . focuses on instrumentation,reviewing state variables in powder processes . . . discusses the sampling of particles from apowder bed or suspension flow as a basic method for evaluating powder handling processes ... andpresents incisive information on various methods and instruments used for on-line measurement ofpowder flow rate, particle concentration in suspension, level of powder in storage vessels, andmore.Complete with references, equations, illustrations, and tables, this volume is essential reading forchemical, mechanical, systems, ceramic, and civil engineers, instrumentation engineers in powderand bulk solid processes, and upper-level undergraduate and graduate students in chemical andmechanical engineering.

Drawing from the third edition of the bestselling "Powder Technology Handbook," this book is focused solely on analyzing the fundamental properties and behavior of particles and particle beds. Powder Technology: Fundamentals of Particles, Powder Beds, and Particle Generation concentrates on the most useful analytical methods of observation, measurement, modeling, and prediction.

This volume carefully incorporates the progressive work and vision of new authors while retaining the concepts that continue to promote innovative research and applications. The authors highlight new information and developments from areas including surface properties and analysis, particle motion in fluids, mechanical properties of a powder bed, and the design and formation of composite particles. They explain how particles deposit, coagulate, and settle in various media, explore different techniques for generating particles in different states, and detail methods of surface modification.

Particularly useful for scientists studying nanoparticle applications, Powder Technology: Fundamentals of Particles, Powder Beds, and Particle Generation incorporates the latest developments in areas including surface properties and analysis, particle motion in fluids, mechanical properties of a powder bed, and the design and formation of composite particles.

Drawing from the third edition of the bestselling "Powder Technology Handbook," this book concentrates on handling methods and unit operations for powder and particle processing techniques. Itexamines the purpose and factors involved in each process-including planning, equipment, measurements, and other necessary considerations.

This book carefully incorporates the progressive work and vision of new authors while retaining the concepts that continue to promote innovative research and applications. In addition to detailing the purpose and implementation of processes including kneading, drying, filtration, and powder coating, the authors highlight recent developments in combustion and heating, electrostatic powder coating, and simulation. They also emphasize practical information including multipurpose equipment, instrumentation for key measurements, and modeling techniques. The text concludes with a review of recent data on the health effects of small particles and the types of protective devices that are currently available.

Powder Technology: Handling and Operations, Process Instrumentation, and Working Hazards offers material scientists and chemical engineers a well-rounded guide to utilizing particle and powder processes for a rapidly expanding array of applications.

Handbook of Modern Coating Technologies: Advanced Characterization Methods reviews advanced characterization methods of modern coating technologies. The topics in this volume consist of scanning vibrating electrode technique, spectroscopic ellipsometry, advances in X-ray diffraction, neutron reflectivity, micro- and nanoprobes, fluorescence technique, stress measurement methods in thin films, micropotentiometry, and localized corrosion studies.

All materials have voids in them, at some scale. Sometimes the voids are ignored, sometimes they are taken into account, and other times they are the focal point of the research. Voids in Materials: From Unavoidable Defects to Designed Cellular Materials takes due notice of all these occurrences, whether designed or unavoidable defects. We define, categorize, and characterize the voids (or empty spaces in materials) and we analyze the effects they have on material properties. This second edition is an updated and expanded central reference for voids in materials and covers all types of voids, intrinsic and intentional, and stochastic and nonstochastic, and the processes and conditions that are needed to create them and is a valuable resource to students in the areas of mechanical engineering, chemical engineering, materials science and engineering, physics, and chemistry, as well as scientists, researchers, and engineers in industry.

Bringing together the leading European expertise in behaviour and design of silos, this important new book is an essential reference source for all concerned with current problems and developments in silo technology. Silos are used in an enormous range of industries and the handling characteristics of many industrial materials require different approaches for successful, economical installations. For the first time, the many approaches taken by specialists in different fields are brought together in a unified way so that common problems can be addressed.
This book is the result of a four-year European project - Concerted Action - Silos - funded under the Brite Euram programme which has involved over 100 expert engineers and researchers from all over Europe, in seven working groups.

eBook available with sample pages: 0203223519

Although sintering is an essential process in the manufacture of ceramics and certain metals, as well as several other industrial operations, until now, no single book has treated both the background theory and the practical application of this complex and often delicate procedure. In Sintering Theory and Practice, leading researcher and materials engineer Randall M. German presents a comprehensive treatment of this subject that will be of great use to manufacturers and scientists alike.

This practical guide to sintering considers the fact that while the bonding process improves strength and other engineering properties of the compacted material, inappropriate methods of control may lead to cracking, distortion, and other defects. It provides a working knowledge of sintering, and shows how to avoid problems while accounting for variables such as particle size, maximum temperature, time at that temperature, and other problems that may cause changes in processing.

The book describes the fundamental atomic events that govern the transformation from particles to solid, covers all forms of the sintering process, and provides a summary of many actual production cycles. Building from the ground up, it begins with definitions and progresses to measurement techniques, easing the transition, especially for students, into advanced topics such as single-phase solid-state sintering, microstructure changes, the complications of mixed particles, and pressure-assisted sintering. German draws on some six thousand references to provide a coherent and lucid treatment of the subject, making scientific principles and practical applications accessible to both students and professionals. In the process, he also points out and avoids the pitfalls found in various competing theories, concepts, and mathematical disputes within the field.

A unique opportunity to discover what sintering is all about—both in theory and in practice

What is sintering? We see the end product of this thermal process all around us—in manufactured objects from metals, ceramics, polymers, and many compounds. From a vast professional literature, Sintering Theory and Practice emerges as the only comprehensive, systematic, and self-contained volume on the subject.

Covering all aspects of sintering as a processing topic, including materials, processes, theories, and the overall state of the art, the book

• Offers numerous examples, illustrations, and tables that detail actual processing cycles, and that stress existing knowledge in the field
• Uses the specifics of various consolidation cycles to illustrate the basics
• Leads the reader from the fundamentals to advanced topics, without getting bogged down in various mathematical disputes over treatments and measurements
• Supports the discussion with critically selected references from thousands of sources
• Examines the sintering behavior of a wide variety of engineered materials—metals, alloys, oxide ceramics, composites, carbides, intermetallics, glasses, and polymers
• Guides the reader through the sintering processes for several important industrial materials and demonstrates how to control these processes effectively and improve present techniques
• Provides a helpful reference for specific information on materials, processing problems, and concepts

For practitioners and researchers in ceramics, powder metallurgy, and other areas, and for students and faculty in materials science and engineering, this book provides the know-how and understanding crucial to many industrial operations, offers many ideas for further research, and suggests future applications of this important technology.

This book offers an unprecedented opportunity to explore sintering in both practical and theoretical terms, whether at the lab or in real-world applications, and to acquire a broad, yet thorough, understanding of this important technology.

"Voids in Materials" treats voids of different shapes and forms in various materials, and examines their effects on material properties. The book covers the origins of voids in materials, how they are sometimes introduced in the form of hollow spheres, and the resultant properties of materials containing voids.

There are many books that focus on foams (which intentionally incorporate voids into materials) and that cover voids incidental to or unwanted in the fabrication of non-porous materials. In fact, all materials have voids. This book starts from the premise that voids are pervasive in all material on some level. It goes beyond foams to provide a comprehensive overview of voids, a central reference for scientists and engineers to use for the effect of voids in materials.
Includes 3D renderings of void geometriesExplains how and why voids are introduced into materials across the length scales; from nanometer-scale voids up to macro-scale voidsProvides a continuous picture of how material properties change as the volume fraction of voids increases, and the implications for product design

Written with both postgraduate students and researchers in academia and industry in mind, this reference covers the chemistry behind metal nanopowders, including production, characterization, oxidation and combustion. The contributions from renowned international scientists working in the field detail applications in technologies, scale-up processes and safety aspects surrounding their handling and storage.

Continuous crystallization is an area of intense research, with particular respect to the pharmaceutical industry and fine chemicals. Improvements in continuous crystallization technologies offer chemical industries significant financial gains, through reduced expenditure and operational costs, and consistent product quality. Written by well-known leaders in the field, The Handbook of Continuous Crystallization presents fundamental and applied knowledge, with attention paid to application and scaling up, and the burgeoning area of process intensification. Beginning with concepts around crystallization techniques and control strategies, the reader will learn about experimental methods and computational tools. Case studies spanning fine and bulk chemicals, the pharmaceutical industry, and employing new mathematical tools, put theory into context.

Low shear polymer powder processing provides unique solutions to many processing problems and offers a set of production techniques, frequently un-paralleled by other production methods. In recent years there has been increased interest in this field but no comprehensive review of the subject has been available until now. In this book, a team of experts have taken the novel approach of treating several processing techniques, such as compacted powder sintering, rotational moulding, powder coating, ram extrusion, and compression moulding, as diverse implementations of a single technology. The first chapters deal with the scientific and engineering fundamentals shared by various polymer powder processing techniques, and are followed by a detailed examination of each technique and some special effects. Polymer Powder Technology will prove invaluable to technologists, plastics and materials engineers, researchers and students working with various aspects of particulate polymer processing.

Powder metallurgy (PM) is a popular metal forming technology used to produce dense and precision components. Different powder and component forming routes can be used to create an end product with specific properties for a particular application or industry. Advances in powder metallurgy explores a range of materials and techniques used for powder metallurgy and the use of this technology across a variety of application areas.
Part one discusses the forming and shaping of metal powders and includes chapters on atomisation techniques, electrolysis and plasma synthesis of metallic nanopowders. Part two goes on to highlight specific materials and their properties including advanced powdered steel alloys, porous metals and titanium alloys. Part three reviews the manufacture and densification of PM components and explores joining techniques, process optimisation in powder component manufacturing and non-destructive evaluation of PM parts. Finally, part four focusses on the applications of PM in the automotive industry and the use of PM in the production of cutting tools and biomaterials.
Advances in powder metallurgy is a standard reference for structural engineers and component manufacturers in the metal forming industry, professionals working in industries that use PM components and academics with a research interest in the field.
Discusses the forming and shaping of metal powders and includes chapters on atomisation techniquesHighlights specific materials and their properties including advanced powdered steel alloys, porous metals and titanium alloysReviews the manufacture and densification of PM components and explores joining techniques

This handbook presents comprehensive coverage of the technology for conveying and handling particulate solids. Each chapter covers a different topic and contains both fundamentals and applications. Usually, each chapter, or a topic within a chapter, starts with one of the review papers. Chapter 1 covers the characterization of the particulate materials. Chapter 2 covers the behaviour of particulate materials during storage, and presents recent developments in storage and feeders design and performance. Chapter 3 presents fundamental studies of particulate flow, while Chapters 4 and 5 present transport solutions, and the pitfalls of pneumatic, slurry, and capsule conveying. Chapters 6, 7 and 8 cover both the fundamentals and development of processes for particulate solids, starting from fluidisation and drying, segregation and mixing, and size-reduction and enlargement. Chapter 9 presents environmental aspects and the classification of the particulate materials after they have been handled by one of the above-mentioned processes. Finally, Chapter 10 covers applications and developments of measurement techniques that are the heart of the analysis of any conveying or handling system.

Powder flow has attracted increased attention in recent years as novel formulated and functional products are being developed in powder forms, particularly in pharmaceutical and high value additive manufacturing industries. This book meets a need for a truly integrated modern treatment of dry powder flow, covering theory, robust characterisation techniques, modelling tools and applications. Written by leaders in the field, the book opens by introducing the wide range of powder processing problems faced by industry, the complexities of powders and the myriad of ways their flow behaviour can be characterised. The authors then move on, with contributions from experts, to describe fundamental properties that can be measured, defining the states of stress and shear rate and the considerations that need to be taken account. By providing a comprehensive treatment of all available characterisation techniques, as well as various modelling tools, the reader obtains a clear, practical overview. Case studies and applications connect theory to practical examples across a broad range of industries. This book stands out by not only providing the reader with guidance on what to measure but also how to interpret results, ensuring this is an invaluable text for anyone working on powder flow in the chemical, pharmaceutical and manufacturing industries, as well as students and researchers across chemical and process engineering disciplines.

When bombarded with X-rays, solid materials produce distinct scattering patterns similar to fingerprints. X-ray powder diffraction is a technique used to fingerprint solid samples, which are then identified and cataloged for future use—much the way the FBI keeps fingerprints on file. The current database of some 70,000 material prints has been put to a broad range of uses, from the analysis of moon rocks to testing drugs for purity.

Introduction to X-ray Powder Diffractometry fully updates the achievements in the field over the past fifteen years and provides a much-needed explanation of the state-of-the-art techniques involved in characterizing materials. It covers the latest instruments and methods, with an emphasis on the fundamentals of the diffractometer, its components, alignment, calibration, and automation.

The first three chapters outline diffraction theory in clear language, accessible to both students and professionals in chemistry, physics, geology, and materials science. The book's middle chapters describe the instrumentation and procedures used in X-ray diffraction, including X-ray sources, X-ray detection, and production of monochromatic radiation. The chapter devoted to instrument design and calibration is followed by an examination of specimen preparation methods, data collection, and reduction. The final two chapters provide in-depth discussions of qualitative and quantitative analysis.

While the material is presented in an orderly progression, beginning with basic concepts and moving on to more complex material, each chapter stands on its own and can be studied independently or used as a professional reference. More than 230 illustrations and tables demonstrate techniques and clarify complex material.

Self-contained, timely, and user-friendly, Introduction to X-ray Powder Diffractometry is an enormously useful text and professional reference for analytical chemists, physicists, geologists and materials scientists, and upper-level undergraduate and graduate students in materials science and analytical chemistry.

X-ray powder diffraction—a technique that has matured significantly in recent years—is used to identify solid samples and determine their composition by analyzing the so-called "fingerprints" they generate when X-rayed. This unique volume fulfills two major roles: it is the first textbook devoted solely to X-ray powder diffractometry, and the first up-to-date treatment of the subject in 20 years.

This timely, authoritative volume features:

• Clear, concise descriptions of both theory and practice—including fundamentals of diffraction theory and all aspects of the diffractometer
• A treatment that reflects current trends toward automation, covering the newest instrumentation and automation techniques
• Coverage of all the most common applications, with special emphasis on qualitative and quantitative analysis
• An accessible presentation appropriate for both students and professionals
• More than 230 tables and illustrations

Introduction to X-ray Powder Diffractometry, a collaboration between two internationally known and respected experts in the field, provides invaluable guidance to anyone using X-ray powder diffractometers and diffractometry in materials science, ceramics, the pharmaceutical industry, and elsewhere.

This book covers the rich phenomenology exhibited by fine powders when they are fluidized by a gas flow. Fine powder cohesiveness leads to poor flowability, clumping, difficulty in fluidizing, irregular avalanching behavior, etc. Despite all the inconveniences, fine powder processes pervade the chemical, pharmaceutical, agricultural and mining industries among others. The author in this book analyzes the mechanism by which interparticle adhesive forces are reduced by means of surface additives. Different techniques have been developed in the last years to assist fluidization by helping the gas flow to mobilize and break cohesive aggregates, which help to homogenize fluidization. As reviewed in this book, the use of these techniques may have a relevant impact on novel processes based on fluidized beds of fine powder and with relevant applications on leading edge technologies such as Atomic Layer Deposition on nanoparticles and CO2 capture by gas-fluidized beds of adsorbent powders. The study of fluidized beds has a marked interdisciplinary character. This book is thus intended for academic and industrial researchers in applied physics, mechanical, chemical, and environmental engineering, who are interested in the special characteristics of fine powders.