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1D Oxide Nanostructures Obtained by Sol-Gel and Hydrothermal Methods (Paperback, 1st ed. 2016)
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1D Oxide Nanostructures Obtained by Sol-Gel and Hydrothermal Methods (Paperback, 1st ed. 2016)
Series: SpringerBriefs in Materials
Expected to ship within 10 - 15 working days
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This book presents wet chemical sol-gel and hydrothermal methods
for 1D oxide nanostructure preparation. These methods represent an
attractive route to multifunctional nanomaterials synthesis, as
they are versatile, inexpensive and, thus, appropriate for
obtaining a wide range of oxide materials with tailored morphology
and properties. Three specific oxides (SiO2, TiO2, ZnO) are
discussed in detail in order to illustrate the principle of the
sol-gel and hydrothermal preparation of 1D oxide nanostructures.
Other oxides synthesized via this method are also briefly
presented. Throughout the book, the correlation between the tubular
structure and the physico-chemical properties of these materials is
highlighted. 1D oxide nanostructures exhibit interesting optical
and electrical properties, due to their confined morphology. In
addition, a well-defined geometry can be associated with chemically
active species. For example, the pure SiO2 nanotubes presented a
slight photocatalytic activity, while the Pt-doped SiO2 tubular
materials act as microreactors in catalytic reactions. In the case
of titania and titanate nanotubes, large specific surface area and
pore volume, ion-exchange ability, enhanced light absorption, and
fast electron-transport capability have attracted significant
research interest. The chemical and physical modifications
(microwave assisted hydrothermal methods) discussed here improve
the formation kinetics of the nanotubes. The ZnO nanorods/tubes
were prepared as random particles or as large areas of small,
oriented 1D ZnO nanostructures on a variety of substrates. In the
latter case a sol-gel layer is deposited on the substrate prior to
the hydrothermal preparation. Using appropriate dopants, coatings
of ZnO nanorods with controlled electrical behavior can be
obtained.
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