Janne Marie Soetbeer determines the optimal dynamical decoupling
(DD) scheme for efficient reduction of electron spin coherence loss
in model systems for spin labelled biomolecules depending on their
particular relaxation behavior. Extending the nth order DD scheme
to double electron-electron resonance (DEER) experiments require
the addition of multiple pump pulses for 1. Incomplete excitation
of pump spin packets introduce signal artefacts which are minimized
by pump pulse optimization including linear-chirp and asymmetric
hyperbolic secant pulses. Prolonging the dipolar evolution time
with decreased signal artefact allows to extent the measurable
interspin distances in biomolecules which were otherwise not
accessible due to spin echo relaxation.
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