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Investigation of Reactions Involving Pentacoordinate Intermediates - The Mechanism of the Wittig Reaction (Paperback, 2012 ed.)
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Investigation of Reactions Involving Pentacoordinate Intermediates - The Mechanism of the Wittig Reaction (Paperback, 2012 ed.)
Series: Springer Theses
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Total price: R2,821
Discovery Miles: 28 210
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In this thesis, the author outlines the discovery of an effect
common to representative examples of all Li salt-free Wittig
Reactions. The implications of such a universally applicable effect
are that all such Wittig reactions occur through the same
mechanism. Although the Wittig reaction was first discovered in
1953, its reaction mechanism has never been definitively settled
with many different variants proposed and disproved. The work in
this thesis shows conclusively that for [2+2] cycloadditions all
Wittig reactions occur by the same irreversible mechanism. In
addition, the author also describes a new chromatography-free
method for the removal of phosphine oxide from the alkene crude
product of the Wittig reaction. The work in this thesis has led to
several publications in high-profile journals.
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