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Analytical electron microscopy is one of the most powerful tools today for characterization of the advanced materials that support the nanotechnology of the twenty-first century. In this book the authors clearly explain both the basic principles and the latest developments in the field. In addition to a fundamental description of the inelastic scattering process, an explanation of the constituent hardware is provided. Standard quantitative analytical techniques employing electron energy-loss spectroscopy and energy-dispersive X-ray spectroscopy are also explained, along with elemental mapping techniques. Included are sections on convergent beam electron diffraction and electron holography utilizing the field emission gun. With generous use of illustrations and experimental data, this book is a valuable resource for anyone concerned with materials characterization, electron microscopy, materials science, crystallography, and instrumentation.
High-resolution electron microscopy (HREM) has become a most
powerful method for investigating the internal structure of
materials on an atomic scale of around 0.1 nm. The authors clearly
explain both the theory and practice of HREM for materials science.
In addition to a fundamental formulation of the imaging process of
HREM, there is detailed explanation of image
simulationindispensable for interpretation of high-resolution
images. Essential information on appropriate imaging conditions for
observing lattice images and structure images is presented, and
methods for extracting structural information from these
observations are clearly shown, including examples in advanced
materials. Dislocations, interfaces, and surfaces are dealt with,
and materials such as composite ceramics, high-Tc superconductors,
and quasicrystals are also considered. Included are sections on the
latest instruments and techniques, such as the imaging plate and
quantitative HREM.
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