This book explains the operating principles of atomic force microscopy with the aim of enabling the reader to operate a scanning probe microscope successfully and understand the data obtained with the microscope. This enhanced second edition to "Scanning Probe Microscopy" (Springer, 2015) represents a substantial extension and revision to the part on atomic force microscopy of the previous book. Covering both fundamental and important technical aspects of atomic force microscopy, this book concentrates on the principles the methods using a didactic approach in an easily digestible manner. While primarily aimed at graduate students in physics, materials science, chemistry, nanoscience and engineering, this book is also useful for professionals and newcomers in the field, and is an ideal reference book in any atomic force microscopy lab.

A comprehensive review of the latest fingerprint development and imaging techniques With contributions from leading experts in the field, Fingerprint Development Techniques offers a comprehensive review of the key techniques used in the development and imaging of fingerprints. It includes a review of the properties of fingerprints, the surfaces that fingerprints are deposited on, and the interactions that can occur between fingerprints, surfaces and environments. Comprehensive in scope, the text explores the history of each process, the theory behind the way fingerprints are either developed or imaged, and information about the role of each of the chemical constituents in recommended formulations. The authors explain the methodology employed for carrying out comparisons of effectiveness of various development techniques that clearly demonstrate how to select the most effective approaches. The text also explores how techniques can be used in sequence and with techniques for recovering other forms of forensic evidence. In addition, the book offers a guide for the selection of fingerprint development techniques and includes information on the influence of surface contamination and exposure conditions. This important resource: Provides clear methodologies for conducting comparisons of fingerprint development technique effectiveness Contains in-depth assessment of fingerprint constituents and how they are utilized by development and imaging processes Includes background information on fingerprint chemistry Offers a comprehensive history, the theory, and the applications for a broader range of processes, including the roles of each constituent in reagent formulations Fingerprint Development Techniques offers a comprehensive guide to fingerprint development and imaging, building on much of the previously unpublished research of the Home Office Centre for Applied Science and Technology.

This book provides an in-depth understanding of molecular recognition mechanisms in designing chromatographical processes for separations. The title explains the importance of chemistry in chromatography and molecule-molecule interaction mechanisms and extends the concepts of separation to isomers and chiral isomers.
"Chromatographic Separations Based on Molecular Recognition" discusses the theoretical interpretations of chromatographic retention processes, explains the molecular recognition concept for the separation of various isomers, and provides a foundation in separation science which will lead to a better grasp of other chemical fields and simplify the design and synthesis of novel stationary phases.

This book discusses fragmentation mechanisms of molecules under mass spectrometry conditions and the resulting peaks observed in ESI-MS/MS experiments. The underlying principles are used to understand everything from small molecules to biological poly-peptides collision induced dissociation. In a theoretical approach, gas phase reactivity of molecular ions is coupled with chemical dynamics simulations.

Stability is one of the most important performances required for silver halide photographic materials. In 1935, Dr. E. 1. Birr introduced the concept of the stabilization ofphotographic emulsions for the first time by inventing a most effective stabilizer, 4-oxo-6-methyl-l,3,3a,7-tetraazaindene (TAl). Dr. Birr's monograph Stabilization ofPhotographic Silver Halide Emulsions was published in 1974, and accepted as a reliable reference book by many photographic scientists and engineers. Since then, silver halide photographic materials have been greatly improved and expanded through active and continual development of various kinds of technologies. Especially, extensive efforts have been made to develop photographic materials with high sensitivity and rapid processing, which rely upon the stability ofphotographic emulsions under various conditions. Thus, the concept and technologies of stabilization ofphotographic silver halide materials have been expanded so extensively that many photographic scientists and engineers eagerly want a reliable, new reference book on the stabilization of photographic emulsions. Dr. Gunther Fischer is one of the most experienced and eminent scientists and engineers in the field of the stabilization of photographic materials with expanded concept. He has been involved in research on the stabilization of pho tographic emulsions since 1964 when he joined the Technical Scientific Laboratory in the Research and Development Department of the Photo Film Company Agfa Wolfen formerly headed by Dr. Birr, whom he succeeded in that position. I was deeply impressed by his fruitful and elaborate achievements in these fields."

This book presents recent research and advances in various solid-liquid separation technologies and some applications for treating produced water. It covers fundamental principles and the importance of produced water in major industrial sectors and compares solid-liquid separation technologies. In addition, this book Presents the results of research studies conducted to evaluate the performance of solid-liquid separation technologies Discusses a wide range of technologies, including membrane, filtration, crystallization, desalination, supercritical fluids, coagulation, and floatation Includes experimental, theoretical, modeling, and process design studies With its comprehensive coverage, this book is an essential reference for chemical researchers, scientists, and engineers in industry, academia, and professional laboratories. It is also an important resource for graduate and advanced undergraduate students studying solid-liquid separations.

Environmental Nanotechnology: Implications and Applications, Volume 99 focuses on the implications and applications of Environmental Nanotechnology. The book presents the various methods used for the production and characterization of nanoparticles, and includes chapters on Nanoparticles: An overview, Nanomaterials and photocatalysis for environment: Applications and characterization, Toxicity of inorganic nanoparticles, Overview of nanoparticles technology usage for water treatment with an emphasis on the emerging water pollutants, Nanotechnology in wastewater treatment, Nanomaterials for groundwater remediation, Development of nano-sensor and biosensor as an air pollution detection technique for the foreseeable future, and more. Additional chapters in this comprehensive release include Nanomaterials as a tool for soil remediation in sustainable agriculture, Impact of nanoparticles in wastewater treatment, Nanoparticles in solid waste: Impact and management strategies, and Global regulations and legislations on nanoparticles usage and application in diverse horizons.

Laboratory Experiments in Trace Environmental Quantitative Analysis is a collection of student-tested experiments that introduce important principles that underlie various laboratory techniques in the field of trace environmental organics and inorganics quantitative analysis. It crosses the more traditional academic disciplines of environmental science and analytical chemistry. The text is organized to begin with minimally rigorous session/experiments and increase in rigor as each session/experiment unfolds. Each experiment features learning objectives, expected student outcomes, and suggestions for further study. Additional features include: Students are introduced to the principles and laboratory practice of instrumental analysis (determinative techniques) that are clearly presented. Students are carefully taken through various ways to prepare samples for trace quantitative analysis (sample prep techniques). Safety warnings are listed within each experiment. Students are introduced to all three types of instrument calibration: external, internal and standard addition. Instructors who are responsible for laboratory courses in analytical chemistry with potential application to environmental sample matrices will find this textbook of value. Graduate programs in environmental science and engineering will also greatly benefit from the content.

This volume discusses the latest mass spectrometry (MS)-based technologies for proteoform identification, characterization, and quantification. Some of the topics covered in this book include sample preparation, proteoform separation, proteoform gas-phase fragmentation, and bioinformatics tools for MS data analysis. Written in the highly successful Methods in Molecular Biology series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and tips on troubleshooting and avoiding known pitfalls. Cutting-edge and comprehensive, Proteoform Identification: Methods and Protocols is a valuable resource for researchers in both academia and the biopharmaceutical industry who are interested in proteoform analysis using MS.

Covers the core principals of different biosensors, designing consideration and innovation to make biosensors for the analysis of food Focuses on principles, designing criteria and different types of biosensors involved in analysis of food samples Discusses practical issues to improve monitoring reliability and its linkage to more fundamental drivers of materials biocompatibility Provide biosensing analysis in Food Quality Analysis

This volume presents updated methods and new developments in the field of mass spectrometry imaging. Chapters guide readers through four parts covering imaging, software, data analysis, new instrumentation, and new methodological approaches. Written in the highly successful Methods in Molecular Biology series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and tips on troubleshooting and avoiding known pitfalls. Authoritative and cutting-edge, Mass Spectrometry Imaging of Small Molecules aims to be a useful practical guide to researchers to help further their study in this field.

Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics. Separate theoretical sections are provided for readers interested in spin-quantum mechanics, as are the appendices providing theoretical backgrounds in linear algebra, quantum mechanics, and angular momentum.
Following a systematic and rigorous description of all important 2D experiments (including the applications of pulsed field gradients), up-to-date coverage is given of three-dimensional and four-dimensional homo- and heteronuclear NMR experiments. The book provides original descriptions of complicated topics such as strong coupling, decoupling, and cross-polarization. The final chapter presents the basic concepts of relaxation, followed by an introduction to density operator relaxation theory.
Multidimensional NMR in Liquids is intended for chemists, biochemists, and others interested in studying molecular structure and dynamics with NMR spectroscopy. It also is suitable for use as a text in advanced undergraduate and graduate courses in NMR.

E = mc2 and the Periodic Table . . .

RELATIVISTIC EFFECTS IN CHEMISTRY

This century's most famous equation, Einstein's special theory of relativity, transformed our comprehension of the nature of time and matter. Today, making use of the theory in a relativistic analysis of heavy molecules, that is, computing the properties and nature of electrons, is the work of chemists intent on exploring the mysteries of minute particles.

The first work of its kind, Relativistic Effects in Chemistry details the computational and analytical methods used in studying the relativistic effects in chemical bonding as well as the spectroscopic properties of molecules containing very heavy atoms. The second of two independent volumes, Part B: Applications contains specific experimental and theoretical results on the electronic states of molecules containing very heavy atoms as well as their spectroscopic properties and electronic structures. The first one-volume catalog of comprehensive computational results, Part B details:

• the relativistic effects on the electronic structure of transition metal clusters, such as the Cu, Ag, and Au triad
• the electronic structure of open-shell transition metal clusters such as Rh3 and Ir3
• the electronic and spectroscopic properties of heteronuclear diatomics of main group p-block elements from Ga to Po, especially the diatomic hydrides, halides, and chalconides
• the clusters of the very heavy main group p-block elements from Ga to Po
• the relativistic effects on molecules containing lanthanide and actinide atoms, including metals inside fullerenes.

An extraordinary new examination of Periodic Table elements, Part B of Relativistic Effects in Chemistry is also evidence of the enduring influence of Einstein's revolutionary theory.

This book provides the readers with the full basic knowledge necessary to understand, evaluate and develop critically any ETAAS analysis. The book covers comprehensively all aspects of the theoretical principles, routine and unusual instrumentation, overlapping possibilities with other techniques and different analytical characteristics of ETAAS at an averaged intermediate/high level. This is a good topic for a text book owing to the wide analytical possibilities of ETAAS in academic and industry laboratories. The book is written by a qualified expert with 30 years' experience working on different aspects of ETAAS.The work guides the readers through an in-depth descriptive appraisal of the chemical and physical processes occurring in an ET atomiser. The work compares favourably with other books already published on this subject as this work shows an overview with some different perspectives, focusing mainly on the processes taking place during an ETAAS analysis. An ordered, rigorous and deep description is found in every chapter. The book would be adequate for undergraduate and graduate students in any course of analytical chemistry, researchers in analytical atomic spectrometry and analysts who routinely use ETAAS. Amateurs and specialists in this field will find a good support in the book.

This book describes the state of the art across the broad range of spectroscopic techniques used in the study of biological systems. It reviews some of the latest advances achieved in the application of these techniques in the analysis and characterization of small and large biological compounds, covering topics such as VUV/UV and UV-visible spectroscopies, fluorescence spectroscopy, IR and Raman techniques, dynamic light scattering (DLS), circular dichroism (CD/SR-CD), pulsed electron paramagnetic resonance techniques, Moessbauer spectroscopy, nuclear magnetic resonance, X-ray methods and electron and ion impact spectroscopies. The second part of the book focuses on modelling methods and illustrates how these tools have been used and integrated with other experimental and theoretical techniques including also electron transfer processes and fast kinetics methods. The book will benefit students, researchers and professionals working with these techniques to understand the fundamental mechanisms of biological systems.

This work pursues a novel route to functionalizing large surfaces with hybrid nanoparticles. It also casts new light on the combined use of surface plasmon resonance and X-rays. SPR spectroscopy is employed to study Au-based plasmonic nanostructures fabricated by novel methods, and a new experimental device is developed combining SPR with X-ray absorption spectroscopy at a synchrotron beamline. Using the new SPR-XAS setup developed in this work, the author has studied in-situ and real-time effects of X-ray irradiation in materials such as glasses and Co-phthalocyanines.

In this unique textbook and reference source, the authors integrate theoretical and applied research from a host of disciplines, including materials science, plasma physics, and advanced transport phenomena. Volume 1, the first of two, covers the fundamentals of plasma physics and gaseous electronics, thermodynamics, and transport properties of plasma.

This book focuses on nanomaterials with antibacterial properties. Antibacterial resistance is a growing concern that poses a serious threat to public health worldwide. This book looks at the fabrication, material's properties, and characterization of a range of metallic, bimetallic, and metal-oxide-based nanomaterials that can be exploited for their antimicrobial properties. A key focus of this book is its emphasis on 'green' synthesis of nanomaterials, as many conventional routes of nanomaterial fabrication do not fulfill key sustainability criteria in terms of their toxicity and lack of eco-friendliness. Additionally, this book introduces the application of nanoparticles to veterinary medicine. Given the ever-increasing global livestock population coupled with the emergence of drug-resistant pathogens of animal origin (bacterial, parasitic, and hemoprotozoa), the use of nanoparticles as antibacterial agents represents a paradigm shift in every aspect of veterinary care. Authored by scholars with combined expertise in nanomaterials and veterinary medicine, this book provides valuable information for researchers working on sustainable nanomaterials with antibacterial properties.

This book discusses chemometric methods for spectroscopy analysis including NIR, MIR, Raman, NMR, and LIBS, from the perspective of practical applied spectroscopy. It covers all aspects of chemometrics associated with analytical spectroscopy, including representative sample selection algorithm, outlier detection algorithm, model updating and maintenance algorithm and strategy and calibration performance evaluation methods.To provide a systematic and comprehensive overview the latest progress of chemometric methods including recent scientific research and practical applications are presented. In addition the book also highlights the improvement of classical algorithms and the extension of common strategies. It is therefore useful as a reference book for researchers engaged in analytical spectroscopy technology, chemometrics, analytical instruments and other related fields.

The book covers different techniques and methodologies involved in the nutritional quality analysis of forages. It also discusses the nutritional quality, anti-nutritional components, factors affecting forage quality, feed processing and conservation. Different techniques and methodologies have been presented in a simplified manner. The book has been divided in separate chapters and each chapter discusses different aspect of forage quality. Further, the book also covers the topics on conservation and processing of forages and management techniques for improving the forage nutritional quality. This book is an essential source of information for research scholars, post-graduate students and scientists working on forage quality estimation and also in livestock and dairy industries.

Here, the authors introduce readers to solving molecular structure elucidation problems using the expert system ACD/Structure Elucidator. They explain in detail the concepts of the Computer-Assisted Structure Elucidation (CASE) approach and point out the crucial role of understanding the axiomatic nature of the data used to deduce the structure. Aspects covered include the main blocks of the expert system and essential features of the mathematical algorithms used. Graduate and PhD students as well as practicing chemists are provided with a detailed explanation of the various practical approaches depending on available spectral data peculiarities and the complexity of the unknown structure. This is supported by a large number of real-world completed examples, most of which are related to the structure elucidation of natural product molecules containing unusual skeletons. Dedicated software and further supplementary material are available at www.acdlabs.com/TeachingSE.

"Hills is probably the best person I can think of to write this book. He has the deepest background combined with considerable experience in solving problems with food." —R. G. Bryant, University of Virginia.

Food scientists have many excellent tools at their disposal with which to study food at both the micro- and macrostructural levels. But, when it comes to analyzing dynamic structural changes in food during processing and storage, none can compare with magnetic resonance imaging (MRI). Still a very young approach, MRI food imaging has contributed greatly to recent advances in food science, and promises to yield much more valuable information in the years ahead. Written by a leading pioneer in the field, Magnetic Resonance Imaging in Food Science covers the latest in MRI food imaging theory and practice.

Written primarily for food scientists and engineers, the book offers a practical, unified approach to the subject. Material is organized in three main parts corresponding to the distances of scale probed by MRI studies—namely, the macroscopic, microscopic, and macromolecular. Throughout, the emphasis is on ways in which studies of food undergoing processes can be modeled using the equations of heat, mass, and momentum transport, and how those models can be used in process design optimization programs.

Magnetic Resonance Imaging in Food Science provides researchers with the most up-to-date, detailed coverage of:

• Traditional and cutting-edge MRI food imaging techniques and technologies, including STRAFI, gradient-echo imaging, and functional imaging
• Whole plant functional imaging, flow imaging and rheology, and other specialized MRI applications
• The roles of food microstructure and molecular relaxation mechanisms in controlling moisture and heat transport
• Techniques for modeling structural changes during food processing.

Magnetic Resonance Imaging in Food Science is an important working resource for all researchers engaged in the never-ending struggle to produce safer, higher-quality foods more efficiently.

Now a routine tool in biomedical and life science research, live cell imaging has made major progress enabling this core biochemical, cell, and molecular biology technique to become even more powerful, versatile, and affordable. In Live Cell Imaging: Methods and Protocols, a panel of expert contributors provide a comprehensive compendium of experimental approaches to live cell imaging in the form of several overview chapters followed by representative examples and case studies covering different aspects of the most current methodology. By examining a range of state-of-the-art protocols extensively validated in complex biological studies, this volume highlights new experimental and instrumental opportunities and helps researchers to select appropriate imaging methods for their specific biological questions and measurement tasks. Written in the highly successful Methods in Molecular BiologyT series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and notes on troubleshooting and avoiding known pitfalls. Authoritative and cutting-edge, Live Cell Imaging: Methods and Protocols promises to contribute greatly to the further development and dissemination of this fundamentally important technology which spans across many disciplines including molecular and cell biology, chemistry, physics, optics, engineering, cell physiology, and medicine. Written for: Molecular and cellular biologists, chemists, physicists, optics specialists, engineers, cell physiologists, and medical doctors

Serves as a practical reference for those involved in Secondary Ion Mass Spectrometry (SIMS)- Introduces SIMS along with the highly diverse fields (Chemistry, Physics, Geology and Biology) to it is applied using up to date illustrations- Introduces the accepted fundamentals and pertinent models associated with elemental and molecular sputtering and ion emission- Covers the theory and modes of operation of the instrumentation used in the various forms of SIMS (Static vs Dynamic vs Cluster ion SIMS)- Details how data collection/processing can be carried out, with an emphasis placed on how to recognize and avoid commonly occurring analysis induced distortions- Presented as concisely as believed possible with All sections prepared such that they can be read independently of each other

This book introduces the reader to thermal field-flow fractionation and discusses its advantages over the fundamental problems associated with traditional column-based analytical techniques commonly used to characterize polymers and macromolecules. The authors discuss the theoretical background, equipment, experimental procedures as well as the recent advances and applications of thermal field-flow fractionation. Complete with several practical examples and troubleshooting guidelines, the book is written for beginners and experienced separation scientists alike and will enable its readers to optimize their experimental conditions for their specific separation needs and problems.