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Developments in Polymer Characterization (Hardcover, 1986 ed.)
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Developments in Polymer Characterization (Hardcover, 1986 ed.)
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The policy adopted in Volume 1 of this series of including a
relatively small number of topics for detailed review has been
continued here. The techniques selected have received considerable
attention in recent years. F or this reason and because of the
significance of the characterisation data, further coverage of 13C
nuclear magnetic resonance spectroscopy and small angle neutron
scattering is given in the first two chapters. In Chapter I a large
part of the review describes the determination of monomer sequence
distributions and configurational sequences in copolymers formed
from more than one polymerisable monomer. The review on neutron
scattering (Chapter 2) is directed towards the determination of the
chain conformation in semi-crystaIIine polymers, which has provided
important results for the interpretation of chain folding and
morphology in crystaIIisable polymers. Laser Raman spectroscopy has
also been used for morphological studies, and this application
together with a description of the theoretical and experimental
aspects of the technique is given in Chapter 3. X-ray photoelectron
spectroscopy because of its extreme sensitivity to surface
characteristics has provided information on polymeric solids that
could not be obtained by other techniques. The principles and
practice of this ESCA technique, including its use for simple
elemental analysis, structural elucidation and depth profiling, are
described in Chapter 4. The final two chapters are mainly concerned
with the chain conformation of polymers in dilute solution.
Ultrasonic techniques (Chapter 5) show pmmise for observing the
dynamics of conformational changes.
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