Long gone are the days when synthetic publications included
parallel preparative experiments to document reproducibility of the
experimental protocols and when journals required such
documentation. The new Proven Synthetic Methods Series addresses
concerns to chemists regarding irreproducibility of synthetic
protocols, lack of characterization data for new compounds, and
inflated yields reported in many chemical communications-trends
that have recently become a serious problem.
Volume One of Carbohydrate Chemistry: Proven Synthetic Methods
includes more detailed versions of protocols previously published
for the synthesis of oligosaccharides, C-glycosyl compounds, sugar
nucleotides, click chemistry, thioglycosides, and thioimidates,
among others. The compilation of protocols covers both common and
less frequently used synthetic methods as well as examples of
syntheses of selected carbohydrate intermediates with general
utility. The major focus of this book is devoted to the proper
practice of state-of-the-art preparative procedures, including:
- References to the starting materials used, reaction setup,
work-up and isolation of products, followed by identification and
proof of purity of the final material
- General information regarding convenience of operation and
comments on safety issues
- Versatile and practically useful methods that have not received
deserved, long-lasting recognition or that are difficult to access
from their primary sources
- Copies of 1D NMR spectra of compounds prepared, showing purity
of materials readers can expect
Exploring carbohydrate chemistry from the academic points of
view, the Carbohydrate Chemistry: Proven Synthetic Methods Series
provides a compendium of preparatively useful procedures checked by
chemists from independent research groups.
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