This work-book will guide you safely, in step-by-step descriptions,
through every detail of the NMR experiments within, beginning with
1D routine experiments and ending with a series of advanced 3D
experiments on a protein: Which experiment can best yield the
desired information?How must the chosen experiment be performed?How
does one read the required information from the spectrum?How does
this particular pulse sequence work?Which other experiments give
similar information?
This third edition of the book, following its two highly
successful predecessors, has been revised and expanded to 206
experiments. They are organized in 15 chapters, covering test
procedures and routine spectra, variable temperature measurements,
the use of auxiliary reagents, 1D multipulse experiments, spectra
of heteronuclides, and the application of selective pulses. The
second and third dimensions are introduced using pulsed field
gradients, and experiments on solid state materials are described.
A key part describes 3D experiments on the protein ubiquitin with
76 amino acids.
What is new in this third edition?
1. 24 new experiments have been inserted into the 14 chapters
that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET,
DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved
HMBC, (1,1)- and (1, n)-ADEQUATE, STD, REDOR, and HR-MAS.
2. 20 new protein NMR experiments have been specially devised
and are collected in the newly added Chapter 15, ProteinNMR, for
which one needs a special model sample: fully 13C- and 15N-labeled
human ubiquitin. Techniques used include the constant time
principle, the PEP method, filters, gradient selection, and the
echo/anti-echo procedure.
The guide has been written by experts in this field, following
the principle of learning by doing: all the experiments have been
specially performed for this book, exactly as described and shown
in the spectra that are reproduced. Being a reference source and
work-book for the NMR laboratory as well as a textbook, it is a
must for every scientist working with NMR, as well as for students
preparing for their laboratory courses.
General
Imprint: |
Wiley-VCH Verlag GmbH
|
Country of origin: |
Germany |
Release date: |
June 2004 |
First published: |
August 2004 |
Authors: |
S. Berger
|
Dimensions: |
243 x 172 x 47mm (L x W x T) |
Format: |
Paperback
|
Pages: |
854 |
Edition: |
3rd Ed. |
ISBN-13: |
978-3-527-31067-8 |
Categories: |
Books >
Science & Mathematics >
Chemistry >
General
|
LSN: |
3-527-31067-3 |
Barcode: |
9783527310678 |
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