Materials syntheses are generally more complex than syntheses of
inorganic or organic compounds, and specific characterization
methods play a more important role. Materials synthesis protocols
often suffer from unclarities, irreproducibility, lack in detail
and lack in standards. The need to change this situation is the
main motivation for this book. A number of detailed protocols has
been collected, ranging from organic polymers to carbonaceous and
ceramic materials, from gels to porous and layered materials and
from powders and nanoparticles to films. Preparation methods
include intercalation and flux methods, sol-gel processing,
templating methods for porous materials, sonochemistry or spray
pyrolysis.
Each contribution provides detailed and unambiguous description
of the hardware, specific characteristics of the procedure, scope
of applicability as well as methods that unequivocally identify and
characterize the material and allow checking whether the synthesis
was successful.
General
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