This book describes the various aspects of microbore column chromatography. It provides readers with an in-depth understanding of the supercritical fluid chromatography and microbore high-performance liquid chromatography.

This timely book provides a succinct summary of methods for the synthesis of bioactive heterocycles using a multicomponent reaction (MCR) approach. The majority of pharmaceuticals and biologically active agrochemicals are heterocycles while countless additives and modifiers used in industrial applications are heterocyclic in nature. With the recent introduction of high-throughput biological evaluation, the importance of MCRs for drug discovery has been recognized and considerable efforts have been focused especially on the design and development of multi-component procedures for the generation of various bioactive heterocycles due to their significant therapeutic potential.

Nitroalkenes have often been referred to as "synthetic chameleons" owing to their reactivity, synthetic utility and biological significance. In the last two decades, the reactivity of nitroalkenes as substrates in diverse catalytic asymmetric transformations has been of tremendous interest on account of the powerful abilities of the nitro group to coordinate and withdraw electrons, as well as its amenability to undergo a wide variety of synthetic transformations. Although numerous original articles and reviews have appeared in the literature, a monograph providing a comprehensive coverage of this topic was conspicuous by its absence. This book features: A systematic, up-to-date, in-depth and well-organized compilation, spread over 12 chapters, of various catalytic asymmetric reactions of nitroalkenes with diverse substrates reported to date A wide coverage of reactions such as Michael additions, Friedel-Crafts reactions, cycloadditions, asymmetric reductions, multicomponent and cascade reactions, as well as other miscellaneous reactions Various chiral organo, metal and even biocatalysts involved in the stereoselective synthesis of multifunctional adducts via catalytic asymmetric reactions of nitroalkenes Schemes and figures detailing all the reagents, reaction conditions and product profiles Mechanistic details, including transition state models, which will be useful for effective catalytic design This book will be an invaluable resource for those who are working in the area of asymmetric catalysis and synthetic methodologies.

This book focuses on flame retardants (FR) for textile materials. It discusses basics of flame retardancy and flammability and covers various types of flame retardants and materials, including natural FRs, halogen, phosphorous, and nanomaterial-based FRs. This book also discusses methods of applications of FRs and discusses FRs and the environment. Covers a variety of interdisciplinary applications in the textile industry Emphasizes environmental aspects Reports on a large number of FR compounds studied globally Discusses in detail recent developments in halogen-free eco-friendly flame retardants Extensively describes basic aspects of flame retardancy and their measurements Aimed at the practitioner and textile engineering professional this work aims to ensure development of safe textile materials for various uses, including apparel, protective wear, floor coverings, upholstery, drapery, and others.

Finite Element Analysis of Weld Thermal Cycles Using ANSYS aims at educating a young researcher on the transient analysis of welding thermal cycles using ANSYS. It essentially deals with the methods of calculation of the arc heat in a welded component when the analysis is simplified into either a cross sectional analysis or an in-plane analysis. The book covers five different cases involving different welding processes, component geometry, size of the element and dissimilar material properties. A detailed step by step calculation is presented followed by APDL program listing and output charts from ANSYS. Features: Provides useful background information on welding processes, thermal cycles and finite element method Presents calculation procedure for determining the arc heat input in a cross sectional analysis and an in-plane analysis Enables visualization of the arc heat in a FEM model for various positions of the arc Discusses analysis of advanced cases like dissimilar welding and circumferential welding Includes step by step procedure for running the analysis with typical input APDL program listing and output charts from ANSYS.

Researchers in chemistry, chemical engineering, pharmaceutical science, forensics, and environmental science make routine use of chemical analysis, but the information these researchers need is often scattered in different sources and difficult to access. The CRC Handbook of Basic Tables for Chemical Analysis: Data-Driven Methods and Interpretation, Fourth Edition is a one-stop reference that presents updated data in a handy format specifically designed for use when reaching a decision point in designing an analysis or interpreting results. This new edition offers expanded coverage of calibration and uncertainty, and continues to include the critical information scientists rely on to perform accurate analysis. Enhancements to the Fourth Edition: Compiles a huge array of useful and important data into a single, convenient source Explanatory text provides context for data and guidelines on applications Coalesces information from several different fields Provides information on the most useful "wet" chemistry methods as well as instrumental techniques, with an expanded discussion of laboratory safety Contains information of historical importance necessary to interpret the literature and understand current methodology. Unmatched in its coverage of the range of information scientists need in the lab, this resource will be referred to again and again by practitioners who need quick, easy access to the data that forms the basis for experimentation and analysis.

This introductory text develops the reader's fundamental understanding of core principles and experimental aspects underlying the operation of nanoelectronic devices. The author makes a thorough and systematic presentation of electron transport in quantum-confined systems such as quantum dots, quantum wires, and quantum wells together with Landauer-Buttiker formalism and non-equilibrium Green's function approach. The coverage encompasses nanofabrication techniques and characterization tools followed by a comprehensive exposition of nanoelectronic devices including resonant tunneling diodes, nanoscale MOSFETs, carbon nanotube FETs, high-electron-mobility transistors, single-electron transistors, and heterostructure optoelectronic devices. The writing throughout is simple and straightforward, with clearly drawn illustrations and extensive self-study exercises for each chapter. Introduces the basic concepts underlying the operation of nanoelectronic devices. Offers a broad overview of the field, including state-of-the-art developments. Covers the relevant quantum and solid-state physics and nanoelectronic device principles. Written in lucid language with accessible mathematical treatment. Includes extensive end-of-chapter exercises and many insightful diagrams.

Synthetic biology is a dynamic, young, ambitious, attractive, and heterogeneous scientific discipline. It is constantly developing and changing, which makes societal evaluation of this emerging new science a challenging task, prone to misunderstandings. Synthetic biology is difficult to capture, and confusion arises not only regarding which part of synthetic biology the discussion is about, but also with respect to the underlying concepts in use. This book offers a useful toolbox to approach this complex and fragmented field. It provides a biological access to the discussion using a 'layer' model that describes the connectivity of synthetic or semisynthetic organisms and cells to the realm of natural organisms derived by evolution.Instead of directly reviewing the field as a whole, firstly our book addresses the characteristic features of synthetic biology that are relevant to the societal discussion. Some of these features apply only to parts of synthetic biology, whereas others are relevant to synthetic biology as a whole. In the next step, these new features are evaluated with respect to the different areas of synthetic biology. Do we have the right words and categories to talk about these new features? In the third step, traditional concepts like "life" and "artificiality" are scrutinized with regard to their discriminatory power. This approach may help to differentiate the discussion on synthetic biology. Lastly our refined view is utilized for societal evaluation. We have investigated the public views and attitudes to synthetic biology. It also includes the analysis of ethical, risk and legal questions, posed by present and future practices of synthetic biology.This book contains the results of an interdisciplinary research project and presents the authors' main findings and recommendations. They are addressed to science, industry, politics and the general public interested in this upcoming field of biotechnology.

Autowave Plasticity: Localization and Collective Modes discusses the nature of plastic flow in solids associated with the development of a localized plastic flow. Written by an authority in the field, the author demonstrates how patterns of localized plastic flow are associated with autowave modes that are generated in a deformable sample and delivers a complete work on the subject. Key Features An original work on the nature of plastic flows in solids, particularly metals and crystals Focuses on plastic flow as an autowave process Contains elements of theories, experimental considerations, and numerical modeling This reference will help readers with creating experimental methods to observe or localize plastic flow and with the modeling of plastic flows. It is a valuable reference for graduate students and research specialists working in material science.

Creep and Creep Rupture of Metals is devoted to the fundamental description of the phenomenon of creep which occurs widely in high-temperature deformation of metals. Special attention is paid to the analysis of long-term strength, which characterizes the stress at which the metal does not fail after a predetermined time. The author details experimental and theoretical results obtained by Soviet and Russian scientists that are absent in currently available publications and demonstrates analytical methods and approaches to achieve long term strength in Metals.

In the adsorption phenomenon the substances from the external environment the gas or liquid are absorbed by a solid surface (adsorbent). Adsorption is used to separate gaseous and liquid mixtures, for drying and purification of gases and liquids. This reference broadly explores the calculation of the equilibrium and dynamic characteristics of adsorption in porous bodies at the molecular level. Two new theories of statistical physics are presented, both developed by the author for the consistent description of the equilibrium distribution of molecules and dynamics of flows in complex porous materials to be able to solve a wide range of practical tasks in the development of new technologies.

Completely revised and reorganized while retaining the approachable style of the first edition, Infrared Detectors, Second Edition addresses the latest developments in the science and technology of infrared (IR) detection. Antoni Rogalski, an internationally recognized pioneer in the field, covers the comprehensive range of subjects necessary to understand modern IR detector theory and technology. He presents each topic with a brief summary of historical background followed by summary of principles underlying performance, an overview of properties, and analysis of the state of the art. Divided into four sections, the book covers fundaments of IR detection, IR thermal detectors, IR photon detectors, and focal plane arrays. It begins with a tutorial introduction to essential of different types of IR detectors and systems. The author explores the theory and technology of different thermal detectors and then moves on to the theory and technology of photon detectors. He concludes his treatment with a discussion of IR focal plane arrays where relations between performance of detector array and infrared system quality are considered. New to the Second Edition: Fundamentals of IR detection, radiometry, and flux-transfer issues needed for IR detector and system analysis Major achievements and trends in the development of IR detectors Novel uncooled detectors such as cantilever, antenna, and optically coupled detectors Type II superlattice detectors Quantum dot IR detectors Terahertz (THz) arrays and new generation of IR detectors, so-called third generation detectors The author accomplishes the difficult task of making the information accessible to a wide readership. A comprehensive analysis of the latest developments in IR detector technology and basic insight into the fundamental processes important to evolving detection techniques, the book provides the most complete and up-to-date resource of its kind, including a summary of useful data, guide to the literature, and overview of applications.

Emulsions and Emulsion Stability, Second Edition provides comprehensive coverage of both theoretical and practical aspects of emulsions. The book presents fundamental concepts and processes in emulsified systems, such as flocculation, coalescence, stability, precipitation, deposition, and the evolution of droplet size distribution. The book explains how to predict emulsion stability and determine droplet sizes in a variety of emulsion systems. It discusses spontaneous emulsification and the formation of "nanoemulsions" as well as droplet-droplet interactions in different electrical fields (electrocoalescence), and the formulation, composition, and preparation variables that contribute to the inversion in emulsion systems. Several chapters emphasize applications such as emulsification encountered in oil spills, asphalt, chemical flooding, acid crude oils, and large-scale industrial wastewater treatment. The survey of experimental characterization methods highlights the importance of thin liquid films in colloidal systems and assesses different NMR applications, ultrasound characterization, video microscopy, and other on-line instrumentation. The last chapter in the book deals with obtaining conductivity measurements as an alternative to online instrumentation. Completely revised and expanded, this second edition of Emulsions and Emulsion Stability offers a well-rounded collection of knowledge that is applicable to all academic and industrial scientists and researchers in the fields of surfactant and emulsion science.

High surface area, a microporous structure, and a high degree of surface reactivity make activated carbons versatile adsorbents, particularly effective in the adsorption of organic and inorganic pollutants from aqueous solutions. Activated Carbon Adsorption introduces the parameters and mechanisms involved in the activated carbon adsorption of organic and inorganic compounds. This text brings together the most significant research on surface structure and processes, adsorption theories and isotherm equations, and applications from the latest literature on carbon adsorption. The book clearly explains the surface-related interactions of activated carbons, their energetics, and the applicability of adsorption isotherm equations and their deviation from adsorption data. It then explores numerous applications in a wide range of areas, such as nuclear technology, vacuum technology, food technology, pharmaceuticals and medicine, gas storage, oil refining, and environmental remediation. Topics include: oils and fats, molecular sieves, refining of liquid fuels, pesticides, dyes, drugs, and toxins. Three chapters are dedicated to environmental applications, including the adsorption of halogenated organic compounds and the removal of hazardous gases and vapors, organo-sulphur compounds, and other inorganic compounds from wastewater and groundwater. Activated Carbon Adsorption presents a complete survey of the growing number of state-of-the-art applications supported by a compilation of the latest perspectives in research concerning carbon surfaces and their adsorption processes from aqueous solutions. Its unified approach promotes further research towards improving and developing newer activated carbon adsorbents and processes for the efficient removal of pollutants from drinking water and industrial effluents.

An in-depth review of important preparative methods for the synthesis and chemical modification of polymers, this authoritative second edition examines the advantages and limitations of various polymerization applications and procedures. It features new approaches and innovative strategies from the most prominent industry and academic laboratories, reflecting the burgeoning role of polymers in modern science and technology. The book analyzes biodegradable polymers for biomedical applications; investigates the use of polyolefins, polymeric dienes, aromatic polyethers, polymides, and metal-containing macromolecules; and covers polymers of acrylic acid, methacrylic acid, and maleic acid.

From Reports in Volume 5: "Recently polymer blends have emerged as one of the most important areas of research activity in the field of polymer science and technology. Because of their satisfactory performance in meeting specific needs of the polymer industry, they have drawn considerable attention in replacing not only many conventional materials, but also some of the polymers that are in vogue. By suitably varying the blend compositions and manipulating the processing conditions, tailor-made products with a unique set of end use properties can be achieved at a much lower cost and within a shorter time than would have been necessary for the development of a new polymer. The usefulness of such blends increases with the increasing range of applications of this type of materials." (Chapter 4) "New and growing demands on polymeric materials cannot be satisfied in future by an assortment extension of basic polymers. Although the introduction of new major-use basic polymer is possible, it seems unlikely in view of current projected economic and technical considerations. On the other hand, new products based on the modification of existing polymers have and will continue to be fruitful areas for both scientific and commercial developments. The driving forces for these developments are: 1. Improved performance, 2. Reduced cost, 3. Present, pending and future legislation dealing with health and environmental issues." (Chapter 11)

This book presents an up to date ethical framework for radiological protection in medicine. It is consistent with the requirements of the system of radiation protection and with the expectations of medical ethics. It presents an approach rooted in the medical tradition, and alert to contemporary social expectations. It provides readers with a practical framework against which they can assess the safety and acceptability of medical procedures, including patients' concerns. It will be an invaluable reference for radiologists, radiation oncologists, regulators, medical physicists, technologists, other practitioners, as well as academics, researchers and students of radiation protection in medicine. Features: An authoritative and accessible guide, authored by a team who have contributed to defining the area internationally Includes numerous practical examples/clinical scenarios that illustrate the approach, presenting a pragmatic approach, rather than dwelling on philosophical theories Informed by the latest developments in the thinking of international organizations

Linear induction accelerators are successfully used as power supplies for numerous devices of relativistic high-frequency electronics. This book addresses ways to solve physical and engineering problems arising in the calculation, design, modeling and operation of linear induction accelerators intended for supplying relativistic microwave devices. It reviews and analyzes both classic and recent studies on the topic of linear induction accelerators (LIA) for generating and amplifying microwave radiation by relativistic devices.

The first book of its kind to highlight the unique capabilities of laser-driven acceleration and its diverse potential, Applications of Laser-Driven Particle Acceleration presents the basic understanding of acceleration concepts and envisioned prospects for selected applications. As the main focus, this new book explores exciting and diverse application possibilities, with emphasis on those uniquely enabled by the laser driver that can also be meaningful and realistic for potential users. It also emphasises distinction, in the accelerator context, between laser-driven accelerated particle sources and the integrated laser-driven particle accelerator system (all-optical and hybrid versions). A key aim of the book is to inform multiple, interdisciplinary research communities of the new possibilities available and to inspire them to engage with laser-driven acceleration, further motivating and advancing this developing field. Material is presented in a thorough yet accessible manner, making it a valuable reference text for general scientific and engineering researchers who are not necessarily subject matter experts. Applications of Laser-Driven Particle Acceleration is edited by Professors Paul R. Bolton, Katia Parodi, and Joerg Schreiber from the Department of Medical Physics at the Ludwig-Maximilians-Universitat Munchen in Munchen, Germany. Features: Reviews the current understanding and state-of-the-art capabilities of laser-driven particle acceleration and associated energetic photon and neutron generation Presents the intrinsically unique features of laser-driven acceleration and particle bunch yields Edited by internationally renowned researchers, with chapter contributions from global experts

III-V semiconductors have attracted considerable attention due to their applications in the fabrication of electronic and optoelectronic devices as light emitting diodes and solar cells. The electrical properties of these semiconductors can also be tuned by adding impurity atoms. Because of their wide application in various devices, the search for new semiconductor materials and the improvement of existing materials is an important field of study. Doping with impurities is a common method of modifying and diversifying the properties of physical and chemical semiconductors. This book covers all known information about phase relations in quaternary systems based on III-V semiconductors, providing he first systematic account of phase equilibria in quaternary systems based on III-V semiconductors and making research originally published in Russian accessible to the wider scientific community. Features: Contains up-to-date experimental and theoretical information Allows readers to synthesize semiconducting materials with predetermined properties Delivers a critical evaluation of many industrially important systems presented in the form of two-dimensional sections for the condensed phases

Amorphous-nanocrystalline alloys are a relatively new class of materials born from the rapid development of new technologies and different methods of producing amorphous and nanocrystalline powders and films, compacting, melt quenching, megaplastic deformation, implantation, laser, plasma, and other high-energy methods. This book considers methods of producing these materials (melt quenching, controlled crystallization, deformation effect, and pulse treatments (photon, laser and ultrasound), spraying thin films, and ion implantation). Theoretical and experimental studies describe plastic deformation mechanisms and physico-mechanical properties. Practical applications are also presented.

This reference is dedicated to the problem of time-temperature stability of amorphous (non-crystalline) metal alloys with strongly nonequilibrium structure and unique physical and mechanical properties that are obtained by quenching from the melt at a rate that exceeds one millions of degrees c.o.s. second. As a stability test, the behavior of the plasticity of amorphous alloys is studied. The book examines the fundamental characteristics of amorphous alloys, the basic laws of structural relaxation, generalized information about the phenomenon of the ductile-brittle transition (temper embrittlement), the development of physically justified methods of predicting the stability of the properties, and provides information about the attempts of controlling the structure for the purpose of suppressing or deceleration of the ductile-brittle transition and, as a consequence, increasing the temperature and temporal stability of the amorphous state.

This book offers unique coverage of the mechanical properties of nano- and micro-dispersed magnetic fluids. Magnetic fluids are artificially created materials that do not exist in the nature. Researchers developing materials and devices are keenly interested in their "mutually exclusive" properties including fluidity, compressibility, and the ability to magnetize up to saturation in relatively small magnetic fields. Applications of micro- and nanodispersed magnetic fluids include magnetic-seals, magnetically operated grease in friction units and supports, separators of non-magnetic materials, oil skimmers and separators, sensors of acceleration and angle, and gap fillers in loudspeakers.

Several statistical techniques are used for the design of materials through extraction of knowledge from existing data banks. These approaches are getting more attention with the application of computational intelligence techniques. This book illustrates the alternative but effective methods of designing materials, where models are developed through capturing the inherent correlations among the variables on the basis of available imprecise knowledge in the form of rules or database, as well as through the extraction of knowledge from experimental or industrial database, and using optimization tools.

Karstified rocks of different lithology cover more than 10% of the continental surface of our planet. It is known that some 20% or even a few percent more of the global population largely depends on karstic groundwater but in many karst areas all over the world there are limited natural resources including absence of drinking waters. The problems of water shortage, equitable water use or water protection from pollution, become more problematic when they come to transboundary regions. The Dinaric region is a classical karst area where created borders of newly established countries after the civil war in 1990s resulted with an urgent need to create ambience for sustainable water management. The project DIKTAS is one of the first ever attempts to establish sustainable integrated management principles in a transboundary karst aquifer of the magnitude of the Dinaric Karst System. This volume presents selected papers from the conference held in June 2014 in Trebinje, Bosnia & Herzegovina including presentations of some of the project's achievements but also number of other research results conducted in karst environments worldwide.