Essential NMR gives scientists and engineers an easy and quick refresher on their NMR knowledge and skills. At the same time, this primer and review affords lecturers material to provide a deliver a framework of basic know-how covering all fields of NMR, i.e. NMR methodology and hardware, chemical analysis, 2D-spectroscopy, NMR imaging, flow NMR, and quality-control NMR. Concise explanatory text, with the key information, is enhanced a color illustration that graphically reinforces understanding. Rigorous derivations are avoided in favor of intuitive arguments. No other teaching-and-learning text addresses all the different aspects of NMR in such a comprehensive and concise fashion.

Nuclear Magnetic Resonance (NMR) has been a fundamental player in the studies of superconducting materials for many decades. This local probe technique allows for the study of the static electronic properties as well as of the low energy excitations of the electrons in the normal and the superconducting state. On that account it has also been widely applied to Fe-based superconductors from the very beginning of their discovery in February 2008. This dissertation comprises some of these very first NMR results, reflecting the unconventional nature of superconductivity and its strong link to magnetism in the investigated compounds LaO1-xFxFeAs and LiFeAs.

Published between 1839 and 1852, this two-volume work records the contribution of William Scoresby (1789-1857) to magnetic science, a field he considered one of 'grandeur'. The result of laborious investigations into magnetism and (with James Prescott Joule) electromagnetism, Scoresby's work was particularly concerned with improving the accuracy of ships' compasses. A whaler, scientist and clergyman, he epitomised the contribution which could be made to exploration and science by provincial merchant mariners - men often less celebrated than their counterparts in the Royal Navy or in metropolitan learned societies. In addition to his pioneering work on magnetic science, Scoresby furthered knowledge of Arctic meteorology, oceanography and geography. Volume 2 records Scoresby's investigations into the problem of navigating on iron-built ships, the section on shipwrecks proving just how pressing this was.

Published between 1839 and 1852, this two-volume work records the contribution of William Scoresby (1789-1857) to magnetic science, a field he considered one of 'grandeur'. The result of laborious investigations into magnetism and (with James Prescott Joule) electromagnetism, Scoresby's work was particularly concerned with improving the accuracy of ships' compasses. A whaler, scientist and clergyman, he epitomised the contribution which could be made to exploration and science by provincial merchant mariners - men often less celebrated than their counterparts in the Royal Navy or in metropolitan learned societies. In addition to his pioneering work on magnetic science, Scoresby furthered knowledge of Arctic meteorology, oceanography and geography. Volume 1 considers the magnetism of steel and suggests ways to determine its quality and hardness.

Like the earth itself, the nucleus of an atom frequently rotates about an axis. Under the influence of a magnetic field the axis of rotation itself rotates. The rate of this 'precessional' motion is proportional to the strength of the magnetic field and usually lies in the region of radio-frequencies. If a collection of such nuclei is placed in a magnetic field is subjected to radio waves at exactly the frequency of precession, there is a resonance effect, which can be used to measure the frequency of the precession. This effect is called nuclear magnetic resonance. The subject concerns all physicists, particularly nuclear physicists and those interested in the solid state. It is of growing importance to chemists, metallurgists and electrical engineers and there have been some biological and geophysical applications. Nuclear magnetic resonance has already found considerable uses in the oil industry, in industries connected with magnet construction, isotope extraction, plastics and rubber.

This book discusses many advances in optical physic, and is aimed at advanced undergraduates taking courses in atomic physics, or graduate students in the fields of lasers, astrophysics, and physical chemistry. The book is intended mainly for experimentalists, and the interaction of electromagnetic radiation with free atoms is introduced using classical or semi-classical calculations wherever possible. Topics discussed include the spontaneous emission of radiation, stimulated transitions and the properties of gas and turnable dye lasers, and the physics and applications of resonance fluorescence, optical double resonance, optical pumping, and atomic beam magnetic resonance experiments.

The content of this volume has been added to "eMagRes" (formerly "Encyclopedia of Magnetic Resonance)" - the ultimate online resource for NMR and MRI. To date there is no single reference aimed at teaching the art of applications guided coil design for use in MRI. This" RF Coils for MRI" handbook is intended to become this reference.

Heretofore, much of the know-how of RF coil design is bottled up in various industry and academic laboratories around the world. Some of this information on coil technologies and applications techniques has been disseminated through the literature, while more of this knowledge has been withheld for competitive or proprietary advantage. Of the published works, the record of technology development is often incomplete and misleading, accurate referencing and attribution assignment being tantamount to admission of patent infringement in the commercial arena. Accordingly, the literature on RF coil design is fragmented and confusing. There are no texts and few courses offered to teach this material. Mastery of the art and science of RF coil design is perhaps best achieved through the learning that comes with a long career in the field at multiple places of employment...until now.

"RF Coils for MRI" combines the lifetime understanding and expertise of many of the senior designers in the field into a single, practical training manual. It informs the engineer on part numbers and sources of component materials, equipment, engineering services and consulting to enable anyone with electronics bench experience to build, test and interface a coil. The handbook teaches the MR system user how to safely and successfully implement the coil for its intended application. The comprehensive articles also include information required by the scientist or physician to predict respective experiment or clinical performance of a coil for a variety of common applications. It is expected that "RF Coils for MRI" becomes an important resource for engineers, technicians, scientists, and physicians wanting to safely and successfully buy or build and use MR coils in the clinic or laboratory. Similarly, this guidebook provides teaching material for students, fellows and residents wanting to better understand the theory and operation of RF coils.

Many of the articles have been written by the pioneers and developers of coils, arrays and probes, so this is all first hand information The handbook serves as an expository guide for hands-on radiologists, radiographers, physicians, engineers, medical physicists, technologists, and for anyone with interests in building or selecting and using RF coils to achieve best clinical or experimental results.

About "EMR Handbooks / eMagRes Handbooks"

The "Encyclopedia of Magnetic Resonance "(up to 2012) and" eMagRes "(from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of "EMR Handbooks / eMagRes Handbooks" on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from "eMagRes." In consultation with the "eMagRes" Editorial Board, the "EMR Handbooks / eMagRes Handbooks" are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of "eMagRes "at your fingertips Visit: www.wileyonlinelibrary.com/ref/eMagResView other "eMagRes" publications here

The new edition of this established workbook consists of worked examples and set problems that cover one- and two-dimensional NMR techniques applied to organic and inorganic systems. Most of the problems are genuine research examples, and this new edition contains eight pages of problems drawn from very recent research work. This second edition is fully compatible with the second edition of the highly successful Modern NMR Spectroscopy: a guide for chemists, and the two books are thoroughly cross referenced throughout.

The idea that a long-lived form of spin order, namely singlet order, can be prepared from nuclear spin magnetisation first emerged in 2004. The unusual properties of singlet order-its long lifetime and the fact that it is NMR silent but interconvertible into other forms of NMR active order-make it a 'smart tag' that can be used to store information for a long time or through distant space points. It is not unexpected then, that since its first appearance, this idea has caught the attention of research groups interested in exploiting this form of order in different fields of research spanning from biology to materials science and from hyperpolarisation to quantum computing. This first book on the subject gives a thorough description of the various aspects that affect the development of the topic and details the interdisciplinary applications. The book starts with a section dedicated to the basic theories of long-lived spin order and then proceeds with a description of the state-of-the-art experimental techniques developed to manipulate singlet order. It then concludes by covering the generalization of the concept of singlet order by introducing and discussing other forms of long-lived spin order.

In-cell NMR spectroscopy is a relatively new field. Despite its short history, recent in-cell NMR-related publications in major journals indicate that this method is receiving significant general attention. This book provides the first informative work specifically focused on in-cell NMR. It details the historical background of in-cell NMR, host cells for in-cell NMR studies, methods for in-cell biological techniques and NMR spectroscopy, applications, and future perspectives. Researchers in biochemistry, biophysics, molecular biology, cell biology, structural biology as well as NMR analysts interested in biological applications will all find this book valuable reading.

Muons, radioactive particles produced in accelerators, have emerged as an important tool to study problems in condensed matter physics and chemistry. Beams of muons with all their spins polarized can be used to investigate a variety of static and dynamic effects and hence to deduce properties concerning magnetism, superconductivity, molecular or chemical dynamics and a large number of other phenomena. The technique was originally the preserve of a few specialists located in particle physics laboratories. Today it is used by scientists from a very wide range of scientific backgrounds and interests. This modern, pedagogic introduction to muon spectroscopy is written with the beginner in the field in mind, but also aims to serve as a reference for more experienced researchers. The key principles are illustrated by numerous practical examples of the application of the technique to different areas of science and there are many worked examples and problems provided to test understanding. The book vividly demonstrates the power of the technique to extract important information in many different scientific contexts, all stemming, ultimately, from the exquisite magnetic sensitivity of the implanted muon spin.

Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known and applied by virtually every synthetically working Organic Chemist. Con- quently, the factors governing the differences in chemical shift values, based on chemical environment, bonding, temperature, solvent, pH, etc. , are well understood, and specialty methods developed for almost every conceivable structural challenge. Proton and carbon NMR spectroscopy is part of most bachelors degree courses, with advanced methods integrated into masters degree and other graduate courses. In view of this universal knowledge about proton and carbon NMR spectr- copy within the chemical community, it is remarkable that heteronuclear NMR is still looked upon as something of a curiosity. Admittedly, most organic compounds contain only nitrogen, oxygen, and sulfur atoms, as well as the obligatory hydrogen and carbon atoms, elements that have an unfavourable isotope distribution when it comes to NMR spectroscopy. Each of these three elements has a dominant isotope: 14 16 32 16 32 N (99. 63% natural abundance), O (99. 76%), and S (95. 02%), with O, S, and 34 14 S (4. 21%) NMR silent. N has a nuclear moment I = 1 and a sizeable quadrupolar moment that makes the NMR signals usually very broad and dif cult to analyse.

The combination of two leading imaging techniques - magnetic resonance imaging and positron emission tomography - is poised to have a large impact and has recently been a driver of research and clinical applications. The hybrid instrument is capable of acquiring both datasets simultaneously and this affords a number of advantages ranging from the obvious, two datasets acquired in the time required for one, through to novel applications. This book describes the basics of MRI and PET and then the technical issues and advantages involved in bringing together the two techniques. Novel applications in preclinical settings, human imaging and tracers are described. The book is for students and scientists entering the field of MR-PET with an MRI background but lacking PET or vice versa. It provides practical details from experts working in the area.

Characterisation Methods in Inorganic Chemistry provides a fresh alternative to the existing theoretical and descriptive inorganic chemistry texts by adopting a techniques-based approach and providing problem-solving opportunities to show how analytical methods are used to help us characterise inorganic compounds. The text covers the full range of analytical techniques employed by inorganic chemists, emphasizing those in most frequent use: NMR, diffraction, UV-Vis spectroscopy, and IR. The additional coverage on other techniques allows readers to study these less widely used methods when relevant to their specific course material. Each chapter follows a clear, structured format, which begins with a brief introduction to the technique and basic theory behind it before moving on to data collection and analysis, typical data and interpretation, with numerous worked examples, self- tests and problems. Online Resource Centre For registered adopters of the book: - Figures and tables of data from the book, ready to download - Additional problems and exercises For students: - Answers to self-test questions - Additional problems and data sets

Magnetic resonance (MR) makes use of tiny radio signals emitted by the nucleus of the atom. There are two important applications -- chemistry, where MR allows us to visualise the architecture of molecules, and medicine, where it provides a clear picture of human anatomy without the need for invasive surgery. This is the first unified treatment of Nuclear Magnetic Resonance (NMR) in chemistry and Magnetic Resonance Imaging (MRI) in medicine, written for a broad non-specialist readership by one of the world's foremost NMR spectroscopists.

Nuclear magnetic resonance spectroscopy (NMR spectroscopy) is a research technique that uses the magnetic properties of atomic nuclei to determine physical and chemical properties of atoms or the molecules in which they are contained. Proton NMR (1H NMR) is a technique that applies NMR spectroscopy specifically to the hydrogen-1 nuclei within the molecules of a substance, in order to determine the structure of that substance's molecules. The use of 1H NMR for the assignment of absolute configuration of organic compounds is a well-established technique. Recent research describes the technique's application to mono-, bi- and trifunctional compounds. In addition, several new auxiliary reagents, mono- and biderivatization procedures, on-resin methodologies and more recently, the use of 13C NMR, have been introduced to the field. In The Assignment of the Absolute Configuration by NMR using Chiral Derivatizing Agents: A Practical Guide, eminent Professor of Organic Chemistry Ricardo Riguera organizes this cutting-edge NMR research. Professor Riguera offers a short and usable guide that introduces the reader to the research with a plethora of details and examples. The book briefly explains the theoretical aspects necessary for understanding the methodology, dedicating most of its space to covering the practical aspects of the assignment, with examples and spectra taken from the authors' own experiments. Upper-level undergraduates, graduate students, and chemical researchers will find this guide useful for their studies and practice.

Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

This highly successful book, details the underlying principles behind the use of magnetic field gradients to image molecular distribution and molecular motion, providing many examples by way of illustration. Following excellent reviews of the hardback edition the book is now available in paperback.

Nuclear magnetic resonsance (NMR) spectrocopy is the most powerful research tool used in chemistry today, but many chemists have yet to realize its true potential. Recent advances in NMR have led to a formidable array of new techniques - and acronyms - which leaves even the professional spectroscopist bewildered. How, then, can chemists decide which approach will solve their particular structural or mechanistic problem?

This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic, and biological chemistry. It also contains much practical advice about the acquisition and use of spectra. Starting from the simple 'one pulse' sequence, the text employs a 'building block' approach to lead naturally to multiple pulse and two-dimensional NMR. Spectra of readily available compounds illustrate each technique. One- and two- dimensional methods are integrated in three chapters which show how to solve problems by making connections between spins through bonds, through space, or through exchange. There are also chapters on spectrum editing and solids. The final chapter contains a case history which attempts to weave the many strands of the text into a coherent strategy.

This second edition reflects the progress made by NMR in the past few years; there is a greater emphasis on inorganic nuclei; some two-colour spectra are used; the treatment of heteronuclear experiments has moved from direct to 'inverse' detection; many new examples and spectra have been included; and the literature to early 1992 has been covered.

An accompanying text, Modern NMR spectroscopy: A workbook of chemical problems, by Jeremy Sanders, Edwin Constable, and Brian Hunter, is available from OUP. Using a combination of worked examples and set problems, this workbook provides a practical guide to the accurate interpretation of NMR spectra, which will be of value to students and professional scientists alike.

The beautiful colors of many inorganic compounds, including minerals and gemstones, as well as the mysterious cold light of luminescence emitted by these materials, have attracted the inquisitiveness of natural philosophers for centuries. The scientific study of such phenomena - the optical spectroscopy of solids - has paid rich dividends in technological advances such as lasers and other optronic devices. This is a book on the art of optical spectroscopy of solids, establishing a theoretical and experimental framework for the subject, which is well illustrated with relevant spectra and experimental data.
Chapters 1 to 5 set down the quantum description of atoms, ions and defects in solids, and the interaction of such centers with electromagnetic radiation. Considerations of symmetry and the effects of lattice vibrations on the spectroscopic properties are treated in detail. The physical bases of prominent experimental techniques are presented in Chapter 6 and their application to color centers, dopant rare-earth and transition-metal ions are described in Chapters 7 -9. The spectroscopic behaviors of magnetic ions at high concentration are detailed in Chapter 10, followed by a brief review of the operational features of solid state lasers that rely on the foregoing discussion of their optical characteristics. Finally, Chapter 12 describes the application of magneto-optical double resonance techniques to the elucidation of the optical properties of insulating and semi-conducting materials. The authors emphasize that their own interests have guided the selection of topics from the panoply of available choices. They have written the book with senior undergraduates and postgraduates inmind: it is expected also to be useful to seasoned investigators from solid state physics and engineering from inorganic chemistry, and from materials and geological sciences.

This textbook is designed for graduate students to introduce the basic concepts of Nuclear Magnetic Resonance spectroscopy (NMR), spectral analysis and modern developments such as multidimensional NMR, in reasonable detail and rigor. The book is self-contained, so, a unique textbook in that sense with end of chapter exercises included supported by a solution manual. Some of the advanced topics are included as Appendices for quick reference. Students of chemistry who have some exposure to mathematics and physics will benefit from this book and it will prepare them to pursue research in different branches of Chemistry or Biophysics or Structural Biology.

Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.

This dictionary is the first to provide a comprehensive explanation of the bewildering array of acronyms and technical terms which have crept into the NMR literature in recent years. Aimed at chemists and biochemists who have only an elementary knowledge of NMR, it provides a clear description of the concepts and basic principles involved, including developments in two-dimensional NMR methods in liquids. Mathematical descriptions are used where appropriate, however the level of mathematical competence required is low, and the more complex aspects are fully explained in the text.

Each term is explained in full, extensive cross-references are included, and suggestions for further reading are included. The new and revised paperback edition of this well-received dictionary includes many new, up-to-date entries - for example, on three- and four-dimensional NMR.

Available in paperback for the first time, this book describes the main methods of one- and two-dimensional high-resolution NMR spectroscopy in liquids within the quantum-mechanical formalism of the density matrix. In view of the increasing importance of NMR in chemistry and biochemistry, it is particularly addressed to those scientists who do not have a working knowledge of quantum calculations.

From reviews of the hardback edition:

`The book fills a gap in the market...' Magnetic Resonance in Chemistry

'Goldman's book is important and timely, written in a thorough, careful manner. It treats a selected number of fundamental two-dimensional NMR experiments at a level appropriate for a general graduate course in two-dimensional NMR spectroscopy. Physics Today

Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and versatile techniques now available for the study of molecular structure and reaction mechanisms. This classic account of modern NMR spctroscopy was heralded on its publication in 1987 as `the lasting text of its age' Nature. Now available in paperback, it provides a thoroughly comprehensive review of modern NMR techniques and the underlying principles. The material is presented in an intuitive manner within a rigourous mathematical framework, and is extensively illustrated throughout. It is, without question, an essential purchase for the self-respecting NMR spectroscopist.