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Books > Science & Mathematics > Chemistry > Physical chemistry > Catalysis
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Rapid Production of Micro- and Nano-particles Using Supercritical Water (Paperback, 2010 ed.)
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Rapid Production of Micro- and Nano-particles Using Supercritical Water (Paperback, 2010 ed.)
Series: Engineering Materials
Expected to ship within 10 - 15 working days
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Thisbookistalkingabouthowtousesupercriticalwater(SCW)torapidlyproduce
micro- and nano-particles of metal oxides, inorganic salts, metals
and organics.
Itcoversbasicprinciples,experimentalmethodologiesandreactors,particlep-
duction,characterizationsandapplicationsaswellastherecentadvancement.
Fine
particlescanbeproducedbybothchemicalandphysicalprecipitationofproducts
from SCW. They can be used as catalysts, materials in ceramics and
electronic devices andcompositematerials.
Particlesareeasilyproduced continuouslyina
owreactorinshortreactiontimes(0. 4s?2min)butcanalsobesynthesizedin
batchreactorsforlongreactiontimes(e. g. ,12h).
Theycanbeeasilystudiedin-situ
microscopically(optical/IR/Raman/SR-XRD)inanopticalmicro-reactor,diamond
anvilcell.
Thesize,sizedistribution,crystalgrowth&structure,andmorphologyof
particlescanbecontrolledbychangingtheconcentrationsofstatingmaterials,pH,
pressures,temperatures,heating&coolingrates,organicmodi
cations,reducingor oxidizingatmospheres, owratesandreactiontimes.
Thisisthe rstbooktosystematicallyintroduceusingSCWforproductionof
neparticles.
Itisanidealreferencebookforengineers,researchersandgraduate
studentsinmaterialscienceandengineering. vii Acknowledgments I
would like to thank Drs. T. Ogi & T. Minowa (Biomass Technology
Research
Center,NationalInstituteofAdvancedIndustrialScienceandTechnology,Japan),
and Profs. K. Arai, H. Inomata, R. L. Smith Jr. and T. Adschiri
(Chemical
Engineering,TohokuUniversity,Japan),whoinitiallyintroducedthehydrothermal
andsupercritical uidsareastomewhenIworkedinJapanfrom1996to1999.
Thanks are also due to Profs. J. A. Kozinski, R. I. L. Guthrie
(Materials Engineering,McGillUniversity,Canada)andI. S.
Butler(Chemistry,McGill)for
theirguidanceinmyworkonhydrothermalprocessduringmyworkinCanadafrom
1999to2007. Profs. W. Bassett (Geological Sciences, Cornell
University) and D. Baker
(Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr.
I-Ming Chou(U. S.
GeologicalSurvey)forusefuldiscussionsofthepressurecalculation
procedure. Drs. M. Watanabe and T. Sato (Research Center of
Supercritical Fluid Technology, Tohoku University, Japan) for
discussions about the experimental set-upofthebatchand owreactors.
Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat
McGillinCanada. ix Contents 1 Introduction...1 1. 1 Background ...1
1. 2 RapidExpansionofSupercriticalSolution(RESS)Process ...4 1. 3
SupercriticalAntisolvent(SAS)Process ...4 1. 4
OtherPhysicalProcesses ...5 1. 5 SupercriticalWaterProcess ...5
References...8 2 Supercritical Water Process...11 2. 1 Introduction
...11 2. 2 BatchReactor ...15 2. 3 FlowReactor...18 2. 4
DiamondAnvilCell(DAC)...20 References...25 3 Metal Oxides
Synthesis...29 3. 1 Introduction ...29 3. 2 Boehmite(AlOOH) ...30
3. 3 Ferrites...31 3. 4 Phosphor(YAG) ...32 3. 5 LiCoO /LiMn O
...33 2 2 4 3. 6 Ce Zr O (x =0?1)...33 1?x x 2 3. 7
PotassiumHexatitanate,PotassiumNiobateandTitania ...35 3. 8
ZincOxide...38 3. 9 Nickel,Nickel/CobaltOxide...
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