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Books > Science & Mathematics > Science: general issues > Scientific equipment & techniques, laboratory equipment
Atomic Force Microscopy: Principles, Developments and Applications
presents Atomic Force Microscopy (AFM) as one of the most powerful
tools for the analysis of morphologies because it creates
three-dimensional images at the angstrom and nano scale. This
technique has been exhaustively used in the analyses of the
dispersion of nanometric components in nanocomposites and in
polymeric blends because of the easiness of the sample preparation
and lower equipment maintenance costs compared to the electron
microscopy. Contributions to different application areas using the
AFM are described, emphasizing the analysis of the morphology of
composites/nanocomposites and polymeric blends based on elastomeric
materials. Following this, the authors examine the basic concept of
DEP and its integration with AFM to generate DEP, as well as review
DEP-based AFM methods of imaging local electric polarizability with
nanoscale spatial resolution. The direct measurement of DEP
strength and polarity using a multi-pass AFM technique is
described, contributing to the optimization and calibration of DEP
integrated nano-devices for the effective control and manipulation
of target biomolecules. The combination of in situ AFM-study of
model crystals and ex situ-scanning of natural crystals makes it
possible to carry out a partial reconstruction of natural
crystallogenetics processes. With the use of these methods and
microtomography, the authors estimate the concentration of silica
in the mother solution at the time of capture of inclusions was
estimated for the first time. Next, a study is presented with the
goal of evaluating the morphology of surface asphalt films obtained
through spin coating and characterized by AFM. The samples were
pure asphalt and modified with two types of asphaltenes called
continental type and archipelago type. The asphaltene fractions in
the micellar system define the morphological stability of the
asphalt resulting from a contribution of all the existing forces
between the supramolecules of the system. The closing study
presents in situ AFM investigations of crystal dissolution. The
statistical data shows considerable differences in tangential
dissolution rate on the two spirals consisting of nine and four
screw dislocations.
This book describes modern focused ion beam microscopes and
techniques and how they can be used to aid materials metrology and
as tools for the fabrication of devices that in turn are used in
many other aspects of fundamental metrology. Beginning with a
description of the currently available instruments including the
new addition to the field of plasma-based sources, it then gives an
overview of ion solid interactions and how the different types of
instrument can be applied. Chapters then describe how these
machines can be applied to the field of materials science and
device fabrication giving examples of recent and current activity
in both these areas.
This book is written specifically for the students of intermediate
(or Higher Secondary) standard. Keeping in view of the standard of
their education, the book is written in simple and lucid language.
Each of the experiments written in the book comprises necessary
introductions and theoretical details alongwith stepwise procedure
for performing practicals, so that they can easily follow this book
in their Laboratory classes. Whenever needed the experiments are
followed by Viva-Vice questions along with their answers. These
questions will help the students to guide them for their college
practical examinations in advance.
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