Although many papers have been published describing methods for the
inorganic analysis of petroleum no book has previously appeared
devoted exclusively to this subject. The purpose of this work is to
provide a laboratory handbook for industrial analysts of various
degrees of professional training covering the determination of
those elements commonly occurring in various types of petroleum
products. The procedures represent, from the author's point of
view, a reasonable compromise among the usual conflicting interests
of speed, accuracy, and cost, and emphasize manufacturing rather
than research applications. CONTENTS: Introduction 1. The Inorganic
Components of Petroleum 2. Preparation of Samples for Inorganic
Analysis: Direct Ashing, Soft Ashing and Wet Oxidation, Direct Wet
Oxidation, Fusion with Pyrosulfate, The Oxygen Bomb, The Peroxide
Bomb, Sodium Dehalogenation, Extraction Methods, Combustion
Methods, Alkaline Sulfide Treatment, Direct Methods, Combustion
Tube, Emission Spectrograph, X-rays 3. Aluminum: Colorimetric
Determination, Gravimetric Determination 4. Arsenic 5. Barium:
Determination in New Lubricating Oils, Determination in Used
Lubricating Oils 6. Boron: Colorimetric Determination, Alkalimetric
Determination 7. Calcium: Determination in New Lubricating Oils and
Additives, Determination in Used Lubricating Oils, Estimation of
Smaller Concentrations 8. Chromium 9. Cobalt: Electrolytic
Determination, Volumetric Determination 10. Copper: Determination
in Gasoline, Determination in Naphthenate Driers, Determination in
Distillates, Determination in Used Lubricating Oils 11. The
Halogens: Peroxide Bomb Combustion, Sodium Dehalogenation,
Extraction Procedures, Wickbold Oxyhydrogen Combustion,
Potentiometric Determination of Bromide and Chloride, Colorimetric
Determination of Chloride, Volumetric Determination of Fluoride 12.
Iron: Determination in Distillates, Determination in Used
Lubricating Oils, Determination in Naphthenate Driers, Colorimetric
Determination, Volumetric Determination 13. Lead: Determination in
Naphthenate Driers, Determination in Light Distillates,
Determination in Lubricating Oils 14. Manganese 15. Molybdenum:
Determination in New Lubricating Oils, Determination in Used
Lubricating Oils 16. Nickel: Determination in Distillates,
Gravimetric Determination 17. Nitrogen: Determination of Total
Nitrogen by Kjeldahl Method, Determination of Basic Nitrogen,
Determination of Quaternary Ammonium Compounds 18. Phosphorus:
Decomposition by Ashing in Presence of Zinc Oxide, Colorimetric
Methods, Alkalimetric Determination of Phosphorus 19. Selenium:
Colorimetric Determination, Volumetric Determination 20. Silicon:
Determination in Synthetic Oils, Determination of Silica in Used
Lubricating Oils 21. Sodium: Decomposition of Sample by Direct
Ashing, Gravimetric Determination, Determination by Flame
Photometer 22. Sulfur: Determination by Peroxide Fusion Bomb,
Determination by Wickbold Oxyhydrogen Combustion 23. Vanadium:
Determination in Distillates, Determination in Fuel Oils,
Volumetric Determination 24. Zinc: Determination in Additives and
Naphthenate Driers, Determination in New and Used Lubricating Oils,
Potentiometric Determination, Gravimetric Determination; Appendix;
Wickbold Apparatus for Oxyhydrogen Combustion; Index
General
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