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Principles of High Resolution NMR in Solids (Paperback, 2nd ed. 1983. Softcover reprint of the original 2nd ed. 1983)
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Principles of High Resolution NMR in Solids (Paperback, 2nd ed. 1983. Softcover reprint of the original 2nd ed. 1983)
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The field of Nuclear Magnetic Resonance (NMR) has developed at a
fascinating pace during the last decade. It always has been an
extremely valuable tool to the organic chemist by supplying
molecular "finger print" spectra at the atomic level. Unfortunately
the high resolution achievable in liquid solutions could not be
obtained in solids and physicists and physical chemists had to live
with unresolved lines open to a wealth of curve fitting procedures
and a vast amount of speculations. High resolution NMR in solids
seemed to be a paradoxon. Broad structure less lines are usually
encountered when dealing with NMR in solids. Only with the recent
advent of mUltiple pulse, magic angle, cross-polarization,
two-dimen sional and multiple-quantum spectroscopy and other
techniques during the last decade it became possible to resolve
finer details of nuclear spin interactions in solids. I have felt
that graduate students, researchers and others beginning to get
involved with these techniques needed a book which treats the
principles, theo retical foundations and applications of these
rather sophisticated experimental techniques. Therefore I wrote a
monograph on the subject in 1976. Very soon new ideas led to the
developement of "two-dimensional spectroscopy" and
"multiple-quantum spectroscopy," topics which were not covered in
the first edition of my book. Moreover an exponential growth of
literature appeared in this area of research leaving the beginner
in an awkward situation of tracing back from a current article to
the roots of the experiment."
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