This book was developed with the goal of providing an easily understood text for those users of the scanning electron microscope (SEM) who have little or no background in the area. The SEM is routinely used to study the surface structure and chemistry of a wide range of biological and synthetic materials at the micrometer to nanometer scale. Ease-of-use, typically facile sample preparation, and straightforward image interpretation, combined with high resolution, high depth of field, and the ability to undertake microchemical and crystallographic analysis, has made scanning electron microscopy one of the most powerful and versatile techniques for characterization today. Indeed, the SEM is a vital tool for the characterization of nanostructured materials and the development of nanotechnology. However, its wide use by professionals with diverse technical backgrounds-including life science, materials science, engineering, forensics, mineralogy, etc., and in various sectors of government, industry, and academia-emphasizes the need for an introductory text providing the basics of effective SEM imaging.A Beginners' Guide to Scanning Electron Microscopy explains instrumentation, operation, image interpretation and sample preparation in a wide ranging yet succinct and practical text, treating the essential theory of specimen-beam interaction and image formation in a manner that can be effortlessly comprehended by the novice SEM user. This book provides a concise and accessible introduction to the essentials of SEM includes a large number of illustrations specifically chosen to aid readers' understanding of key concepts highlights recent advances in instrumentation, imaging and sample preparation techniques offers examples drawn from a variety of applications that appeal to professionals from diverse backgrounds.

In this book, the authors use molecular dynamics simulations to conduct a comprehensive study of the compression/superheating limit and phase transition of 2D (monolayer, bilayer, and trilayer) water/ice constrained in graphene nanocapillaries. When subjected to nanoscale confinement and under ultrahigh pressure, water and ice behave quite differently than their bulk counterparts, partly because the van der Waals pressure can spark a water-to-ice transformation, known as the metastability limit of two-dimensional (2D) liquids. From a mechanical standpoint, this liquid-to-solid transformation characterizes the compression limit (or metastability limit) of 2D water. The findings presented here could help us to better understand the phase behavior of 2D confined water/ice.

Written by experts in the field, this book describes advanced techniques for the chemical synthesis of functional organic nanoparticles and proposes new characterization and manipulation methods for single nanoparticles. Theoretical and experimental studies of the physical and chemical properties of organic particles, semiconductor particles and liquid droplets are reported. The text gives not only scientific details but also discusses the general and historical background, applications, and future perspectives. A clear interpretation of technical terms and concepts is included where necessary. The material for the book originates from the research activities of the collaboration project "Laser Chemistry of Single Organic Nanometer Particles" supported by the Ministry of Education, Science Sports and Culture of Japan. It is written primarily for graduate students, researchers and engineers.

This book covers the performance aspects of nanocomposite supercapacitor materials based on transition metal oxides, activated carbon, carbon nanotubes, carbon nanofibers, graphene and conducting polymers. It compares the performance of simple electrode materials versus binary and ternary composites, while highlighting the advantages and challenges of different supercapacitor electrode materials. This book is part of the Handbook of Nanocomposite Supercapacitor Materials. Supercapacitors have emerged as promising devices for electrochemical energy storage, playing an important role in energy harvesting for meeting the current demands of increasing global energy consumption. The handbook covers the materials science and engineering of nanocomposite supercapacitors, ranging from their general characteristics and performance to materials selection, design and construction. Covering both fundamentals and recent developments, this handbook serves a readership encompassing students, professionals and researchers throughout academia and industry, particularly in the fields of materials chemistry, electrochemistry, and energy storage and conversion. It is ideal as a reference work and primary resource for any introductory senior-level undergraduate or beginning graduate course covering supercapacitors.

This book addresses the application of nanotechnology to cosmetics. Edited by three respected experts in the field, the book begins with a general overview of the science behind cosmetics and skin care today, and of the status quo of nanotechnology in cosmetics. Subsequent chapters provide detailed information on the different nanoparticles currently used in cosmetics; the production and characterization of nanoparticles and nanocosmetics; and regulatory, safety and commercialization aspects. Given its scope, the book offers an indispensable guide for scientists in academia and industry, technicians and students, as well as a useful resource for decision-makers in the field and consumer organizations. Chapter 6 of this book is available open access under a CC BY 4.0 licence at link.springer.com.

This book presents peer-reviewed articles from the 1st International Conference on Trends in Modern Physics (TiMP 2021) held at Assam Don Bosco University in Guwahati, India, between February 26 and 27, 2021. This conference was the 3rd in a series of annual conferences of the Department of Physics, ADBU, with the 1st and 2nd being national conferences. The conference was jointly organized by the Department of Physics, ADBU, and the Indian Association of Physics Teachers (IAPT) to promote greater synergy between thematic areas of astrophysics and cosmology, plasma physics, material and nanophysics, nuclear physics, and particle physics

This thesis focuses on the design and synthesis of novel one-dimensional colloidal chalcogenide hetero-nanostructures for enhancing solar energy conversion applications. Semiconducting nanomaterials are particular attractive for energy conversion due to the quantum confinement effects dictating their unique optical and electronic properties. Steering the photo-induced charge-flow based on unique bandgap alignment in semiconductor heterojunctions is critical for photo-electric/chemical conversion. The author presents the controllable preparation strategies to synthesize 1D chalcogenide hetero-nanostructures with various fine structures, further been used as excellent template materials for preparing other novel and complex hybrid architectures through a series of chemical transformations. The heterogeneous growth mechanisms of novel hetero-nanostructures is studied for developing a facile and general method to prepare more novel heterostructures. The band gap structure simulations, detailed charge carrier behaviour and unique solar energy conversion properties of the prepared hybrid nanostructures are deeply investigated. This work would open a new door to rationally designing hybrid systems for photo-induced applications.

Volume 2 of the Handbook of Colloid and Interface Science is a survey into the theory of dispersions in a variety of fields, as well as characterization by rheology. It is an ideal reference work for research scientists, universities, and industry practitioners looking for a complete understanding of how colloids and interfaces behave in the areas of materials science, chemical engineering, and colloidal science.

This book focuses on the preparation and characterisation of polyvinyl alcohol (PVA)/ halloysite nanotube (HNT) bionanocomposite films with different HNT contents for potential use in food packaging. It examines the effect of material composition and nanofiller content on mechanical, thermal and optical properties in relation to their morphological structures, and also comprehensively describes the water resistance, biodegradation and migration rates of such bionanocomposites, as well as their barrier properties in terms of water vapour transmission, and water vapour, air and oxygen permeabilities. Further, this book discusses the use of Nielsen model and Cussler model to predict the relative permeability of bionanocomposites, demonstrating that Nielsen model is more effective and in better agreement with experimental data obtained. Lastly, it discusses the application of bionanocomposite films in food packaging to prolong the shelf life of freshly cut avocados and peaches.

This book highlights some of the latest advances in nanotechnology and nanomaterials from leading researchers in Ukraine, Europe and beyond. It features contributions presented at the 8th International Science and Practice Conference Nanotechnology and Nanomaterials (NANO2020), which was held on August 26-29, 2020 at Lviv Polytechnic National University, and was jointly organized by the Institute of Physics of the National Academy of Sciences of Ukraine, University of Tartu (Estonia), University of Turin (Italy), and Pierre and Marie Curie University (France). Internationally recognized experts from a wide range of universities and research institutions share their knowledge and key findings on material properties, behavior, and synthesis. This book's companion volume also addresses topics such as nano-optics, energy storage, and biomedical applications.

This book describes advanced research on the structures and photochemical properties of polyatomic molecules and molecular clusters having various functionalities under cold gas-phase conditions. Target molecules are crown ethers, polypeptides, large size protonated clusters, metal clusters, and other complex polyatomic molecules of special interest. A variety of advanced frequency and time-domain laser spectroscopic methods are applied. The book begins with the principle of an experimental setup for cold gas-phase molecules and various laser spectroscopic methods, followed by chapters on investigation of specific molecular systems. Through a molecular-level approach and analysis by quantum chemical calculation, it is possible to learn how atomic and molecular-level interactions (van der Waals, hydrogen-bonding, and others) control the specific properties of molecules and clusters. Those properties include molecular recognition, induced fitting, chirality, proton and hydrogen transfer, isomerization, and catalytic reaction. The information will be applicable to the design of new types of functional molecules and nanoparticles in the broad area that includes applied chemistry, drug delivery systems, and catalysts.

Very small particles are able to show astonishing properties. For example, gold atoms can be combined like strings of pearls, while nanoparticles can form one-, two- and three-dimensional layers. These assemblies can be used, for instance, as semiconductors, but other electronic as well as optical properties are possible.
An introduction to the booming field of "nanoworld" or "nanoscience," from fundamental principles to their use in novel applications.
With its clear structure and comprehensive coverage, backed by numerous examples from recent literature, this is a prime reference for chemists and materials scientists working with and developing nanoparticle systems.
A bestselling title in its second edition. A must-have reference for chemists and materials scientists.

This book draws on the main themes covered during the International Workshop on Molecular Architectonics which took place in Shiretoko, Japan from August 3 to 6, 2015. The concepts and results explored in this book relate to the term "molecular architectonics" which stands for electronic, optical and information-processing functions being orchestrated by molecular assemblies. This area is defined as the third stage of single-molecule electronics and builds on stage one, where measurements were performed on single-molecule layered films, and stage two, the resulting quantitative analyses. In this work, experts come together to write about the most important aspects of molecular architectonics. This interdisciplinary, visionary and unique book is of interest to scientists working on electronic materials, surface science and information processing sciences using noise and fluctuation.

Volume 1 of the Handbook of Colloid and Interface Science is a survey of the theory of colloids in a variety of fields, as well as theircharacterization by rheology. It is an ideal reference work for research scientists, universities, and industry practitioners looking for a complete understanding of how colloids and interfaces behave.

This book presents a unique collection of up-to-date applications of graphene for water science. Because water is an invaluable resource and the intelligent use and maintenance of water supplies is one of the most important and crucial challenges that stand before mankind, new technologies are constantly being sought to lower the cost and footprint of processes that make use of water resources as potable water as well as water for agriculture and industry, which are always in desperate demand. Much research is focused on graphene for different water treatment uses. Graphene, whose discovery won the 2010 Nobel Prize in physics, has been a shining star in the material science in the past few years. Owing to its interesting electrical, optical, mechanical and chemical properties, graphene has found potential applications in a wide range of areas, including water purification technology. A new type of graphene-based filter could be the key to managing the global water crisis. According to the World Economic Forum's Global Risks Report, lack of access to safe, clean water is the biggest risk to society over the coming decade. Yet some of these risks could be mitigated by the development of this filter, which is so strong and stable that it can be used for extended periods in the harshest corrosive environments, and with less maintenance than other filters on the market. The graphene-based filter could be used to filter chemicals, viruses, or bacteria from a range of liquids. It could be used to purify water, dairy products or wine, or in the production of pharmaceuticals. This book provides practical information to all those who are involved in this field.

This book is an amalgamation of knowledge, experience, and expertise in various aspects of nanotechnology, by experts who are proficient in designing of novel nanoformulations that are used in the treatment of various challenging and prevalent diseases. It is an exhaustive compilation of the multi-faceted arena of nanoformulations and the healthcare system that caters to the needs of academicians, scholars, researchers etc. The most important aspect of the book covers various types of nanoformulations and their applications in treatment of communicable and non-communicable diseases. Each chapter focuses on a particular nanoformulation as well as a disease including the pathophysiology of the disease, the current treatment modalities of diseases, the role of nanoformulation in treatment and other future aspects and directions for further work. Coverage includes neuropathic pain, colon targeting, nose-to-brain drug delivery, skin cancer, arthritis and tuberculosis.

This book presents some of the latest achievements in nanotechnology and nanomaterials from leading researchers in Ukraine, Europe, and beyond. It features selected peer-reviewed contributions from participants in the 5th International Science and Practice Conference Nanotechnology and Nanomaterials (NANO2017) held in Chernivtsi, Ukraine on August 23-26, 2017. The International Conference was organized jointly by the Institute of Physics of the National Academy of Sciences of Ukraine, Ivan Franko National University of Lviv (Ukraine), University of Tartu (Estonia), University of Turin (Italy), and Pierre and Marie Curie University (France). Internationally recognized experts from a wide range of universities and research institutions share their knowledge and key results on topics ranging from nanooptics and nanoplasmonics to interface studies. This book's companion volume also addresses topics such as energy storage and biomedical applications.

This book provides an overview of polyolefine production, including several recent breakthrough innovations in the fields of catalysis, process technology, and materials design. The industrial development of polymers is an extraordinary example of multidisciplinary cooperation, involving experts from different fields. An understanding of structure-property and processing relationships leads to the design of materials with innovative performance profiles. A comprehensive description of the connection between innovative material performance and multimodal polymer design, which incorporates both flexibility and constraints of multimodal processes and catalyst needs, is provided. This book provides a summary of the polymerization process, from the atomistic level to the macroscale, process components, including catalysts, and their influence on final polymer performance. This reference merges academic research and industrial knowledge to fill the gaps between academic research and industrial processes. * Connects innovative material performance to the flexibility of multimodal polymer design processes; * Provides a comprehensive description of the polymerization process from the atomic level to the macroscale; * Presents a polyhedric view of multimodal polymer production, including structure, property, and processing relationships, and the development of new materials.

This book discusses the latest developments of the synthesis, preparation, characterization, and applications of nano/microstructure-based materials in biomedical and energetic fields. It introduces several popular approaches to fabricating these materials, including template-assisted fabrication, electrospinning of organic/inorganic hybrid materials, biomineralization-mediated self-assembly, etc. The latest results in material evaluation for targeted applications are also presented. In particular, the book highlights the latest advances and future challenges in polymer nanodielectrics for energy storage applications. As such, it offers a valuable reference guide for scholars interested in the synthesis and evaluation of nano/microstructure-based materials, as well as their biomedical and energetic applications. It also provides essential insights for graduate students and scientists pursuing research in the broad fields of composite materials, polymers, organic/inorganic hybrid materials, nano-assembly, etc.

This thesis reports on essential experimental work in the field of novel two-dimensional (2D) atomic crystals beyond graphene. It especially describes three new 2D crystal materials, namely germanene, hafnene, and monolayer PtSe2 fabricated experimentally for the first time, using an ultra-high vacuum molecular beam epitaxy (UHV-MBE) system. Multiple characterization techniques, including scanning tunneling microscope (STM), low energy electron diffraction (LEED), scanning transmission electron microscope (STEM), and angle-resolved photoemission spectroscopy (ARPES), combined with theoretical studies reveal the materials' atomic and electronic structures, which allows the author to further investigate their physical properties and potential applications. In addition, a new epitaxial growth method for transition metal dichalcogenides involving direct selenization of metal supports is developed. These studies represent a significant step forward in expanding the family of 2D crystal materials and exploring their application potentials in future nanotechnology and related areas.

This book presents the select proceedings of the International Conference on Functional Material, Manufacturing and Performances (ICFMMP) 2019. The book provides the state-of-the-art research, development, and commercial prospective of recent advances in materials science and engineering. The contents cover various synthesis and fabrication routes of functional and smart materials for applications in mechanical engineering, manufacturing, metrology, nanotechnology, physics, chemical and biological sciences, civil engineering, food science among others. It also provides the evolutionary behavior of materials science for industrial applications. This book will be a useful resource for researchers as well as professionals interested in the highly interdisciplinary field of materials science.

Introducing the fields of nanomaterials and devices, and their applications across a wide range of academic disciplines and industry sectors, Donglu Shi takes an approach that provides a bridge between the knowledge acquisition and practical work, providing a starting point for the research and development of applications.

The major areas covered in this book are: - The characterization of nanomaterials, their preparation methods and performance testing techniques - The design and development of nano-scale devices - The applications of nanomaterials, with examples taken from different industry sectors, such as lighting, energy, bioengineering and medicine / medical devices. Key nanomaterial types are covered, such as carbon nanotubes, nanobiomaterials, nano-magnetic materials, semiconductor materials and nanocomposites. Shi also provides detailed coverage of key emerging technologies such as DNA nanotechnology and spintronics. This resulting text is equally relevant for advanced students (senior and graduate) and for engineers and scientists from a variety of different academic backgrounds working in the multi-disciplinary field of nanotechnology.

Provides detailed guidance for the characterization of nanomaterials, their preparation, and performance testing. Explains the principles and challenges of the design and development of nano-scale devices Explores applications through cases taken from a range of different sectors, including electronics, energy and medicine.

This second edition provides new and updated methods that detail new DNA nanotechnology techniques. Chapters focus on DNA origami nanostructures for arranging matter in the nanoscale or on their manipulation with the aid of other technologies, on procedures for making nucleic acids nanostructures of different kinds, and methods to simulate complex nanostructures or to use them in biosensing. Written in the highly successful Methods in Molecular Biology series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and tips on troubleshooting and avoiding known pitfalls. Authoritative and cutting-edge, DNA Nanotechnology: Methods and Protocols, Second Edition aims to ensure successful results in the further study of this vital field.

Processing of polymer nanocomposites usually requires special attention since the resultant structure-micro- and nano-level, is directly influenced by among other factors, polymer/nano-additive chemistry and the processing strategy. This book consolidates knowledge, from fundamental to product development, on polymer nanocomposites processing with special emphasis on the processing-structure-property-performance relationships in a wide range of polymer nanocomposites. Furthermore, this book focuses on emerging processing technologies such as electrospinning, which has very exciting applications ranging from medical to filtration. Additionally, the important role played by the nanoparticles in polymer blends structures has been illustrated in the current book, with special focus on fundamental aspects and properties of nanoparticles migration and interface crossing in immiscible polymer blend nanocomposites. This book introduces readers to nanomaterials and polymer nanocomposites processing. After defining nanoparticles and polymer nanocomposites and discussing environmental aspects, the second chapter focuses on the synthesis and functionalization of nanomaterials with applications in polymers. A brief overview on nanoclay and nanoclay-containing polymer nanocomposites is provided in third chapter. The fourth chapter provides an overview of the polymer nanocomposites structural elucidation techniques, such as X-ray diffraction and scattering, microscopy and spectroscopy, rheology. The fifth chapter is dedicated to the polymer nanocomposites processing technologies, among which electrospinning, which has very exciting applications ranging from medical to filtration. The last chapter provides an overview on how melt-processing strategy impact structure and mechanical properties of polymer nanocomposites by taking polypropylene-clay nanocomposite as a model system. The book is useful to undergraduate and postgraduate students (polymer engineering, materials science & engineering, chemical & process engineering), as well as research & development personnel, engineers, and material scientists.