This book is intended for researchers who are interested in investigating the nanomechanical properties of materials using advanced instrumentation techniques. The chapters of the book are written in an easy-to-follow format, just like solved examples. The book comprehensively covers a broad range of materials such as polymers, ceramics, hybrids, biomaterials, metal oxides, nanoparticles, minerals, carbon nanotubes and welded joints. Each chapter describes the application of techniques on the selected material and also mentions the methodology adopted for the extraction of information from the raw data.
This is a unique book in which both equipment manufacturers and equipment users have contributed chapters. Novices will learn the techniques directly from the inventors and senior researchers will gain in-depth information on the new technologies that are suitable for advanced analysis. On the one hand, fundamental concepts that are needed to understand the nanomechanical behavior of materials is included in the introductory part of the book. On the other hand, dedicated chapters describe the utilization of advanced numerical modeling in understanding the properties of complex materials.
This book is useful for students and researchers from diverse backgrounds including chemistry, physics, materials science & engineering, biotechnology and biomedical engineering.It is well suited as a textbook for students andas a reference book for researchers."

At present, the marketplace for professionals, researchers, and graduate students in solid-state physics and materials science lacks a book that presents a comprehensive discussion of ferroelectrics and related materials in a form that is suitable for experimentalists and engineers. This book proposes to present a wide coverage of domain-related issues concerning these materials. This coverage includes selected theoretical topics (which are covered in the existing literature) in addition to a plethora of experimental data which occupies over half of the book.

The book presents experimental findings and theoretical understanding of ferroic (non-magnetic) domains developed during the past 60 years. It addresses the situation by looking specifically at bulk crystals and thin films, with a particular focus on recently-developed microelectronic applications and methods for observations of domains with techniques such as scanning force microscopy, polarized light microscopy, scanning optical microscopy, electron microscopy, and surface decorating techniques.

"Domains in Ferroic Crystals and Thin Films" covers a large area of material properties and effects connected with static and dynamic properties of domains, which are extremely relevant to materials referred to as ferroics. In other textbooks on solid state physics, one large group of ferroics is customarily covered: those in which magnetic properties play a dominant role. Numerous books are specifically devoted to magnetic ferroics and cover a wide spectrum of magnetic domain phenomena. In contrast, "Domains in Ferroic Crystals and Thin Films" concentrates on domain-related phenomena in nonmagnetic ferroics. These materials are still inadequately represented in solid state physics textbooks and monographs.

This book presents a collection of papers presented at the 3rd World Congress on Integrated Computational Materials Engineering (ICME), a specialty conference organized by The Minerals, Metals & Materials Society (TMS). This meeting convened ICME stakeholders to examine topics relevant to the global advancement of ICME as an engineering discipline. The papers presented in these proceedings are divided into six sections: (1) ICME Applications; (2) ICME Building Blocks; (3) ICME Success Stories and Applications (4) Integration of ICME Building Blocks: Multi-scale Modeling; (5) Modeling, Data and Infrastructure Tools, and (6) Process Optimization. . These papers are intended to further the global implementation of ICME, broaden the variety of applications to which ICME is applied, and ultimately help industry design and produce new materials more efficiently and effectively.

Applications of EPR in Radiation Research is a multi-author contributed volume presented in eight themes: I. Elementary radiation processes (in situ and low temperature radiolysis, quantum solids); II: Solid state radiation chemistry (crystalline, amorphous and heterogeneous systems); III: Biochemistry, biophysics and biology applications (radicals in biomaterials, spin trapping, free-radical-induced DNA damage); IV: Materials science (polymeric and electronic materials, materials for treatment of nuclear waste, irradiated food); V: Radiation metrology (EPR-dosimetry, retrospective and medical applications); VI: Geological dating; VII: Advanced techniques (PELDOR, ESE and ENDOR spectroscopy, matrix isolation); VIII: Theoretical tools (density-functional calculations, spectrum simulations).

This book highlights the latest advances in AFM nano-manipulation research in the field of nanotechnology. There are numerous uncertainties in the AFM nano-manipulation environment, such as thermal drift, tip broadening effect, tip positioning errors and manipulation instability. This book proposes a method for estimating tip morphology using a blind modeling algorithm, which is the basis of the analysis of the influence of thermal drift on AFM scanning images, and also explains how the scanning image of AFM is reconstructed with better accuracy. Further, the book describes how the tip positioning errors caused by thermal drift and system nonlinearity can be corrected using the proposed landmark observation method, and also explores the tip path planning method in a complex environment. Lastly, it presents an AFM-based nano-manipulation platform to illustrate the effectiveness of the proposed method using theoretical research, such as tip positioning and virtual nano-hand.

This book collects several contributions presented at the 2019 meeting of the Italian Synchrotron Radiation Society (SILS), held in Camerino, Italy, from 9 to 11 September 2019. Topics included are recent developments in synchrotron radiation facilities and instrumentation, novel methods for data analysis, applications in the fields of materials physics and chemistry, Earth and environmental science, coherence in x-ray experiments. The book is intended for advanced students and researchers interested in synchrotron-based techniques and their application in diverse fields.

This book reviews the recent development of fabrication methods and various properties of lotus-type porous metals and their applications. The nucleation and growth mechanism of the directional pores in metals are discussed in comparison with a model experiment of carbon dioxide pores in ice. Three casting techniques are introduced to produce not only metals and alloys but also intermetallic compounds, semiconductors, and ceramics: mold casting, continuous zone melting, and continuous casting. The latter has merits for mass production of lotus metals to control porosity, pore size and pore direction. Furthermore, anisotropic behavior of elastic, mechanical properties, thermal and electrical conductivity, magnetic properties, and biocompatibility are introduced as peculiar features of lotus metals.

This thesis describes the development of a new technique to solve an important industrial inspection requirement for a high-value jet-engine component. The work - and the story told in the thesis - stretches all the way from the fundamentals of wave propagation in anisotropic material and ultrasonic array imaging through to device production and site trials. The book includes a description of a new method to determine crystallographic orientation from 2D ultrasonic array data. Another new method is described that enables volumetric images of an anisotropic material to be generated from 2D ultrasonic array data, based on measured crystallographic orientation. After extensive modeling, a suitable 2D array and deployment fixtures were manufactured and tested on in situ turbine blades in real engines. The final site trial indicated an order of magnitude improvement over the best existing technique in the detectability of a certain type of root cracking. The Development of a 2D Ultrasonic Array Inspection for Single Crystal Turbine Blades should be an inspiration for those starting out on doctoral degrees as it shows the complete development cycle from basic science to industrial usage.

A discussion of developments in the measurement and interpretation of advanced laboratory stress-strain testing of geomaterials. It includes a collection of case studies which apply the test results and is based on the activities of the technical committee No 29 of the ISSMGE.

This volume of Modern Aspects contains seven chapters. The major topics covered in the first six chapters of this volume include fundamentals of solid state electrochemistry; kinetics of electrochemical hydrogen entry into metals and alloys; oxidation of organics; fuel cells; electrode kinetics of trace-anion catalysis; nano structural analysis. The last chapter is a corrected version of chapter four from Volume 35. Faisal M. AI-faqeer and Howard W. Pickering begin the first chapter by going back to 1864 and Cailletet who found that some hydrogen evolved and was absorbed by iron when it was immersed in dilute sulfuric acid. The absorption of hydrogen into metals and alloys can lead to catastrophic failures of structures. They discuss the kinetics of electrochemical hydrogen entry into metals and alloys. In chapter three, Clyde L. Briant reviews the electrochemistry, corrosion and hydrogen embrittlement of unalloyed titanium. He begins by reviewing the basic electrochemistry and general corrosion of titanium. He also discusses pitting and galvanostatic corrosion followed by a review of hydrogen embrittlement emphasizing the formation of hydrides and the effect of these on titanium's mechanical properties. Christos Comninellis and Gy6rgy F6ti discuss the oxidative electrochemical processes of organics in chapter three. They begin by defining direct and indirect electrochemical oxidation of organics. They introduce a model that allows them to distinguish between active (strong) and non-active (weak) anodes. Different classes of organic compounds are used for kinetic models of organic oxidation at active and non-active type anodes.

Fiber sensing technologies have enabled both fundamental studies and a wide spectrum of applications in every aspect of life. This book highlights the recent advancement in fiber sensing technologies based on newly developed sensing mechanisms, advanced fiber structures, and functional materials. In particular, the integration of functional materials with different electrical, optical, thermal, or mechanical properties into a single fiber offers a wealth of new opportunities in sensing. The book covers the major developments in novel fiber materials, such as semiconductors, metals, polymers, soft glasses, and carbon materials, as well as the sensing applications based on both single fiber and multi-dimensional fiber arrays for temperature, light, strain, vibration, electric and magnetic fields, hazardous chemicals, gases, and physiological signals.

"Evaluating Measurement Accuracy, 2nd Edition" is intended for those who are concerned with measurements in any field of science or technology. It reflects the latest developments in metrology and offers new results, but is designed to be accessible to readers at different levels: scientists who advance the field of metrology, engineers and experimental scientists who use measurements as tool in their professions, students and graduate students in natural sciences and engineering, and, in parts describing practical recommendations, technicians performing mass measurements in industry, quality control, and trade. This book presents material from the practical perspective and offers solutions and recommendations for problems that arise in conducting real-life measurements. This new edition adds a method for estimating accuracy of indirect measurements with independent arguments, whose development Dr. Rabinovich was able to complete very recently. This method, which is called the Method of Enumeration, produces estimates that are no longer approximate, similar to the way the method of reduction described in the first edition removed approximation in estimating uncertainty of indirect measurements with dependent arguments. The method of enumeration completes addressing the range of problems whose solutions signify the emergence of the new theory of accuracy of measurements. A new method is added for building a composition of histograms, and this method forms a theoretical basis for the method of enumeration.Additionally, as a companion to this book, a concise practical guide that assembles simple step-by-step procedures for typical tasks the practitioners are likely to encounter in measurement accuracy estimation is available at SpringerLink.

This book presents selected contributions to the Symposium of Aeronautical and Aerospace Processes, Materials and Industrial Applications of the XXV International Materials Research Congress (IMRC). Each chapter addresses scientific principles behind processing and production of materials for aerospace/aeronautical applications. The chapter deals with microstructural characterization including composites materials and metals. The second chapter deals with corrosion in aerospace components is a large and expensive problema for aerospace industry. Finally, the last chapter covers modeling and simulation of different processes to evaluate and optimize the forming process. This book is meant to be useful to academics and professionals.

By illustrating a wide range of specific applications in all major industries, this work broadens the coverage of X-ray diffraction beyond basic tenets, research and academic principles. The book serves as a guide to solving problems faced everyday in the laboratory, and offers a review of the current theory and practice of X-ray diffraction, major advances and potential uses.

This collection on "Mechanics of Generalized Continua - from Micromechanical Basics to Engineering Applications" brings together leading scientists in this field from France, Russian Federation, and Germany. The attention in this publication is be focussed on the most recent research items, i.e., - new models, - application of well-known models to new problems, - micro-macro aspects, - computational effort, - possibilities to identify the constitutive equations, and - old problems with incorrect or non-satisfying solutions based on the classical continua assumptions.

Synchrotron radiation is today extensively used for fundamental and applied research in many different fields of science. Its exceptional characteristics in terms of intensity, brilliance, spectral range, time structure and now also coherence pushed many experimental techniques to previously un-reachable limits, enabling the performance of experiments unbelievable only few years ago.

The book gives an up-to-date overview of synchrotron radiation research today with a view to the future, starting from its generation and sources, its interaction with matter, illustrating the main experimental technique employed and provides an overview of the main fields of research in which new and innovative results are obtained.

The book is addressed to PhD students and young researchers to provide both an introductory and a rather deep knowledge of the field. It will also be helpful to experienced researcher who want to approach the field in a professional way.

This book describes in 2 parts experimental data with simple explanations (Part I) and itinerant electron theories (Part II) about magnetism and its related properties of 3d-intermetallic compounds. Unlike 3d-metal alloys and oxides, theoretical as well as experimental studies on 3d-intermetallic compounds such as 3d-pnictides and chalcogenides, on which we focus in this book, seem unfortunately delayed. The objective of this book is to motivate active studies in this ?eld in the future. We discuss in detail magnetic and related properties of the 3d-transition-metal pnictides and chalcogenides, which include the intermetallic compounds expressed as MX and M X, and their mixed compoundsM M X, MX X and M M X, 2 1?x x 1?y 2?x y x where M (M)isa3d element and X (X ) a pnicogen (P, As, Sb, and Bi) or a chalcogen (S, Se, and Te). Most of the MX-type compounds crystallize either in the hexagonalNiAs-type structure or in the orthorhombicMnP-type structure which is regarded as a distorted NiAs-type structure. Crystallographic phase transition b- ween the NiAs- and the MnP-typesoccursin some of MX-typecompoundswhen the temperaturechanges. The M X-type compoundscrystallize in the tetragonalCu Sb- 2 2 typestructure.Asdescribedin detailinthisbook,manyofthecompoundsmentioned aboveexhibitveryinterestingmagneticandcrystallographicphasetransitionscaused by various means such as change of temperature, applications of external magnetic ?eld or pressure, and change of the composition x in the case of mixed compounds.

The objective of this book is to discuss the current status of research and development of boron-rich solids as sensors, ultra-high temperature ceramics, thermoelectrics, and armor. Novel biological and chemical sensors made of stiff and light-weight boron-rich solids are very exciting and efficient for applications in medical diagnoses, environmental surveillance and the detection of pathogen and biological/chemical terrorism agents. Ultra-high temperature ceramic composites exhibit excellent oxidation and corrosion resistance for hypersonic vehicle applications. Boron-rich solids are also promising candidates for high-temperature thermoelectric conversion. Armor is another very important application of boron-rich solids, since most of them exhibit very high hardness, which makes them perfect candidates with high resistance to ballistic impact. The following topical areas are presented: *Boron-rich solids: science and technology *Synthesis and sintering strategies of boron rich solids *Microcantilever sensors *Screening of the possible boron-based thermoelectric conversion materials; *Ultra-high temperature ZrB2 and HfB2 based composites *Magnetic, transport and high-pressure properties of boron-rich solids *Restrictions of the sensor dimensions for chemical detection *Armor

This volume comprises the proceedings of the Third International Conference on Calcined Clays for Sustainable Concrete held in New Delhi, India in October 2019. The papers cover topics related to geology of clay, hydration and performance of blended systems with calcined clays, alkali activated binders, and economic and environmental impacts of the use of calcined clays in cement-based materials. The book presents research on influence of processing on reactivity of calcined clays, influence of clay mineralogy on reactivity, geology of clay deposits, and the environmental impact of use of calcined clays in cement and concrete and field applications of calcined clay in concrete. Apart from giving an overview of the progress of research during the last two years, this work also covers the state-of-the art on the practical aspects of production and use of calcined clays in construction. The contents of this volume will prove useful to researchers and graduate students working in the areas of cement chemistry, cement production, and concrete design.

From reviews of previous volumes: 'This volume continues the valuable service that has been rendered by the Modern Aspects series.'-Journal of Electroanalytical Chemistry 'Extremely well referenced and very readable....Maintains the overall high standards of the series.'-Journal of the American Chemical Society

The main objective of this book is to cover the basic understanding of thermal conduction mechanisms in various high thermal conductivity materials including diamond, cubic boron nitride, and also the latest material like carbon nanotubes.

The book is intended as a good reference book for scientists and engineers involved in addressing thermal management issues in a broad spectrum of industries.

Leading researchers from industry and academic institutions who are well known in their areas of expertise have contributed a chapter in the field of their interest.

The clamor for non-carbon dioxide emitting energy production has directly impacted on the development of nuclear energy. As new nuclear plants are built, plans and designs are continually being developed to manage the range of challenging requirement and problems that nuclear plants face especially when managing the greatly increased operating temperatures, irradiation doses and extended design life spans. Materials for Nuclear Plants: From Safe Design to Residual Life Assessments provides a comprehensive treatment of the structural materials for nuclear power plants with emphasis on advanced design concepts. Materials for Nuclear Plants: From Safe Design to Residual Life Assessments approaches structural materials with a systemic approach. Important components and materials currently in use as well as those which can be considered in future designs are detailed, whilst the damage mechanisms responsible for plant ageing are discussed and explained. Methodologies for materials characterization, materials modeling and advanced materials testing will be described including design code considerations and non-destructive evaluation concepts. Including models for simple system dynamic problems and knowledge of current nuclear power plants in operation, Materials for Nuclear Plants: From Safe Design to Residual Life Assessments is ideal for students studying postgraduate courses in Nuclear Engineering. Designers on courses for code development, such as ASME or ISO and nuclear authorities will also find this a useful reference.

This text on numerical methods applied to the analysis of electromagnetic nondestructive testing (NOT) phenomena is the first in a series devoted to all aspects of engineering nondestructive evaluation. The timing of this series is most appropriate as many university engineering/physics faculties around the world, recognizing the industrial significance of the subject, are organizing new courses and programs with engineering NOE as a theme. Additional texts in the series will cover electromagnetics for engineering NOE, microwave NOT methods, ultrasonic testing, radiographic methods and signal processing for NOE. It is the intended purpose of the series to provide senior-graduate level coverage of the material suitable for university curricula and to be generally useful to those in industry with engineering degrees who wish to upgrade their NOE skills beyond those needed for certification. This dual purpose for the series reflects the very applied nature of NOE and the need to develop suitable texts capable of bridging the gap between research laboratory studies of NOE phenomena and the real world of certification and industrial applications. The reader might be tempted to question these assertions in light of the rather mathematical nature of this first text. However, the subject of numerical modeling is of critical importance to a thorough understanding of the field-defect interactions at the heart of all electromagnetic NOT phenomena.

This book embraces all physiochemical aspects of the structure and molecular dynamics of water, focusing on its role in biological objects, e.g. living cells and tissue, and in the formation of functionally active structures of biological molecules and their ensembles. Water is the single most abundant chemical found in all living things. It offers a detailed look into the latest modern physical methods for studying the molecular structure and dynamics of the water and provides a critical analysis of the existing literature data on the properties of water in biological objects. Water as a chemical reagent and as a medium for the formation of conditions for enzymatic catalysis is a core focus of this book. Although well suited for active researchers, the book as a whole, as well as each chapter on its own, can be used as fundamental reference material for graduate and undergraduate students throughout chemistry, physics, biophysics and biomedicine.

A state-of-the-art report prepared by RILEM Technical Committee 116-PCD. At present, durability of concrete is controlled by specifying the materials to be used, the methods of mixing, placing, curing and so on. This approach is often unsatisfactory and it is a common objective of concrete researchers and engineers to develop performance criteria which allow the potential durability of a particular concrete mix or structure to be estimated. However, the complexity of concrete as a material and the difficulty of developing consistent and reliable test methods has meant that progress has been slow. International interest in the subject is growing strongly with the development of international standards and so this book is very timely in giving an authoritative, international review of the subject. It will set the scene for the next few years as a key source of information and advice.