Nanoscale structures and materials have been explored in many biological applications because of their novel and impressive physical and chemical properties. Such properties allow remarkable opportunities to study and interact with complex biological processes. This book analyses the state of the art of piezoelectric nanomaterials and introduces their applications in the biomedical field. Despite their impressive potentials, piezoelectric materials have not yet received significant attention for bio-applications. This book shows that the exploitation of piezoelectric nanoparticles in nanomedicine is possible and realistic, and their impressive physical properties can be useful for several applications, ranging from sensors and transducers for the detection of biomolecules to sensible substrates for tissue engineering or cell stimulation. The book also focuses on the preparation, characterization and bio-applications of piezoelectric nanoparticles.

This book focuses on structural characterisation techniques for porous materials. Covering a range of techniques, including gas sorption, mercury porosimetry, thermoporometry, NMR and imaging methods, this practical guide presents the basic theory behind each characterisation technique, and discusses the practicalities of the experimental and data analysis approaches needed for complex industrial samples. The book shows readers how to approach characterising a particular sort of material for the first time and then how to develop a strategy for more in-depth analysis. It also demonstrates how to determine the best techniques for solving particular problems, and describes methods of obtaining the required information, as well as the limitations of various methods. It particularly highlights a scientific approach involving parameter validation and simple acquisition. Featuring examples taken from case studies of real-world industrial materials, this book is intended for industrial practitioners and researchers. It provides a manual of potential techniques and answers questions concerning porous materials that arise in areas such as the catalyst industry, the oil and gas sector, batteries, fuel cells, tissue engineering scaffolds and drug delivery devices.

There is a growing need in both industrial and academic research to obtain accurate quantitative results from continuous wave (CW) electron paramagnetic resonance (EPR) experiments. This book describes various sample-related, instrument-related and software-related aspects of obtaining quantitative results from EPR expe- ments. Some speci?c items to be discussed include: selection of a reference standard, resonator considerations (Q, B, B ), power saturation, sample position- 1 m ing, and ?nally, the blending of all the factors together to provide a calculation model for obtaining an accurate spin concentration of a sample. This book might, at ?rst glance, appear to be a step back from some of the more advanced pulsed methods discussed in recent EPR texts, but actually quantitative "routine CW EPR" is a challenging technique, and requires a thorough understa- ing of the spectrometer and the spin system. Quantitation of CW EPR can be subdivided into two main categories: (1) intensity and (2) magnetic ?eld/mic- wave frequency measurement. Intensity is important for spin counting. Both re- tive intensity quantitation of EPR samples and their absolute spin concentration of samples are often of interest. This information is important for kinetics, mechanism elucidation, and commercial applications where EPR serves as a detection system for free radicals produced in an industrial process. It is also important for the study of magnetic properties. Magnetic ?eld/microwave frequency is important for g and nuclear hyper?ne coupling measurements that re?ect the electronic structure of the radicals or metal ions.

This book is a collection of experimental studies demonstrating structure-function relationships in various biological systems having particular surface specialization to increase/decrease friction and adhesion. Studies on snake skin, adhesive pads, wing-interlocking devices and sticky mouthparts of insects as well as anti-adhesive and adhesive surfaces of plants are included in the volume containing four main subsections: (1) adhesion, (2) friction, (3) attachment-devices, (4) attachment-related behavior. Numerous experimental methods for characterizing tribological properties of biological surfaces at macro-, micro-, and nanoscale levels are demonstrated. This book is an excellent collection of publications on biotribology for both engineers and physicists working with biological systems as well as for biologists studying friction and adhesion. Inspirations from biology reported here may be also potentially interesting for biomimetics.

Industrial radiography is a well-established non-destructive testing (NDT) method in which the basic principles were established many years ago. However, during 1993-95 the European Standards Organisa tion (CEN) commenced drafting many new standards on NDT including radiographic methods, and when completed these will replace national standards in all the EC member countries. In some cases these standards vary significantly from those in use in the UK at present. These CEN standards are accepted by majority, not unanimous voting, so they will become mandatory even in countries which vote against them. As most are likely to be legal by the time this second edition is published, they are described in the appropriate places in the text. The most important new technical development is the greater use of computers in radiology. In the first edition, computerized tomography was only briefly mentioned at the end of Chapter 11, as it was then largely a medical method with only a few equipments having found a place in industrial use. The method depends on a complex computer program and a large data store. Industrial equipments are now being built, although their spread into industry has been slow. Computer data storage is also being used for radiographic data. Small computers can now store all the data produced by scanning a radiographic film with a small light-spot, and various programs can be applied to these data."

In five chapters, this volume presents recent developments in fatigue assessment. In the first chapter, a generalized Neuber concept of fictitious notch rounding is presented where the microstructural support factors depend on the notch opening angle besides the loading mode. The second chapter specifies the notch stress factor including the strain energy density and J-integral concept while the SED approach is applied to common fillet welded joints and to thin-sheet lap welded joints in the third chapter. The forth chapter analyses elastic-plastic deformations in the near crack tip zone and discusses driving force parameters. The last chapter discusses thermomechanical fatigue, stress, and strain ranges.

This book discusses the latest developments in narrow fabrics from research institutions, machinery building companies and producers of such products, presented during the International Week of Narrow Fabrics in March 2016 in Moenchengladbach, Germany. It also demonstrates different applications of braided and woven fabrics. Braided and woven narrow products are produced using completely different techniques, but have a lot of similarities in their applications - they are used as belts, ropes and tubes in areas ranging from medical textiles, cables, technical and home applications to large-scale transport belts and long tubes for transporting oil from the bottom of the ocean.

This book provides comprehensive coverage of all aspects of physical testing of elastomers (rubbers and thermoplastic elastomers) including mechanical, electrical, thermal and all aspects of durability. Elastomers are an important class of materials used in such products as tyres, seals and hose which have markedly different properties to other materials. The importance of testing of elastomers means that a comprehensive text on the subject is essential. The advantage over general materials testing books is being more specific while the advantage over general rubber technology books is that testing is dealt with in depth.

The subject of mechanical behavior has been in the front line of basic studies in engineering curricula for many years. This textbook was written for engineering students with the aim of presenting, in a relatively simple manner, the basic concepts of mechanical behavior in solid materials. A second aim of the book is to guide students in their laboratory experiments by helping them to understand their observations in parallel with the lectures of their various courses; therefore the first chapter of the book is devoted to mechanical testing. Another aim of the book is to provide practicing engineers with basic help to bridge the gap of time that has passed from their graduation up to their actual involvement in engineering work. The book also serves as the basis for more advanced studies and seminars when pursuing courses on a graduate level. The content of this textbook and the topics discussed correspond to courses that are usually taught in universities and colleges all over the world, but with a different and more modern approach. It is however unique by the inclusion of an extensive chapter on mechanical behavior in the micron and submicron/nanometer range. Mechanical deformation phenomena are explained and often related to the presence of dislocations in structures. Many practical illustrations are provided representing various observations encountered in actual structures of particularly technical significance. A comprehensive list of references at the end of each chapter is included to provide a broad basis for further studying the subject.

This thesis presents the first direct observations of the 3D-shape, size and electrical properties of nanoscale filaments, made possible by a new Scanning Probe Microscopy-based tomography technique referred to as scalpel SPM. Using this innovative technology and nm-scale observations, the author achieves essential insights into the filament formation mechanisms, improves the understanding required for device optimization, and experimentally observes phenomena that had previously been only theoretically proposed.

This book is a continuous learning tool for experienced technical staff facing laser vibrometry technology for the first time. The book covers both theoretical aspects and practical applications of laser Doppler vibrometry, and is accompanied by a multimedia presentation that allows the audience to browse the content and come as close as possible to performing real experiments. After a brief introduction, Chapter 2 presents supporting theory, providing general information on light sources, light scattering and interference for a better understanding of the rest of the book. Chapter 3 examines the theory of laser vibrometers, explaining interferometers from an optical perspective and in terms of the related electronics. It also addresses options like tracking filters and different signal demodulation strategies, since these have a significant impact on the practical use of vibrometers. Chapter 4 explores the configurations that are encountered in today's instrumentation, with a focus on providing practical suggestions on the use of laser vibrometers. Lastly, Chapter 5 investigates metrology for vibration and shock measurements using laser interferometry, and analyses the uncertainty of laser vibrometers in depth.

Advances in Polymer Science enjoys a longstanding tradition and good reputation in its community. Each volume is dedicated to a current topic, and each review critically surveys one aspect of that topic, to place it within the context of the volume. The volumes typically summarize the significant developments of the last 5 to 10 years and discuss them critically, presenting selected examples, explaining and illustrating the important principles, and bringing together many important references of primary literature. On that basis, future research directions in the area can be discussed. Advances in Polymer Science volumes thus are important references for every polymer scientist, as well as for other scientists interested in polymer science - as an introduction to a neighboring field, or as a compilation of detailed information for the specialist.

This volume covers various aspects of cross-linked polyethylene (XLPE). The contents include manufacture, morphology, structure, properties, applications, early stage development, cross-linking techniques, recycling process, physical and chemical properties as well as the scope and future aspects of XLPE. It focuses on the life cycle analysis of XLPE and their industrial applications and commercial importance. This book will be of use to academic and industry researchers, as well as graduate students working in the fields of polymer science and engineering, materials science, and chemical engineering.

This collection represents a cross-section of the papers presented at the 6th International Conference on Recrystallization and Grain Growth. The volume is divided into nine sections: * Grain growth theory and simulation * Recrystallization theory and simulation * Low carbon and IF steels * High strength steels * Electrical steels * Stainless steels * Aluminum and magnesium alloys * Nickel and nickel based superalloys * Unconventional and advanced materials

Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.

This book is about the pattern formation and the evolution of crack propagation in engineering materials and structures, bridging mathematical analyses of cracks based on singular integral equations, to computational simulation of engineering design. The first two parts of this book focus on elasticity and fracture and provide the basis for discussions on fracture morphology and its numerical simulation, which may lead to a simulation-based fracture control in engineering structures. Several design concepts are discussed for the prevention of fatigue and fracture in engineering structures, including safe-life design, fail-safe design, damage tolerant design.

After starting with basic elasticity and fracture theories in parts one and two, this book focuses on the fracture morphology that develops due to the propagation of brittle cracks or fatigue cracks.

In part three, the mathematical analysis of a curved crack is precisely described, based on the perturbation method. The stability theory of interactive cracks propagating in brittle solids may help readers to understand the formation of a fractal-like cracking patterns in brittle solids, while the stability theory of crack paths helps to identify the straight versus sharply curved or sometimes wavy crack paths observed in brittle solids.

In part four, the numerical simulation method of a system of multiple cracks is introduced by means of the finite element method, which may be used for the better implementation of fracture control in engineering structures.

This book is part of a series on Mathematics for Industry and will appeal to structural engineers seeking to understand the basic backgrounds of analyses, but also to mathematicians with an interest in how such mathematical solutions are evaluated in industrial applications."

Light scattering is a very powerful method to characterize the structure of polymers and nanoparticles in solution. Recent technical developments have strongly enhanced the possible applications of this technique, overcoming previous limitations like sample turbidity or insufficient experimental time scales. However, despite their importance, these new developments have not yet been presented in a comprehensive form. In addition, and maybe even more important to the broad audience, there lacks a simple-to-read textbook for students and non-experts interested in the basic principles and fundamental techniques of light scattering. As part of the Springer Laboratory series, this book tries not only to provide such a simple-to-read and illustrative textbook about the seemingly very complicated topic of light scattering from polymers and nanoparticles in dilute solution, but also intends to cover some of the newest technical developments in experimental light scattering.

This book presents a systematic and comprehensive exposition of the theory of measurement accuracy and provides solutions that fill significant and long-standing gaps in the classical theory. It eliminates the shortcomings of the classical theory by including methods for estimating accuracy of single measurements, the most common type of measurement. The book also develops methods of reduction and enumeration for indirect measurements, which do not require Taylor series and produce a precise solution to this problem. It produces grounded methods and recommendations for summation of errors. The monograph also analyzes and critiques two foundation metrological documents, the International Vocabulary of Metrology (VIM) and the Guide to the Expression of Uncertainty in Measurement (GUM), and discusses directions for their revision. This new edition adds a step-by-step guide on how to evaluate measurement accuracy and recommendations on how to calculate systematic error of multiple measurements. There is also an extended section on the method of reduction, which provides an alternative to the least-square method and the method of enumeration. Many sections are also rewritten to improve the structure and usability of the material. The 3rd edition reflects the latest developments in metrology and offers new results, and it is designed to be accessible to readers at various levels and positions, including scientists, engineers, and undergraduate and graduate students. By presenting material from a practical perspective and offering solutions and recommendations for problems that arise in conducting real-life measurements, author Semyon Rabinovich offers an invaluable resource for scientists in any field.

Computational Methods for Microstructure-Property Relationships introduces state-of-the-art advances in computational modeling approaches for materials structure-property relations. Written with an approach that recognizes the necessity of the engineering computational mechanics framework, this volume provides balanced treatment of heterogeneous materials structures within the microstructural and component scales. Encompassing both computational mechanics and computational materials science disciplines, this volume offers an analysis of the current techniques and selected topics important to industry researchers, such as deformation, creep and fatigue of primarily metallic materials.

Researchers, engineers and professionals involved with predicting performance and failure of materials will find Computational Methods for Microstructure-Property Relationships a valuable reference.

Dynamic Failure of Materials and Structures discusses the topic of dynamic loadings and their effect on material and structural failure. Since dynamic loading problems are very difficult as compared to their static counterpart, very little information is currently available about dynamic behavior of materials and structures. Topics covered include the response of both metallic as well as polymeric composite materials to blast loading and shock loadings, impact loadings and failure of novel materials under more controlled dynamic loads. These include response of soft materials that are important in practical use but have very limited information available on their dynamic response. Dynamic fragmentation, which has re-emerged in recent years has also been included. Both experimental as well as numerical aspects of material and structural response to dynamic loads are discussed.

Written by several key experts in the field, Dynamic Failure of Materials and Structures will appeal to graduate students and researchers studying dynamic loadings within mechanical and civil engineering, as well as in physics and materials science.

Number 25 of this acclaimed series breaks new ground with articles on charge transfer across liquid-liquid interfaces, electrochemical techniques to study hydrogen ingress in metals, and electrical breakdown of liquids. Also included are articles on the measurement of corrosion and ellipsometry, bringing these older subjects up to date.

Prometheus brought fire to mankind Arthur R. von Hippel "Dielectrics and Waves," 1954 Our contribution? There are only few areas of research and development of a comparable scientific and technological extension as microwave and high frequency processing. "Pr- essing" means not only application of radiation of 300 MHz to 300 GHz f- quency to synthesis, heating or ionisation of matter but also generation, transm- sion and detection of microwave and radio frequency radiation. Microwave and high frequency sources positioned in the orbit are the foun- tion of modern satellite telecommunication systems, gyrotron tubes being pr- ently developed in different countries all over the world will most probably be the major devices to open up a new era of energy supply to mankind be means of - sion plasma. Although initiated by military purposes during the Second World War (RADAR, Radio Detection and Ranging), microwave and high frequency utilisation has spread over almost every important aspect of normal day life since than, from individual mobile phones and kitchen microwave ovens to industrial food processing, production of composites as sustainable building materials, green chemistry, medical applications and finally infrastructure installations like GPS and Galileo, to name only few examples. These different areas of microwave and high frequency radiation application can not be unified within one group of scientists and technologists. There are s- eral distinguished communities active e.g., in the area of telecommunication s- tems, strong microwaves for fusion plasma or plasma based materials processing.

This outstanding thesis provides a wide-ranging overview of the growth of titanium dioxide thin films and its use in photo-electrochemicals such as water splitting. The context for water splitting is introduced with the theory of semiconductor-liquid junctions, which are dealt with in detail. In particular plasmonic enhancement of TiO2 by the addition of gold nanoparticles is considered in depth, including a thorough and critical review of the literature, which discusses the possible mechanisms that may be at work. Plasmonic enhancement is demonstrated with gold nanoparticles on Nb-doped TiO2. Finally, the use of temperature and pressure to control the phase and morphology of thin films grown by pulsed laser deposition is presented.

The research and its outcomes presented here is devoted to the use of x-ray scattering to study correlated electron systems and magnetism. Different x-ray based methods are provided to analyze three dimensional electron systems and the structure of transition-metal oxides. Finally the observation of multipole orderings with x-ray diffraction is shown.

- self-contained and well illustrated

- complete and comprehensive derivation of mechanical/mathematical results with enphasis on issues of practical importance

- combines classical subjects of fracture mechanics with modern topics such as microheterogeneous materials, piezoelectric materials, thin films, damage

- mechanically and mathematically clear and complete derivations of results