A new experimental method - the "Stiffnessometer", is developed to measure elementary properties of a superconductor, including the superconducting stiffness and the critical current. This technique has many advantages over existing methods, such as: the ability to measure these properties while minimally disturbing the system; the ability to measure large penetration depths (comparable to sample size), as necessary when approaching the critical temperature; and the ability to measure critical currents without attaching contacts and heating the sample. The power of this method is demonstrated in a study of the penetration depth of LSCO, where striking evidence is found for two separate critical temperatures for the in-plane and out-of-plane directions. The results in the thesis are novel, important and currently have no theoretical explanation. The stiffnessometer in a tool with great potential to explore new grounds in condensed matter physics.

This book highlights the acoustical metamaterials' capability to manipulate the direction of sound propagation in solids which in turn control the scattering, diffraction and refraction, the three basic mechanisms of sound propagation in solids. This gives rise to several novel theories and applications and hence the name new acoustics. As an introduction, the book mentions that symmetry of acoustic fields is the theoretical framework of acoustical metamaterials. This is then followed by describing that acoustical metamaterials began with locally resonant sonic materials which ushered in the concept of negative acoustic parameters such as mass density and bulk modulus. This complies with form invariance of the acoustic equation of motion which again exemplifies the symmetry property of acoustic fields.

In this thesis, the author investigates experimentally and numericallythe fracture behavior of an electron beam welded joint made fromtwo butt S355 plates. The 2D Rousselier model, the Gurson-Tvergaard-Needleman (GTN) model and the cohesive zone model (CZM) wereadopted to predict the crack propagation of thick compact tension (CT)specimens. Advantages and disadvantages of the three mentioned modelsare discussed. The cohesive zone model is suggested as it is easy to usefor scientists & engineers because the CZM has less model parametersand can be used to simulate arbitrary crack propagation. The resultsshown in this thesis help to evaluate the fracture behavior of a metallicmaterial. A 3D optical deformation measurement system (ARAMIS) andthe synchrotron radiation-computed laminography (SRCL) techniquereveal for the first time the damage evolution on the surface of the sampleand inside a thin sheet specimen obtained from steel S355. Damageevolution by void initiation, growth and coalescence are visualized in2D and 3D laminographic images. Two fracture types, i.e., a flat crackpropagation originated from void initiation, growth and coalescenceand a shear coalescence mechanism are visualized in 2D and 3D imagesof laminographic data, showing the complexity of real fracture. Inthe dissertation, the 3D Rousselier model is applied for the first timesuccessfully to predict different microcrack shapes before shear cracksarise by defining the finite elements in front of the initial notch withinhomogeneous f0-values. The influence of the distribution of inclusionson the fracture shape is also discussed. For the analyzed material, ahomogeneous distribution of particles in the material provides thehighest resistance to fracture.

This books presents a current look at friction stir welding technology from application to characterization and from modeling to R&D. It is a compilation of the recent progress relating to friction stir technologies including derivative technologies, high-temperature applications, industrial applications, dissimilar alloy/materials, lightweight alloys, simulation, and characterization. With contributions from leaders and experts in industry and academia, this will be a comprehensive source for the field of Friction Stir Welding and Processing.

The book presents a series of concise papers by researchers specialized in various fields of continuum and computational mechanics and of material science. The focus is on principles and strategies for multiscale modeling and simulation of complex heterogeneous materials, with periodic or random microstructure, subjected to various types of mechanical, thermal, chemical loadings and environmental effects. A wide overview of complex behavior of materials (plasticity, damage, fracture, growth, etc.) is provided. Among various approaches, attention is given to advanced non-classical continua modeling which, provided by constitutive characterization for the internal and external actions (in particular boundary conditions), is a very powerful frame for the gross mechanical description of complex material behaviors, able to circumvent the restrictions of classical coarse-graining multiscale approaches.

This collection gives broad and up-to-date results in the research and development of materials characterization and processing. Coverage is well-rounded from minerals, metals, and materials characterization and developments in extraction to the fabrication and performance of materials. In addition, topics as varied as structural steels to electronic materials to plant-based composites are explored. The latest research presented in this wide area make this book both timely and relevant to the materials science field as a whole. The book explores scientific processes to characterize materials using modern technologies, and focuses on the interrelationships and interdependence among processing, structure, properties, and performance of materials. Topics covered include ferrous materials, non-ferrous materials, minerals, ceramics, clays, soft materials, method development, processing, corrosion, welding, solidification, composites, extraction, powders, nanomaterials, advanced materials, and several others.

This book presents the relationships between tensile damage and fracture, fatigue hysteresis loops, stress-rupture, fatigue life and fatigue limit stress, and stochastic loading stress. Ceramic-matrix composites (CMCs) possess low material density (i.e., only 1/4 - 1/3 of high-temperature alloy) and high-temperature resistance, which can reduce cooling air and improve structure efficiency. Understanding the failure mechanisms and internal damage evolution represents an important step to ensure reliability and safety of CMCs. This book investigates damage and fracture of fiber-reinforced ceramic-matrix composites (CMCs) subjected to stochastic loading, including: (1) tensile damage and fracture of fiber-reinforced CMCs subjected to stochastic loading; (2) fatigue hysteresis loops of fiber-reinforced CMCs subjected to stochastic loading; (3) stress rupture of fiber-reinforced CMCs with stochastic loading at intermediate temperature; (4) fatigue life prediction of fiber-reinforced CMCs subjected to stochastic overloading stress at elevated temperature; and (5) fatigue limit stress prediction of fiber-reinforced CMCs with stochastic loading. This book helps the material scientists and engineering designers to understand and master the damage and fracture of ceramic-matrix composites under stochastic loading.

This book discusses the mechanisms of electric conductivity in various ionic liquid systems (protic, aprotic as well as polymerized ionic liquids). It hence covers the electric properties of ionic liquids and their macromolecular counterpanes, some of the most promising materials for the development of safe electrolytes in modern electrochemical energy devices such as batteries, super-capacitors, fuel cells and dye-sensitized solar cells. Chapter contributions by the experts in the field discuss important findings obtained using broadband dielectric spectroscopy (BDS) and other complementary techniques. The book is an excellent introduction for readers who are new to the field of dielectric properties of ionic conductors, and a helpful guide for every scientist who wants to investigate the interplay between molecular structure and dynamics in ionic conductors by means of dielectric spectroscopy.

Failure Mechanisms in Semiconductor Devices Second Edition E. Ajith Amerasekera Texas Instruments Inc., Dallas, USA Farid N. Najm University of Illinois at Urbana-Champaign, USA Since the successful first edition of Failure Mechanisms in Semiconductor Devices, semiconductor technology has become increasingly important. The high complexity of today's integrated circuits has engendered a demand for greater component reliability. Reflecting the need for guaranteed performance in consumer applications, this thoroughly updated edition includes more detailed material on reliability modelling and prediction. The book analyses the main failure mechanisms in terms of cause, effects and prevention and explains the mathematics behind reliability analysis. The authors detail methodologies for the identification of failures and describe the approaches for building reliability into semiconductor devices. Their thorough yet accessible text covers the physics of failure mechanisms from the semiconductor die itself to the packaging and interconnections. Incorporating recent advances, this comprehensive survey of semiconductor reliability will be an asset to both engineers and graduate students in the field.

The book describes developments in the crystal growth of bulk II-VI semiconductor materials. A fundamental, systematic, and in-depth study of the physical vapor transport (PVT) growth process is the key to producing high-quality single crystals of semiconductors. As such, the book offers a comprehensive overview of the extensive studies on ZnSe and related II-VI wide bandgap compound semiconductors, such as CdS, CdTe, ZnTe, ZnSeTe and ZnSeS. Further, it shows the detailed steps for the growth of bulk crystals enabling optical devices which can operate in the visible spectrum for applications such as blue light emitting diodes, lasers for optical displays and in the mid-IR wavelength range, high density recording, and military communications. The book then discusses the advantages of crystallization from vapor compared to the conventional melt growth: lower processing temperatures, the purification process associated with PVT, and the improved surface morphology of the grown crystals, as well as the necessary drawbacks to the PVT process, such as the low and inconsistent growth rates and the low yield of single crystals. By presenting in-situ measurements of transport rate, partial pressures and interferometry, as well as visual observations, the book provides detailed insights into in the kinetics during the PVT process. This book is intended for graduate students and professionals in materials science as well as engineers preparing and developing optical devices with semiconductors.

This collection focuses on all aspects of science and technology related to friction stir welding and processing.

With both nickel and cobalt featuring heavily in modern industry, there is an ongoing and intense interest in ore supplies and processing, applications development, and recycling. This book presents a collection of authoritative papers covering the latest advances in all aspects of nickel and cobalt processing, including fundamentals, technology, operating practices, and related areas of Platinum-Group Metals (PGM) processing. Special emphasis is given to the treatment of sulphide and laterite ores, concentrates, and secondary materials for the production of nickel and cobalt.

This volume introduces a comprehensive theory of deformation and fracture to engineers and applied scientists. Here "comprehensive" means that the theory can describe all stages of deformation from elastic to plastic and plastic to fracturing stage on the same basis (equations). The comprehensive approach is possible because the theory is based on a fundamental physical principle called the local symmetry, or gauge invariance, as opposed to phenomenology. Professor Yoshida explains the gist of local symmetry (gauge invariance) intuitively so that engineers and applied physicists can digest it easily, rather than describing physical or mathematical details of the principle. The author also describes applications of the theory to practical engineering, such as nondestructive testing in particular, with the use of an optical interferometric technique called ESPI (Electronic Speckle-Pattern Interferometry).The book is not a manual of applications. Instead, it provides information on how to apply physical concepts to engineering applications.

This book addresses the current status, challenges and future directions of data-driven materials discovery and design. It presents the analysis and learning from data as a key theme in many science and cyber related applications. The challenging open questions as well as future directions in the application of data science to materials problems are sketched. Computational and experimental facilities today generate vast amounts of data at an unprecedented rate. The book gives guidance to discover new knowledge that enables materials innovation to address grand challenges in energy, environment and security, the clearer link needed between the data from these facilities and the theory and underlying science. The role of inference and optimization methods in distilling the data and constraining predictions using insights and results from theory is key to achieving the desired goals of real time analysis and feedback. Thus, the importance of this book lies in emphasizing that the full value of knowledge driven discovery using data can only be realized by integrating statistical and information sciences with materials science, which is increasingly dependent on high throughput and large scale computational and experimental data gathering efforts. This is especially the case as we enter a new era of big data in materials science with the planning of future experimental facilities such as the Linac Coherent Light Source at Stanford (LCLS-II), the European X-ray Free Electron Laser (EXFEL) and MaRIE (Matter Radiation in Extremes), the signature concept facility from Los Alamos National Laboratory. These facilities are expected to generate hundreds of terabytes to several petabytes of in situ spatially and temporally resolved data per sample. The questions that then arise include how we can learn from the data to accelerate the processing and analysis of reconstructed microstructure, rapidly map spatially resolved properties from high throughput data, devise diagnostics for pattern detection, and guide experiments towards desired targeted properties. The authors are an interdisciplinary group of leading experts who bring the excitement of the nascent and rapidly emerging field of materials informatics to the reader.

This volume constitutes the state-of-the-art in active interrogation, widely recognized as indispensable methods for addressing current and future nuclear security needs. Written by a leading group of science and technology experts, this comprehensive reference presents technologies and systems in the context of the fundamental physics challenges and practical requirements. It compares the features, limitations, technologies, and impact of passive and active measurement techniques; describes radiation sources for active interrogation including electron and ion accelerators, intense lasers, and radioisotope-based sources; and it describes radiation detectors used for active interrogation. Entire chapters are devoted to data acquisition and processing systems, modeling and simulation, data interpretation and algorithms, and a survey of working active measurement systems. Active Interrogation in Nuclear Security is structured to appeal to a range of audiences, including graduate students, active researchers in the field, and policy analysts. The first book devoted entirely to active interrogation Presents a focused review of the relevant physics Surveys available technology Analyzes scientific and technology trends Provides historical and policy context Igor Jovanovic is a Professor of Nuclear Engineering and Radiological Sciences at the University of Michigan and has previously also taught at Penn State University and Purdue University. He received his Ph.D. from University of California, Berkeley and worked as physicist at Lawrence Livermore National Laboratory. Dr. Jovanovic has made numerous contributions to the science and technology of radiation detection, as well as the radiation sources for use in active interrogation in nuclear security. He has taught numerous undergraduate and graduate courses in areas that include radiation detection, nuclear physics, and nuclear security. At University of Michigan Dr. Jovanovic is the director of Neutron Science Laboratory and is also associated with the Center for Ultrafast Optical Science. Anna Erickson is an Assistant Professor in the Nuclear and Radiological Engineering Program of the G.W. Woodruff School of Mechanical Engineering at Georgia Institute of Technology. Previously, she was a postdoctoral researcher in the Advanced Detectors Group at Lawrence Livermore National Laboratory. Dr. Erickson received her PhD from Massachusetts Institute of Technology with a focus on radiation detection for active interrogation applications. Her research interests focus on nuclear non-proliferation including antineutrino analysis and non-traditional detector design and characterization. She teaches courses in advanced experimental detection for reactor and nuclear nonproliferation applications, radiation dosimetry and fast reactor analysis.

This book presents the select proceedings of the International Conference on Functional Material, Manufacturing and Performances (ICFMMP) 2019. The book primarily covers recent research, theories, and practices relevant to surface engineering and processing of materials. It focuses on the lesser-known technologies and advanced manufacturing methods which may not be standardized yet but are highly beneficial to material and manufacturing industrial engineers. The book includes current advances in the field of coating, deposition, cladding, nanotechnology, surface finishing, precision machining, processing, and emerging advanced manufacturing technologies which enhance the performance of materials in terms of corrosion, wear and fatigue. The book can be a valuable reference for beginners, researchers, and professionals interested in materials processing and allied fields.

This book demonstrates the potential of novel in-situ experiments, performed on microscopic and macroscopic length scales, for investigating localized deformation processes in metallic materials, particularly their kinetics and the associated evolution of local strain fields. It features a broad methodological portfolio, spanning optical and electron microscopy, digital image correlation, infrared theromgraphy and acoustic emission testing, and particularly focuses on identifying the localized microscopic deformation processes in high-strength/high-ductility CrMnNi TRIP/TWIP (TRansformation Induced Plasticity/TWinning Induced Plasticity) steels. Presenting state-of-the art methodology applied to topical and pertinent problems in materials engineering, this book is a valuable resource for researchers and graduate students working in the field of plasticity and deformation of structural materials.

This monograph deals with the mechanics and thermodynamics of materials with memory, including properties of the dynamical equations that describe their evolution in time under varying loads. A work in four parts, the first is an introduction to continuum mechanics, including classical fluid mechanics, linear and non-linear elasticity. The second part considers continuum thermodynamics and its use to derive constitutive equations of materials with memory, including viscoelastic solids, fluids, heat conductors and some examples of non-simple materials. In the third part, free energies for materials with linear memory constitutive relations are discussed. The concept of a minimal state is introduced. Explicit formulae are presented for the minimum and related free energies. The final part deals with existence, uniqueness, and stability results for the integrodifferential equations describing the dynamical evolution of viscoelastic materials, including a new approach based on minimal states rather than histories. There are also chapters on the controllability of thermoelastic systems with memory, the Saint-Venant problem for viscoelastic materials and on the theory of inverse problems. The second edition includes a new chapter on thermoelectromagnetism as well as recent findings on minimal states and free energies. It considers the case of minimum free energies for non-simple materials and dielectrics, together with an introduction to fractional derivative models.

The field of stress analysis has gained its momentum from the widespread applications in industry and technology and has now become an important part of materials science. Various destructive as well as nondestructive methods have been developed for the determination of stresses. This timely book provides a comprehensive review of the nondestructive techniques for strain evaluation written by experts in their respective fields.

The main part of the book deals with X-ray stress analysis (XSA), focussing on measurement and evaluation methods which can help to solve the problems of today, the numerous applications of metallic, polymeric and ceramic materials as well as of thin-film-substrate composites and of advanced microcomponents. Furthermore it contains data, results, hints and recommendations that are valuable to laboratories for the certification and accreditation of their stress analysis.

Stress analysis is an active field in which many questions remain unsettled. Accordingly, unsolved problems and conflicting results are discussed as well. The assessment of the experimentally determined residual and structural stress states on the static and dynamic behavior of materials and components is handled in a separate chapter.

Students and engineers of materials science and scientists working in laboratories and industries will find this book invaluable.

This book and its companion volumes contain plastics additives formulations based on information received from numerous industrial companies and other organizations. Each formulation is identified by a description of its end use.

Due to their high stiffness and strength and their good processing properties short fibre reinforced thermoplastics are well-established construction materials. Up to now, simulation of engineering parts consisting of short fibre reinforced thermoplastics has often been based on macroscopic phenomenological models, but deformations, damage and failure of composite materials strongly depend on their microstructure. The typical modes of failure of short fibre thermoplastics enriched with glass fibres are matrix failure, rupture of fibres and delamination, and pure macroscopic consideration is not sufficient to predict those effects. The typical predictive phenomenological models are complex and only available for very special failures. A quantitative prediction on how failure will change depending on the content and orientation of the fibres is generally not possible, and the direct involvement of the above effects in a numerical simulation requires multi-scale modelling. One the one hand, this makes it possible to take into account the properties of the matrix material and the fibre material, the microstructure of the composite in terms of fibre content, fibre orientation and shape as well as the properties of the interface between fibres and matrix. On the other hand, the multi-scale approach links these local properties to the global behaviour and forms the basis for the dimensioning and design of engineering components. Furthermore, multi-scale numerical simulations are required to allow efficient solution of the models when investigating three-dimensional problems of dimensioning engineering parts. Bringing together mathematical modelling, materials mechanics, numerical methods and experimental engineering, this book provides a unique overview of multi-scale modelling approaches, multi-scale simulations and experimental investigations of short fibre reinforced thermoplastics. The first chapters focus on two principal subjects: the mathematical and mechanical models governing composite properties and damage description. The subsequent chapters present numerical algorithms based on the Finite Element Method and the Boundary Element Method, both of which make explicit use of the composite's microstructure. Further, the results of the numerical simulations are shown and compared to experimental results. Lastly, the book investigates deformation and failure of composite materials experimentally, explaining the applied methods and presenting the results for different volume fractions of fibres. This book is a valuable resource for applied mathematics, theoretical and experimental mechanical engineers as well as engineers in industry dealing with modelling and simulation of short fibre reinforced composites.

Polycrystalline SiGe has emerged as a promising MEMS (Microelectromechanical Systems) structural material since it provides the desired mechanical properties at lower temperatures compared to poly-Si, allowing the direct post-processing on top of CMOS. This CMOS-MEMS monolithic integration can lead to more compact MEMS with improved performance. The potential of poly-SiGe for MEMS above-aluminum-backend CMOS integration has already been demonstrated. However, aggressive interconnect scaling has led to the replacement of the traditional aluminum metallization by copper (Cu) metallization, due to its lower resistivity and improved reliability. Poly-SiGe for MEMS-above-CMOS sensors demonstrates the compatibility of poly-SiGe with post-processing above the advanced CMOS technology nodes through the successful fabrication of an integrated poly-SiGe piezoresistive pressure sensor, directly fabricated above 0.13 m Cu-backend CMOS. Furthermore, this book presents the first detailed investigation on the influence of deposition conditions, germanium content and doping concentration on the electrical and piezoresistive properties of boron-doped poly-SiGe. The development of a CMOS-compatible process flow, with special attention to the sealing method, is also described. Piezoresistive pressure sensors with different areas and piezoresistor designs were fabricated and tested. Together with the piezoresistive pressure sensors, also functional capacitive pressure sensors were successfully fabricated on the same wafer, proving the versatility of poly-SiGe for MEMS sensor applications. Finally, a detailed analysis of the MEMS processing impact on the underlying CMOS circuit is also presented.

This book highlights time reversal acoustics, techniques based on the symmetry properties of acoustic fields. It has the unique feature that the first eleven chapters of the book are on the indepth studies of the theories of time reversal acoustics. The remaining chapters are on the four major applications of time reversal acoustics, together with their experimental setups and case studies: underwater communication, seismic exploration,nondestructive evaluation, and medical ultrasound imaging.. The gauge invariance approach to acoustic fields, proposed by the author in 2007, is confirmed by the successful fabrication of acoustical metamaterials and the applications of time reversal acoustics to superresolution. The book also presents groundbreaking applications of time reversal acoustics to underwater communication technology and the application of metamaterials to time reversal acoustics.

The series Advances in Polymer Science presents critical reviews of the present and future trends in polymer and biopolymer science. It covers all areas of research in polymer and biopolymer science including chemistry, physical chemistry, physics, material science. The thematic volumes are addressed to scientists, whether at universities or in industry, who wish to keep abreast of the important advances in the covered topics. Advances in Polymer Science enjoys a longstanding tradition and good reputation in its community. Each volume is dedicated to a current topic, and each review critically surveys one aspect of that topic, to place it within the context of the volume. The volumes typically summarize the significant developments of the last 5 to 10 years and discuss them critically, presenting selected examples, explaining and illustrating the important principles, and bringing together many important references of primary literature. On that basis, future research directions in the area can be discussed. Advances in Polymer Science volumes thus are important references for every polymer scientist, as well as for other scientists interested in polymer science - as an introduction to a neighboring field, or as a compilation of detailed information for the specialist. Review articles for the individual volumes are invited by the volume editors. Single contributions can be specially commissioned. Readership: Polymer scientists, or scientists in related fields interested in polymer and biopolymer science, at universities or in industry, graduate students

This book presents selected papers presented at the 8th International Conference "Design, Modeling and Experiments of Advanced Structures and Systems" (DeMEASS VIII, held in Moscow, Russia in May 2017) and reflects the modern state of sciences in this field. The contributions contain topics like Piezoelectric, Ferroelectric, Ferroelastic and Magnetostrictive Materials, Shape Memory Alloys and Active Polymers, Functionally Graded Materials, Multi-Functional Smart Materials and Structures, Coupled Multi-Field Problems, Design and Modeling of Sensors and Actuators, Adaptive Structures.