Strategies and Tactics in Organic Synthesis, Volume 15, provides a forum for investigators to discuss their approach to the science and art of organic synthesis. Rather than a simple presentation of data or a secondhand analysis, this classic provides stories that vividly demonstrate the power of the human endeavor known as organic synthesis and the creativity and tenacity of its practitioners. Firsthand accounts of each project present the excitement of conception, the frustration of failure and the joy experienced when either rational thought or good fortune gives rise to the successful completion of a project. Readers will be educated, challenged and inspired by these accounts, which portray the idea that triumphs do not come without challenges. This innovative approach also helps illustrate how challenges to further advance the science and art of organic synthesis can be overcome, driving the field forward to meet the demands of society by discovering new reactions, creating new designs and building molecules with atom and step economies that provide functional solutions to create a better world.

Modern Sample Preparation for Chromatography, Second Edition explains the principles of sample preparation for chromatographic analysis. A variety of procedures are applied to make real-world samples amenable for chromatographic analysis and to improve results. This book's authors discuss each procedure's advantages, disadvantages and their applicability to different types of samples, along with their fit for different types of chromatographic analysis. The book contains numerous literature references and examples of sample preparation for different matrices and new sections on green approaches in sample preparation, progress in automation of sample preparation, non-conventional solvents for LLE (ionic liquids, deep eutectic mixtures, and others), and more.

Annual Reports on NMR Spectroscopy, Volume 103, the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy includes a variety of updated chapters covering Recent Applications of 17O Solid State NMR in Biochemistry, NMR Studies of Ferromagnetic Materials, Very Fast MAS Solid State NMR Studies of Pharmaceuticals, Recent Advances in Benchtop NMR and Applications, Ultra-Fast Magic Angle Spinning Nuclear Magnetic Resonance.

Chemistry of Functional Materials Surfaces and Interfaces: Fundamentals and Applications gives a descriptive account of interfacial phenomena step-by-step, from simple to complex, to provide readers with a strong foundation of knowledge in interfacial materials chemistry. Many case studies are provided to give real-world examples of problems and their solutions, allowing readers to make the connection between fundamental understanding and applications. Emerging applications in nanomaterials and nanotechnology are also discussed. Throughout the book, the author explains the common interface and surface equations, models, methods, and applications in the creation of functional materials. The goal of Chemistry of Functional Materials Surfaces and Interfaces is to provide readers with the basic understanding of the common tools of surface and interface chemistry for application in materials science and nanotechnology. This book is suitable for researchers and practitioners in the disciplines of materials science and engineering and surface and interface chemistry.

Spectroscopy, Diffraction and Tomography in Art and Heritage Science gives an overview of the main spectroscopy and diffraction techniques currently available for cultural heritage research. It starts with an introductory, general discussion of spectroscopy and diffraction and the kinds of information they can give. Further sections deal with, respectively, typical laboratory methods, mobile equipment, and large-scale instruments and infrastructural methods. The work concludes with comments on combining and comparing multiple techniques, sources of error, and limitations of the analytical methods.

Metal-Catalyzed Asymmetric Hydrogenation, Volume 68 in the Advances in Catalysis series, fills the gap between journal papers and textbooks across diverse areas of catalysis research. For more than 60 years, this series has recorded and presented the latest progress in the field of catalysis, giving the scientific community comprehensive and authoritative reviews. Chapters in this new release include Asymmetric hydrogenation of functionalized olefins, Asymmetric hydrogenation of unfunctionalized olefins or with poorly coordinative groups, Asymmetric hydrogenation of imines, Asymmetric hydrogenation of ketones, Asymmetric hydrogenation in industry, and Computational insights into metal-catalyzed asymmetric hydrogenation. This series is an invaluable and comprehensive resource for chemical engineers and chemists working in the field of catalysis in both academia and industry, with this release focusing on solid acids, surface acidity and heterogeneous acid catalysis.

Applications of Heterocycles in the Design of Drugs and Agricultural Products, Volume 134 in the Advances in Heterocyclic Chemistry series represents the most definitive series in the field - one of great importance to organic chemists, polymer chemists, and many biological scientists. Chapters in this updated volume cover Hydroxy azoles as carboxylic acid bioisosteres, Cyclic sulfoxides and sulfones in drug design, Thiazoles and topological control in drug design, Applications of fused pyrrolidine [3.3.0] heterocycles in drug design, 1,4 Disubstituted and 1,4,5 trisubstituted-1,2,3-triazoles in drug discovery and development: from the flask to the clinic, and Conformationally restricted [3.2.2]- and [3.2.1]-3-azabicyclic diamines. Because biology and organic chemistry increasingly intersect, the associated nomenclature is being used more frequently in explanations. Written by established authorities in the field from around the world, this comprehensive review combines descriptive synthetic chemistry and mechanistic insight to yield an understanding of how chemistry drives the preparation and useful properties of heterocyclic compounds.

Practical Guide to Rotational Moulding, Third Edition, takes a step-by-step approach to rotomoulding, covering applications, moulds, machinery, materials, and design. This third edition has been thoroughly revised to include the latest advances, including novel materials and moulds, new products, and automation. The book begins with a chapter that introduces the rotational moulding process, analyses advantages and disadvantages, and explores common applications for rotomoulded products. The subsequent chapters provide detailed, methodical coverage of moulds, machinery, materials, and design for functionality, supported by clear illustrations and diagrams. Finally, challenges and future developments are discussed. This hands-on technical guide helps engineers, designers and practitioners to understand all aspects of rotomoulding, with the aim of producing performant end products and parts, with uniform wall thickness and potentially in complex shapes. The book is also of great interest to professionals across the plastics industry, as well as researchers and advanced students in plastics engineering, industrial design, mechanical engineering, chemical engineering, and materials science and engineering.

Conducting Polymer-Based Nanocomposites: Fundamentals and Applications delivers an up-to-date overview on cutting-edge advancements in the field of nanocomposites derived from conjugated polymeric matrices. Design of conducting polymers and resultant nanocomposites has instigated significant addition in the field of modern nanoscience and technology. Recently, conducting polymer-based nanocomposites have attracted considerable academic and industrial research interest. The conductivity and physical properties of conjugated polymers have shown dramatic improvement with nanofiller addition. Appropriate fabrication strategies and the choice of a nanoreinforcement, along with a conducting matrix, may lead to enhanced physicochemical features and material performance. Substantial electrical conductivity, optical features, thermal stability, thermal conductivity, mechanical strength, and other physical properties of the conducting polymer-based nanocomposites have led to high-performance materials and high-tech devices and applications. This book begins with a widespread impression of state-of-the-art knowledge in indispensable features and processing of conducting polymer-based nanocomposites. It then discusses essential categories of conducting polymer-based nanocomposites such as polyaniline, polypyrrole, polythiophene, and derived nanomaterials. Subsequent sections of this book are related to the potential impact of conducting polymer-based nanocomposites in various technical fields. Significant application areas have been identified for anti-corrosion, EMI shielding, sensing, and energy device relevance. Finally, the book covers predictable challenges and future opportunities in the field of conjugated nanocomposites.

Processing Technology for Bio-Based Polymers: Advanced Strategies and Practical Aspects brings together the latest advances and novel technologies surrounding the synthesis and manufacture of biopolymers, ranging from bio-based polymers to synthetic polymers from bio-derived monomers. Sections examine bio-based polymer chemistry, discuss polymerization process and emerging design technologies, cover manufacturing and processing approaches, explain cutting-edge approaches and innovative applications, and focus on biomedicals and other key application areas. Final chapters provide detailed discussion and an analysis of economic and environmental concerns, practical considerations, challenges, opportunities and future trends. This is a valuable resource for researchers, scientists and advanced students in polymer science, bio-based materials, nanomaterials, plastics engineering, biomaterials, chemistry, biotechnology, and materials science and engineering, as well as R&D professionals, engineers and industrialists interested in the development of biopolymers for advanced products and applications.

The Thermodynamics of Phase and Reaction Equilibria, Second Edition, provides a sound foundation for understanding abstract concepts of phase and reaction equilibria (e.g., partial molar Gibbs energy, fugacity, and activity), and shows how to apply these concepts to solve practical problems using numerous clear examples. Available computational software has made it possible for students to tackle realistic and challenging problems from industry. The second edition incorporates phase equilibrium problems dealing with nonideal mixtures containing more than two components and chemical reaction equilibrium problems involving multiple reactions. Computations are carried out with the help of Mathcad (R).

Fundamentals and Recent Advances in Nanocomposites Based on Polymers and Nanocellulose brings together the latest research in cellulose-based nanocomposites, covering fundamentals, processing, properties, performance, applications, and the state of the art. The book begins by explaining the fundamentals of cellulose and cellulose-based nanocomposites, including sources, extraction, types, classification, linkages, model structure, model compounds, and characterization techniques. The second part of the book covers the incorporation of cellulose fillers to improve the properties or characteristics of nanocomposites, organized by composite category, including in aerogels, thermoplastic composites, thermoset composites, bioplastic composites, carbon nanofibers, rubber composites, carbon fibers, and foaming materials. Throughout these chapters, there is an emphasis on the latest innovations and application potential. Finally, applications are explored in more detail, notably focusing on the utilization of nanocellulose in biodegradable composites for biomedical applications, along with other important industrial application areas. This book is of great interest to researchers, scientists, and advanced students working with bio-based materials, and across polymer science, nanomaterials, composite materials, plastics engineering, chemical engineering, materials science and engineering, as well as R&D professionals, engineers, and industrialists interested in the development of bio-based materials for advanced applications or material commercialization.

Gas Chromatography, Second Edition, offers a single source of authoritative information on all aspects relating to the practice of gas chromatography. A focus on short, topic-focused chapters facilitates the identification of information that will be of immediate interest for familiar or emerging uses of gas chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh and deepen their understanding of fundamental and instrumental aspects of gas chromatography and tools for the interpretation and management of chromatographic data. Users will find a consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This new edition restores the contemporary character of the book with respect to those involved in advancing the technology, analyzing the data produced, or applying the technique to new application areas. New topics covered include hyphenated spectroscopic detectors, micromachined instrument platforms, derivatization and related microchemical techniques, petrochemical applications, volatile compounds in the atmosphere, and more.

Studies in Natural Products Chemistry, Volume 69 covers the synthesis, testing and recording of the medicinal properties of natural products, providing cutting-edge accounts of fascinating developments in the isolation, structure elucidation, synthesis, biosynthesis and pharmacology of a diverse array of bioactive natural products. Natural products in the plant and animal kingdom offer a huge diversity of chemical structures that are the result of biosynthetic processes. With rapid developments in spectroscopic techniques and accompanying advances in high-throughput screening techniques, it has become possible to rapidly isolate and determine the structures and biological activity of natural products, thus opening up opportunities in drug development.

Analysis and Characterisation of Metal-Based Nanomaterials, Volume 93 in the Comprehensive Analytical Chemistry series, introduces recent developments in analytical methodologies for detection, characterization and quantification of metal-based nanomaterials and their applications to a variety of complex environmental, biological and food samples as well as different consumer products. Single-particle inductively coupled plasma mass spectrometry is highlighted as a powerful analytical tool for number-based concentration and size distribution, also from the metrological viewpoint. An emerging approach for the measurement of multi-metal nanoparticles by single-particle inductively coupled plasma time-of-flight mass spectrometry is discussed. Imaging of metal-based nanoparticles by hyphenated inductively coupled plasma-based techniques is also introduced. The potential of different liquid chromatography and field flow fractionation separation techniques hyphenated to inductively coupled plasma mass spectrometry is emphasized as a powerful tool in particular for complex matrices and small particles sizes. The use of different microscopic techniques for the characterization of metal-based nanoparticles and characterization of metal-based nanoparticles as contrast agents for magnetic resonance imaging are presented. Moreover, occurrence, behaviour and fate of inorganic nanoparticles in the environment is overviewed. Finally, the need for quality control standards and reference nano-materials is emphasized throughout.

Graphene to Polymer/Graphene Nanocomposites: Emerging Research and Opportunities brings together the latest advances and cutting-edge methods in polymer/graphene nanocomposites that offer attractive properties and features, leading to a broad range of valuable applications. The initial chapters of this book explain preparation, properties, modification, and applications of graphene and graphene-based multifunctional polymeric nanocomposites. Later, the state-of-the-art potential of polymer/graphene nanocomposites for hierarchical nanofoams, graphene quantum dots, graphene nanoplatelets, graphene nanoribbons, etc., has been elucidated. The subsequent chapters focus on specific innovations and applications including stimuli-responsive graphene-based materials, anticorrosive coatings, applications in electronics and energy devices, gas separation and filtration membrane applications, aerospace applications, and biomedical applications. Throughout the book, challenges, and future opportunities in the field of polymer/graphene nanocomposites are discussed and analyzed. This is an important resource for researchers, scientists, and students/academics working with graphene and across the fields of polymer composites, nanomaterials, polymer science, chemistry, chemical engineering, biomedical engineering, materials science, and engineering, as well those in an industrial setting who are interested in graphene or innovative materials.

Chemistry, Manufacture and Applications of Natural Rubber, Second Edition presents the latest advances in the processing, properties and advanced applications of natural rubber (NR), drawing on state-of-the-art research in the field. Chapters cover manufacturing, processing and properties of natural rubber, describing biosynthesis, vulcanization for improved performance, strain-induced crystallization, self-reinforcement, rheology and mechanochemistry for processing, computer simulation of properties, scattering techniques and stabilizing agents. Applications covered include natural rubber, carbon allotropes, eco-friendly soft bio-composites using NR matrices and marine products, the use of NR for high functionality such as shape memory, NR for the tire industry, and natural rubber latex with advanced applications. This is an essential resource for academic researchers, scientists and (post)graduate students in rubber science, polymer science, materials science and engineering, and chemistry. In industry, this book enables professionals, R&D, and producers across the natural rubber, tire, rubber and elastomer industries, as well as across industries looking to use natural rubber products, to understand and utilize natural rubber for cutting-edge applications.

Catalysis in Biomass Conversion, Volume 77 in the Advances in Inorganic Chemistry series, presents timely and informative summaries on current progress in a variety of subject areas. This acclaimed serial features reviews written by experts in the field, serving as an indispensable reference to advanced researchers that empowers readers to pursue new developments in each field. Users will find this to be a comprehensive overview of recent findings and trends from the last decade that covers various kinds of inorganic topics, from theoretical oriented supramolecular chemistry, to the quest for accurate calculations of spin states in transition metals.

Sample Return Missions: The Last Frontier of Solar System Exploration examines the discoveries and results obtained from sample return missions of the past, present, and future. It analyses the results in the context of the current state of knowledge and their relation to the formation and evolution of planetary bodies, as well as to the available technologies and techniques. It provides detailed descriptions of experimental procedures applied to returned samples. Beginning with an overview of previous missions, Sample Return Missions then goes on to provide an overview of facilities throughout the world used to analyze the returned samples. Finally, it addresses techniques for collection, transport, and analysis of the samples, with an additional focus on lessons learned and future perspectives. Providing an in-depth examination of a variety of missions, with both scientific and engineering implications, this book is an important resource for the planetary science community, as well as the experimentalist and engineering communities.

Natural Polyphenols from Wood: Tannin and Lignin - An Industrial Perspective is a detailed guide to the sourcing and processing of tannin and lignin for valuable advanced applications across areas such as fuels, chemicals, drugs, and food. Drawing on the latest academic research and patent literature, this book provides strong practical understanding of the use of these valuable materials in novel industrial applications. This book introduces natural polyphenols from wood and the fundamental aspects of carbon management within the tree. In-depth presentation of extraction and characterization methods is followed by an extensive coverage of practical and industrial applications of wood polyphenols. This is an essential resource for researchers and advanced students working with lignin or tannin, and across biopolymer science, biomass, wood chemistry, paper, wood adhesives, polymer materials, renewable resources, and biotechnology. It also supports industrial R&D and scientists working with wood polyphenols or bio-based polymers.

Adsorption: Fundamental Processes and Applications, Volume 33 in the Interface Science and Technology Series, discusses the great technological importance of adsorption and describes how adsorbents are used on a large scale as desiccants, catalysts, catalyst supports, in the separation of gases, the purification of liquids, pollution control, and in respiratory protection. Finally, it explores how adsorption phenomena play a vital role in many solid-state reactions and biological mechanisms, as well as stressing the importance of the widespread use of adsorption techniques in the characterization of surface properties and the texture of fine powders.