This volume entitled Advanced Science and Technology of Sintering, contains the edited Proceedings of the Ninth World Round Table Conference on Sintering (IX WRTCS), held in Belgrade, Yugoslavia, September 1-4 1998. The gathering was one in a series of World Round Table Conferences on Sintering organised every four years by the Serbian Academy of Sciences and Arts (SASA) and the International Institute for the Science of Sintering (IISS). The World Round Table Conferences on Sintering have been traditionally held in Yugoslavia. The first meeting was organised in Herceg Novi in 1969 and since then they have regularly gathered the scientific elite in the science of sintering. It is not by chance that, at these conferences, G. C. Kuczynski, G. V. Samsonov, R. Coble, Ya. E. Geguzin and other great names in this branch of science presented their latest results making great qualitative leaps in the its development. Belgrade hosted this conference for the first time. It was chosen as a reminder that 30 years ago it was the place where the International Team for Sintering was formed, further growing into the International Institute for the Science of Sintering. The IX WRTCS lasted four days. It included 156 participants from 17 countries who presented the results of their theoretical and experimental research in 130 papers in the form of plenary lectures, oral presentations and poster sections.

Ordered intermetallics constitute a unique class of metallic materials which may be developed as new-generation materials for structural use at high temperatures in hostile environments. At present, there is a worldwide interest in intermetallics, and extensive efforts have been devoted to intermetallic research and development in the U.S., Japan, European countries, and other nations. As a result, significant advances have been made in all areas of intermetallic research. This NATO Advanced Workshop on ordered intermetallics (1) reviews the recent progress, and (2) assesses the future direction of intermetallic research in the areas of electronic structure and phase stability, deformation and fracture, and high-temperature properties. The book is divided into six parts: (1) Electronic Structure and Phase Stability; (2) Deformation and Dislocation Structures; (3) Ductility and Fracture; (4) Kinetic Processes and Creep Behavior; (5) Research Programs and Highlights; and (6) Assessment of Current Research and Recommendation for Future Work. The first four parts review the recent advances in the three focus areas. The fifth part provides highlights of the intermetallic research under major programs and in different institutes and countries. The last part provides a forum for the discussion of research areas for future studies.

Covering current advances in the science and technology of polymeric and organic materials, each chapter is a self-contained review of progress, and particular emphasis has been placed on obtaining an overall understanding of the state of the art in each area. This is the first book to provide a background perspective on this field of research, and is suitable for both professional researchers and postgraduate students.

This concise survey describes the requirements on materials operating in high-temperature environments and the processes that increase the temperature capability of metals, ceramics, and composites. The major part deals with the applicable materials and their specific properties, with one entire chapter devoted to coatings. Written for engineering and science students, researchers, and managers in industry.

The development of new experimental techniques to study phenomena, such as the anomalous skin effect, cyclotron resonance in magnetic fields normal to then metal surface, and high-frequency properties of metals, as well as the discovery of collective excitations arising from electron-electron correlations, have offered a new impetus for the analysis of the electronic properties of metals. This book discusses the local geometry of the Fermi surface and its effects on high-frequency phenomena in metals and metallic conductors. After an introductory chapter reviewing the electron-liquid theory of metals the discussion turns to techniques useful in analyzing properties of real Fermi surfaces, which are rarely spherical. In subsequent chapters these techniques are applied to concrete problems such as the anomalous skin effect, cyclotron resonance, attenuation of ultrasonic fields, dopplerons, the effects of zero-curvature portions of the Fermi surface, and the behavior of the Fermi surface in low-dimensional structures.

The microanalytical technique of atom probe tomography (APT) permits the spatial coordinates and elemental identities of the individual atoms within a small volume to be determined with near atomic resolution. Therefore, atom probe tomography provides a technique for acquiring atomic resolution three dimensional images of the solute distribution within the microstructures of materials. This monograph is designed to provide researchers and students the necessary information to plan and experimentally conduct an atom probe tomography experiment. The techniques required to visualize and to analyze the resulting three-dimensional data are also described. The monograph is organized into chapters each covering a specific aspect of the technique. The development of this powerful microanalytical technique from the origins offield ion microscopy in 1951, through the first three-dimensional atom probe prototype built in 1986 to today's commercial state-of-the-art three dimensional atom probe is documented in chapter 1. A general introduction to atom probe tomography is also presented in chapter 1. The various methods to fabricate suitable needle-shaped specimens are presented in chapter 2. The procedure to form field ion images of the needle-shaped specimen is described in chapter 3. In addition, the appearance of microstructural features and the information that may be estimated from field ion microscopy are summarized. A brief account of the theoretical basis for processes of field ionization and field evaporation is also included.

Frontiers in Magnetism of Reduced Dimension Systems presents a definitive statement of our current knowledge and the state of the art in a field that has yet to achieve maturity, even though there are a number of potential applications of thin magnetic films and multilayers, such as magnetic sensors, data storage/retrieval media, actuators, etc. The book is organized into 13 chapters, each including a lecture and contributed papers on a similar subject. Five chapters deal with theoretical descriptions of electron transport phenomena, relaxation processes, nonlinear paramagnetic interactions, phase transitions and macroscopic quantum effects in magnetic films and particles. The description of different characterization techniques occupies an important place in the book. Separate chapters are dedicated to magnetic resonances (FMR, SWR, NMR), magneto-optical spectroscopy, controlling chaos, magnetoelastic phenomena and magnetic resonance force microscopy. A further chapter gives a detailed review, spread over a number of papers, of materials in current use in information storage devices.

Silicon Carbide Microsystems for Harsh Environments reviews state-of-the-art Silicon Carbide (SiC) technologies that, when combined, create microsystems capable of surviving in harsh environments, technological readiness of the system components, key issues when integrating these components into systems, and other hurdles in harsh environment operation. The authors use the SiC technology platform suite the model platform for developing harsh environment microsystems and then detail the current status of the specific individual technologies (electronics, MEMS, packaging). Additionally, methods towards system level integration of components and key challenges are evaluated and discussed based on the current state of SiC materials processing and device technology. Issues such as temperature mismatch, process compatibility and temperature stability of individual components and how these issues manifest when building the system receive thorough investigation. The material covered not only reviews the state-of-the-art MEMS devices, provides a framework for the joining of electronics and MEMS along with packaging into usable harsh-environment-ready sensor modules.

Thisbookiswrittenforthosescientistsandengineerswhowishtounderstand the synthesis, physical and chemical properties, and applications of inorganic and metallic nanotubular materials. The original version of this book, written inJapanese,coveredthoseoforganic,inorganic,andmetallicnanotubular- terials or almost all the other nanotubular materials than carbon nanotubes. This English version is concerned with only the chapters of inorganic and metallic nanotubular materials. In most industries worldwide, recent attention is unexceptionally focused on the research and development of highly functional new materials or te- nologies leading to energetically highly e?cient activities. Nanotubular - terials are one of the materials with such technological potentials because of their nano-sized unique structures available, for example, functionalization at their internal and external surfaces. In 1991, Dr. S. Iijima discovered a tu- lar material of carbon and named it carbon nanotubes. Since then, worldwide attention has been focused on the basic and functional properties of the novel materials and in more recent times the research phase has developed into an advanced stage based on strategic researches toward various applications. Carbon nanotubes have thus become synonymous with nanotubular materials and still more a symbol of nanotechnology because of their unique, valuable, and versatile properties.

In this, the only book available to combine both theoretical and practical aspects of x-ray diffraction, the authors emphasize a "hands on" approach through experiments and examples based on actual laboratory data. Part I presents the basics of x-ray diffraction and explains its use in obtaining structural and chemical information. In Part II, eight experimental modules enable the students to gain an appreciation for what information can be obtained by x-ray diffraction and how to interpret it. Examples from all classes of materials -- metals, ceramics, semiconductors, and polymers -- are included. Diffraction patterns and Bragg angles are provided for students without diffractometers. 192 illustrations.

A conference on Metallurgical Effects at High Strain Rates was held at Albuquerque, New Mexico, February 5 through 8, 1973, under joint sponsorship of Sandia Laboratories and the Physical Metallurgy Committee of The Metallurgical Society of AIME. This book presents the written proceedings of the meeting. The purpose of the conference was to gather scientists from diverse disciplines and stimulate interdisciplinary discussions on key areas of materials response at high strain rates. In this spirit, it was similar to one of the first highly successful con ferences on this subject held in 1960, in Estes Park, Colorado, on The Response of Metals to High Velocity Deformation. The 1973 conference was able to demonstrate rather directly the increased understanding of high strain rate effects in metals that has evolved over a period of roughly 12 years. In keeping with the interdisciplinary nature of the meeting, the first day was devoted to a tutorial session of invited papers to provide attendees of diverse backgrounds with a common basis of understanding. Sessions were then held with themes centered around key areas of the high strain rate behavior of metals."

"High Performance Grinding and Advanced Cutting Tools" discusses the fundamentals and advances in high performance grinding processes, and provides a complete overview of newly-developing areas in the field. Topics covered are grinding tool formulation and structure, grinding wheel design and conditioning and applications using high performance grinding wheels. Also included are heat treatment strategies for grinding tools, using grinding tools for high speed applications, laser-based and diamond dressing techniques, high-efficiency deep grinding, VIPER grinding, and new grinding wheels.

The increasing use of powder metallurgy techniques to make an almost infinite variety of materials and products places greater emphasis on utilization of sophisticated experimental techniques. Usually research and development efforts initiate the use of newly developed equipment and analytical procedures. Indeed, the contents of this book are strongly linked to research endeavors, in both the academic and industrials worlds. However, this volume can serve a much needed function in industrial applied powder metallurgy. Although many research ers will find the contents of great value, the technical personnel more involved with production, quality control, customer services and product design now have at their dispo sal a means to learn about the potential uses of several very important techniques. With today's "knowledge explosion" the present set of papers greatly facilitates the comprehension and adoption of new procedures. If powder metallurgy is to continue its rapid rate of growth in virtually all segments of industry, then the transition of modern equipment and procedures from tools of research and development laboratories to everyday plant operations and applications must be hastened. The editors hope that this volume aids in this process, as well as assisting students and researchers by providing a ready source of up-to-date useful information.

Fermi Surfaces of Low-Dimensional Organic Metals and Superconductors is an introduction to quasi-one- and quasi-two-dimensional organic metals and a review of the current knowledge on the electronic structure of these materials. The principal structural, electronic, and superconducting properties are described and illustrated with many examples. The book introduces the basic theoretical concepts necessary for the understanding of the experimental techniques and reviews in detail recent results in the investigation of the Fermi surface topology. The book is intended both as an introduction and as a reference book for active researchers.

The International Symposium on Shape Memory Effects and Appli cations was held at the University of Toronto on May 19-20, 1975, in four sessions over two days, as part of the regular 1975 Spring Meeting of The Metallurgical Society of AlME, sponsored by the Physical Metallurgy Committee of The Metallurgical Society. This was the first symposium on the subject, the only previous meeting at all related being the 1968 NOL Symposium on TiNi and Associated Compounds. One of the major intentions of this Symposium was to provide a forum for cross-communication between workers in the diverse metallurgical areas pertinent to shape memory effects, areas such as martensitic transformation, crystallography and thermodynamics, mechanical behavior, stress-induced transformation, lattice sta bility, and alloy development. Authors were encouraged to place an emphasis on delineation of general controlling factors and mech anisms, and on comparison of shape memory effect alloy systems with systems not exhibiting SME."

Electrometallurgy is a broad field but it is not a new one. It was the great Faraday in the 1830s who discovered laws covering the electrodeposition of metals and its relation to the current passed and equivalent weight of the metal undergoing depo- tion. Since that time, applications and developments of his discoveries have spread to many areas of technology. Electrowinning is the most well known, partly because it embraces the process by which aluminum is extracted from its ores. In electrorefining, the impure metal is made into anode and the pure metal dissolved therefrom is deposited on a cathode. Electroplating is exemplified by its use in the manufacture of car bumpers. Finally, in electroreforming, objects may be metallized, often with a very thin layer of the coating desired. The numerous technologies vary greatly in the degree to which they are intell- tualized. Until the work of Popov et al. , electrometallurgy has been regarded as largely empirical, an activity in which there was much art and little science. This will all change with the publication of this book. Several aspects of the background of its senior author, Konstantin Popov, make him uniquely suited to the job of intellectual- ing electrometallurgy. First, he had as his mentor the great surely the leading electrochemist in Eastern Europe since the death of Frumkin. Second, he has had ample experience with the leading electrochemical engineer in America, Ralph White.

Corrosion affects every industry in which metal is involved, from manufacturing machinery to transport pipelines, and it is estimated to cost the global economy trillions of dollars per year. Many of the traditional methods for inhibiting corrosion are highly toxic (such as hexavalent chromium) or do not degrade readily in the environment (such as Benzotriazole) meaning they pose a risk to human and environmental health. Much recent work in the area has gone into searching for greener alternatives that will be both safe and effective. Beginning with a look at the fundamentals of corrosion inhibition and an explanation of the concepts of green chemistry, this book discusses various types of chemical that have been tested for their potential as greener corrosion inhibitors with reference to industrial applications. Green Corrosion Inhibition is a valuable reference for chemists and chemical engineers working in both research and design and academia who want to learn more about green corrosion inhibitors, their synthesis, design, and industrial scale applications.

Five years ago, the worldwide powder metallurgy fraternity gathered in New York City to attend the first international conference devoted entirely to powder metal lurgy to take place in the United States. It was a tentative venture, entered into by the sponsors with no idea as to whether it would fail or succeed. The only assurances we had were that the metal-powder producing and consuming industries were rapidly expanding and that powder metallurgy was truly becoming one of the international sciences. The 1960 Conference was successful not only in terms of attendance and interest, but also in terms of knowledge gained. The literature had been enriched by the contributions of its participants to foster and encourage this type of world wide exchange. Thus, another such conference was held in 1965-expanded in scope and supplemented by an exhibition of the latest advances in raw materials, processing equipment, and finished products of powder metallurgy. On behalf of the Conference sponsors-the Metal Powder Industries Federa tion, the American Powder Metallurgy Institute, and the Metallurgical Society of AIME-I thank all those who participated and who helped make the 1965 Interna tional Powder Metallurgy Conference a rewarding experience and memorable event in our industry's history. Support of the National Science Foundation, which made it possible for several speakers from abroad to participate in the program, is gratefully acknowledged.

"Modern Physical Metallurgy" describes, in a very readable form, the fundamental principles of physical metallurgy and the basic techniques for assessing microstructure. This book enables you to understand the properties and applications of metals and alloys at a deeper level than that provided in an introductory materials course.

The eighth edition of this classic text has been updated to provide a balanced coverage of properties, characterization, phase transformations, crystal structure, and corrosion not available in other texts, and includes updated illustrations along with extensive new real-world examples and homework problems.
Renowned coverage of metals and alloys from one of the world's leading metallurgy educatorsCovers new materials characterization techniques, including scanning tunneling microscopy (STM), atomic force microscopy (AFM), and nanoindentationProvides the most thorough coverage ofcharacterization, mechanical properties, surface engineering and corrosion of any textbook in its fieldIncludes new worked examples with real-world applications, case studies, extensive homework exercises, and a full online solutions manual and image bank"

In view of the dramatically increased interest in the study of grain boundaries during the past few years, the Physical Metal lurgy Committee of The Institute of Metals Division of The Metal lurgical Society, AIME, sponsored a four-session symposium on the NATURE AND BEHAVIOR OF GRAIN BOUNDARIES, at the TMS-AIME Fall Meeting in Detroit, Michigan, October 18-19, 1971. The main ob jectives of this symposium were to examine the more recent develop ments, theoretical and experimental, in our understanding of grain boundaries, and to stimulate further studies in these and related areas. This volume contains most of the papers presented at the Symposium. It is regrettable that space limitations allow the inclusion of only four of the unsolicited papers, in addition to thirteen invited papers. The papers are grouped into three sections according to their major content: STRUCTURE OF GRAIN BOUNDARIES, ENERGETICS OF GRAIN BOUNDARIES, and GRAIN BOUNDARY MOTION AND RELATED PHENOMENA. Grain boundaries, or crystal interfaces, have been of both academic and practical interest for many years. An early seminar on "Metal Interfaces" was documented in 1952 by ASM. The Fourth Metallurgical Colloquium held in France, 1960, had a broad coverage on "Properties of Grain Boundaries". More recently the Australian Institute of Metals sponsored a conference on interfaces, with the proceedings being published by Butterworths in 1969.

This publication documents Proceedings of the Symposium on Metal lurgy and Technology of Refractory Metal Alloys, held in Washington, D.C. at the Washington Hilton Hotel on April 25-26, 1968, under sponsorship of the Refractory Metals Committee, Institute of Metals Division, of the Metallurgical Society of AIME, and the National Aeronautics and Space Administration. The Symposium presented critical reviews of selected topics in refractory metal alloys, thereby contributing to an in-depth understanding of the state-of-the-art, and establishing a base line for further research, development, and application. This Symposium is fifth in a series of conferences on refractory metals, sponsored by the Metallurgical Society of AlME. Publications issuing from the conferences are valuable technical and historical source books, tracing the evolution of refractory metals from early laboratory alloying studies to their present status as useful engineering materials. Refractory metals are arbitrarily defined by melting point. A 0 melting temperature of over 3500 F was selected as the minimum for this Symposium, thus excluding chromium and vanadium, which logically could be treated with other refractory metals in Groups VA and VIA of the periodic table. The Refractory Metals Committee is planning reviews of chromium and vanadium in subsequent conferences.

An uncomfortable observation in the Shift Logs and Process Control records of most aluminum smelting plants is that process control failures, large and small, happen every day. Although only a small fraction of these failures give rise to catastrophic events, the difference between a disaster we read about and a failure which, although expensive, has no irreversible consequences, is only chance. Control for Aluminum Production and Other Processing Industries exemplifies new control thinking fused with an understanding of process variability, and how to diagnose abnormalities and their causes in aluminum production plants. Many real life examples in the book demonstrate the importance of human behavior and a scientific, questioning approach in the control of a technologically complex process. Written from the perspective of production staff and management, the book also gives readers a view into the human aspects of accidents and their analogy with failures in control of production. Production plants regularly experience more control failures than successes and staff must continuously strive to establish stability and control of their process. Through on-the-job experiences of the authors and their industry colleagues, the control experiences described in this book provide readers with a foundation for building their own robust control rationale and a framework for avoidance of plant control problems.

Atomic diffusion in metals was first discovered some sixty-five years ago, and since then a considerable wealth of data has ac cumulated on diffusion in various systems. However, work prior to about the year 1940 is now mainly of historical interest, since ex periments were often carried out under experimental conditions and with methods of analysis leading to uncertainties in inter preting the measured diffusion coefficients. Data on diffusion rates are of importance in processes which are controlled by rates of atomic migration such as growth of phases and homogenization of alloys. In addition diffusion plays an important part in theories of such phenomena as oxidation, plastic deformation, sintering, and creep. A tremendous advance in diffusion studies was made possible by the availability of radioactive isotopes of sufficiently high spe cific activity after the second world war. Measurements of self diffusion rates then became possible using radioactive isotopes having the same chemical properties as the solvent material, and it also became possible to study tracer impurity diffusion when the concentration of the impurity is so small as not to alter the chemi cal homogeneity of the system. In the last ten to fifteen years the purity of materials used in diffusion studies has increased con siderably and the methods of analysis have become more stand ardized."

During the translation, the author had the opportunity to re view several chapters, taking into consideration the more recent literature. As far as possible all new theoretical concepts and experi mental data published before 1963 have been quoted and discussed under the theoretical viewpoint of this book. A new chapter "Passivity and Inhibition During High-Tempera ture Oxidation" was introduced. Section 4.8 was enlarged by a dis cussion of the transition from internal to external oxidation. The author very much appreciates the cooperation of the trans lator and of Plenum Press. Gottingen, April 1.965 Karl Hauffe v Preface The number of publications concerned with oxidation and cor rosion processes has become so copious that many engineers and scientists find it practically impossible to obtain an overall view of the growing body of knowledge and to bring order to the confusing multiplicity of experimental data. As a result the need for a compre hensive survey of the present state of research in this field has be come more and more urgent."

THE PHYSICAL BASIS FOR HETEROGENEOUS CATALYSIS is the proceedings of the ninth Battelle Colloquium in the Materials Sciences, held in Gstaad, Switzerland, September 2-6, 1974. It took as its theme the application of modern theoretical and experimental surface physics to heterogeneous catalysis. Progress in the field by classical chemical methods seemed to have slowed down, at a time when the need for better catalysts was particularly great. The Organizing Committee thought it might be possible to accelerate progress by the application of the powerful techniques evolved in recent years for studying atomically clean surfaces. However, the translation of ideas derived from clean single crystal surfaces with well characterized chemisorbed layers to real catalysts with high ratios of surface to mass on which reactions were taking place and requiring transport of mass and energy is a giant step, raising many questions and requiring thorough discussion by surface physicists on the one hand and catalytic chemists on the other. The 1974 Battelle Colloquium provided a forum for this exchange. As its usual custom, the Colloquium started the first day of introduc tory lectures by three distinguished scientists who have contributed impor tantly over many years to this field."