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Books > Science & Mathematics > Chemistry > Physical chemistry > Solid state chemistry
This book is a chemist's approach to the subject. Many concepts of solid state science have been explained in a simple lucid manner so that undergraduate students can read it independently. Some chapters have been rewritten for this edition and new chapters have been added. It is recommended to serve as a textbook for courses at both undergraduate and postgraduate levels.
This hands-on reference tool provides the most up-to-date information needed to synthesize molecules by solid-phase synthesis (SPS)-employing polymeric support (resins), anchoring linkages (handles), coupling reagents (activators), and protection schemes. The volume presents new strategies for creating a wide variety of compounds invaluable for drug discovery in coming years. Thoroughly analyzes peptides, DNA, carbohydrates, conjugates of biomolecules, and small molecules. Written by 35 internationally recognized authorities, Solid-Phase Synthesis provides experimental procedures and a literature review for peptides, DNA, PNA, carbohydrates, peptidomimetics, and small molecule assembly describes the preparation of solid supports and handles (linkers) as well as their appropriate incorporation into a synthetic strategy discusses methods for the construction of more complex peptides: cyclic (lactam and disulfide), glyco-, phospho-, sulfo- and nucleopeptides explains the protocols for the preparation of side-chain and N-alpha protecting groups for amino acids surveys the various coupling reagents and methods for peptide chain elongation considers convergent peptide synthesis (fragment condensations) examines engineering designs for automation details techniques for the purification and analysis of peptides and combination libraries and more Containing over 2400 references and more than 300 tables, drawings, and equations, Solid-Phase Synthesis is an eminently practical and quick-reference guide for organic, combinatorial, and medicinal chemists and biochemists; pharmacists, pharmacologists, and pharmaceutical researchers; molecular and cell biologists; enzymologists; immunologists; neurobiologists; and graduate and medical school students in these disciplines.
Basics of Polymer Chemistry is of great interest to the chemistry audience. The basic properties of polymers, including diverse fundamental and applied aspects, are presented. This book constitutes a basis for understanding polymerization, and it presents a comprehensive overview of the scientific research of polymers. The chapters presented can be used as a reference for those interested in understanding the sustainable development in polymers. Basics of Polymer Chemistry provides a balanced coverage of the key developments in this field, and highlights recent and emerging technical achievements. The topics covered present a comprehensive overview of the subject area and are therefore of interest to professors and students. The recent developments in polymerization using catalysts, homo and copolymerization are presented, and it contains current efforts in designing new polymer architectures. Improved property performance attributes of the polymers by controlling their molecular-structural characteristics such as molecular weight distribution, monomer type content distribution, and branching level are also discussed.
This volume focuses on the wealth of existing literature on physical metallurgy, and deals with materials in different states of order and the process of order evolution. It is a valuable reference by students and researchers in the field of materials science and metallurgy.
With a modern, comprehensive approach directed towards computational mechanics, this book covers a unique combination of subjects at present unavailable in any other text. It includes vital information on ‘variational principles’ constituting the cornerstone of the finite element method. In fact this is the only method by which Nonlinear Solid Mechanics is utilized in engineering practice. The book opens with a fundamental chapter on vectors and tensors. The following chapters are based on nonlinear continuum mechanics - an inevitable prerequisite for computational mechanicians. In addition, continuum field theory (applied to a representative sample of hyperelastic materials currently used in nonlinear computations such as incompressible and compressible materials) is presented, as are transversely isotropic materials, composite materials, viscoelastic materials and hyperelastic materials with isotropic damage. Another central chapter is devoted to the thermodynamics of materials, covering both finite thermoelasticity and finite thermoviscoelasticity. Also included are:
This extensive reference/text explores the principles,
instrumentation, processes, and programs of pharmaceutical solid
science as well as new aspects on one-component systems,
micromeritics, polymorphism, solid-state stability, cohesion,
powder flow, blending, single- unit sustained release, and tablet
coating.
Crystallisation, the spontaneous arrangement of molecular building blocks into ordered solid particles, is a fascinating phenomenon. Understanding the dynamic, molecular-scale processes that underlie crystal nucleation and growth holds the key to designing the production of specific crystalline materials The ability to induce crystallisation how, when and where we want it is key to material synthesis. Such capabilities will transform industrial and environmental sectors, including healthcare, formulated products, oil and gas, water, mining and advanced materials. This Discussion focuses on the following four themes: Understanding crystal nucleation mechanisms: where do we stand? Growing crystals by design Controlling polymorphism Learning Lessons from Nature - the future of biomimetics
Solid State Chemistry and its Applications, 2nd Edition: Student Edition is an extensive update and sequel to the bestselling textbook Basic Solid State Chemistry, the classic text for undergraduate teaching in solid state chemistry worldwide. Solid state chemistry lies at the heart of many significant scientific advances from recent decades, including the discovery of high-temperature superconductors, new forms of carbon and countless other developments in the synthesis, characterisation and applications of inorganic materials. Looking forward, solid state chemistry will be crucial for the development of new functional materials in areas such as energy, catalysis and electronic materials. This revised edition of Basic Solid State Chemistry has been completely rewritten and expanded to present an up-to-date account of the essential topics and recent developments in this exciting field of inorganic chemistry. Each section commences with a gentle introduction, covering basic principles, progressing seamlessly to a more advanced level in order to present a comprehensive overview of the subject. This new Student Edition includes the following updates and new features: * Expanded coverage of bonding in solids, including a new section on covalent bonding and more extensive treatment of metallic bonding. * Synthetic methods are covered extensively and new topics include microwave synthesis, combinatorial synthesis, mechano-synthesis, atomic layer deposition and spray pyrolysis. * Revised coverage of electrical, magnetic and optical properties, with additional material on semiconductors, giant and colossal magnetoresistance, multiferroics, LEDs, fibre optics and solar cells, lasers, graphene and quasicrystals. * Extended chapters on crystal defects and characterisation techniques. * Published in full colour to aid comprehension. * Extensive coverage of crystal structures for important families of inorganic solids is complemented by access to CrystalMaker(R) visualization software, allowing readers to view and rotate over 100 crystal structures in three dimensions. * Solutions to exercises and supplementary lecture material are available online. Solid State Chemistry and its Applications, 2nd Edition: Student Edition is a must-have textbook for any undergraduate or new research worker studying solid state chemistry.
The quest for efficient and durable battery technologies is one of the key challenges for enabling the transition to renewable energy economies. Magnesium batteries, and in particular rechargeable non-aqueous systems, are an area of extensive opportunity and intense research. Rechargeable magnesium batteries hold numerous advantages over current lithium-ion batteries, namely the relative abundance of magnesium to lithium and the potential for magnesium batteries to greatly outperform their Li-ion counterparts. Magnesium Batteries comprehensively outlines the scientific and technical challenges in the field, covering anodes, cathodes, electrolytes and particularly promising systems such as the Mg-S cell. Edited by a leading figure in the field of electrochemical energy storage, with contributions from global experts, this book is a vital resource for students and researchers at all levels. Whether entering into the subject for the first time or extending their knowledge of battery materials across chemistry, physics, energy, engineering and materials science this book provides an ideal reference for anyone interested in the state-of-the-art and future of magnesium batteries.
The second edition of a modern introduction to the chemistry and physics of solids. This textbook takes a unique integrated approach designed to appeal to both science and engineering students. "Review of 1st edition" "an extremely wide-ranging, useful book that is accessible to anyone with a firm grasp of high school science...this is an outstanding and affordable resource for the lifelong learner or current student." Choice, 2005 The book provides an introduction to the chemistry and physics of solids that acts as a foundation to courses in materials science, engineering, chemistry, and physics. It is equally accessible to both engineers and scientists, through its more scientific approach, whilst still covering the material essential to engineers. This edition contains new sections on the use of computing methods to solve materials problems and has been thoroughly updated to include the many developments and advances made in the past 10 years, e.g. batteries, solar cells, lighting technology, lasers, graphene and graphene electronics, carbon nanotubes, and the Fukashima nuclear disaster. The book is carefully structured into self-contained bite-sized chapters to enhance student understanding and questions have been designed to reinforce the concepts presented. The supplementary website includes Powerpoint slides and a host of additional problems and solutions.
"Introduction to Solid State NMR Spectroscopy" is written for
undergraduate and graduate students of chemistry, either taking a
course in advanced or solid-state nuclear magnetic resonance
spectroscopy or undertaking research projects where solid-state NMR
is likely to be a major investigative technique. It will also serve
as a practical introduction in industry, where the techniques can
provide new or complementary information to supplement other
investigative techniques.
By covering solid-state NMR spectroscopy in a clear,
straightforward and approachable way with detailed descriptions of
the major solid-state NMR experiments focussing on what the
experiments do and what they tell the researcher, this book will
serve as an ideal introduction to the subject. These descriptions
are backed up by separate mathematical explanations for those who
wish to gain a more sophisticated quantitative understanding of the
phenomena. With additional coverage of the practical implementation
of solid-state NMR experiments integrated into the discussion, this
book will be essential reading for all those using, or about to
use, solid-state NMR spectroscopy.
Dr Melinda Duer is a senior lecturer in the Department of Chemistry at the University of Cambridge, Cambridge, UK.
Ultrafast science has long been limited to the investigation of molecular processes. Over the past 10 years investigation of ultrafast processes has expanded to material science, including aspects relevant to the solid-state such as excitation of electrons in band structures and collective phonon excitation. Specific probes for electronic and structural reorganization, such as X-ray diffraction and ARPES, have been advanced. Furthermore, experimental techniques including XFEL science, THz science and various pump-probe methods, as well as the theoretical understanding of ultrafast, out-of-equilibrium and multiscale processes driven by light or THz excitation, have seen rapid development. This volume brings together a complementarity of internationally-leading experimental material scientists and theoreticians in this field to explore and exchange their ideas about the key aspects of ultrafast science, designing new ways to control materials and understanding transformation processes. The topics covered include: Material science: ultrafast transformation, electron-phonon coupling, multi-scale aspects Theory of out of equilibrium light-induced phenomena Optical excitation processes THz and laser field excitation processes
The second edition of a modern introduction to the chemistry and physics of solids. This textbook takes a unique integrated approach designed to appeal to both science and engineering students. "Review of 1st edition" "an extremely wide-ranging, useful book that is accessible to anyone with a firm grasp of high school science...this is an outstanding and affordable resource for the lifelong learner or current student." Choice, 2005 The book provides an introduction to the chemistry and physics of solids that acts as a foundation to courses in materials science, engineering, chemistry, and physics. It is equally accessible to both engineers and scientists, through its more scientific approach, whilst still covering the material essential to engineers. This edition contains new sections on the use of computing methods to solve materials problems and has been thoroughly updated to include the many developments and advances made in the past 10 years, e.g. batteries, solar cells, lighting technology, lasers, graphene and graphene electronics, carbon nanotubes, and the Fukashima nuclear disaster. The book is carefully structured into self-contained bite-sized chapters to enhance student understanding and questions have been designed to reinforce the concepts presented. The supplementary website includes Powerpoint slides and a host of additional problems and solutions.
A thorough exploration of the atomic structures and properties of the essential engineering interfaces—an invaluable resource for students, teachers, and professionals The most up-to-date, accessible guide to solid-vapor, solid-liquid, and solid-solid phase transformations, this innovative book contains the only unified treatment of these three central engineering interfaces. Employing a simple nearest-neighbor broken-bond model, Interfaces in Materials focuses on metal alloys in a straightforward approach that can be easily extended to all types of interfaces and materials. Enhanced with nearly 300 illustrations, along with extensive references and suggestions for further reading, this book provides:
Spanning the fields of chemical, electrical and computer engineering, materials science, solid-state physics, and microscopy, Interfaces in Materials bridges a major gap in the literature of surface and interface science.
Praise for the First Edition: "Very useful for researchers in solid-state chemistry and as a textbook of advanced inorganic chemistry for PhD students." —Advanced Materials. This book provides unified coverage of the structure, properties, and synthesis of transition metal oxides. Written by two world-class scientists, it offers both an excellent window on modern solid-state chemistry and a gateway to understanding the behavior of inorganic solids. Scientists and advanced students in inorganic and solid-state chemistry, materials science, ceramics, and condensed matter science will welcome this updated Second Edition, which features new or expanded material on:
Plus:
Chemistry has a vital role to play in materials processing and in the development of new materials that can meet the changing needs of today's technology. This volume addresses both the basic underlying principles and the technological relevance of major topics in advanced materials chemistry, including:
Bringing together a battery of important information in a single source, this stand-alone reference is an invaluable companion for aspiring and practicing organic, inorganic, solid-state, and surface chemists, as well as polymer and materials scientists.
Used in materials science, physical chemistry and physics, density functional methods provide a unifying description of electronic properties applicable to all materials while also giving specific information on the system under study. A large number of very different materials and systems (atoms, molecules, macromolecules, clusters, bulk solids, surfaces and interfaces) are presently being studied with methods based on density functional formalism. Density Functional Methods in Chemistry and Materials Science reports the results of this research. This book will be of particular interest to those research materials science from a theoretical standpoint. This work will demonstrate how the formalism has become a methodology leading to useful information on structural and electronic properties of a broad range of materials.
Discover the exciting, promising field of molecular level
artificial photosynthesis
Chemical kinetics in solids are often dependent on numerous factors, and it's important for researchers to understand both the interactions relating to these factors, and how their own procedural choices may influence outcomes. Kinetics of Processes in the Solid State provides an authoritative overview of reactions in solids and helps readers quickly and easily identify the kinetic processes at play in their own work. Beginning with an introduction to the nature of solids and transformations, the book goes on to outline rate laws and experimental techniques, followed by such key areas as nucleation, phase transformations and crystallization. Chapters on the kinetics of dehydration, decomposition and polymers follow, before the book concludes by reviewing kinetics in relation to some important applications. Drawing on the experience of its expert author, Kinetics of Processes in the Solid State is a practical introduction to the field for chemists and researchers whose work is directly related to these interactions, and additionally for all those in related fields whose work would be enhanced by an understanding of these processes.
Solid Phase Microextraction: Theory and Practice Janusz Pawliszyn Solid phase microextraction (SPME) is a recently proposed solvent-free sampling and sample preparation technique. SPME represents a quick, sensitive, and economical approach that can be adopted for field work and can be easily integrated with present analytical instrumentation into an automation process. Written by the inventor of the technique, Solid Phase Microextraction: Theory and Practice describes the theoretical and practical aspects of this new technology, which received an "R&D 100" Award in 1994 recognizing its invention as a major advancement in the analytical sciences. Solid Phase Microextraction: Theory and Practice, the first book on SPME, offers the reader:
The time has come for an assessment of the most important
techniques for the fabrication of advanced catalysts. Catalyst
production alone is more than a billion dollar business each year,
and the product value of chemical processes using advanced
catalysts is a few trillion dollars annually. This book seeks to
provide a modern, materials science account of the best and most
current techniques for the synthesis of advanced catalytic
materials.
Adsorption: Fundamental Processes and Applications, Volume 33 in the Interface Science and Technology Series, discusses the great technological importance of adsorption and describes how adsorbents are used on a large scale as desiccants, catalysts, catalyst supports, in the separation of gases, the purification of liquids, pollution control, and in respiratory protection. Finally, it explores how adsorption phenomena play a vital role in many solid-state reactions and biological mechanisms, as well as stressing the importance of the widespread use of adsorption techniques in the characterization of surface properties and the texture of fine powders.
The Physics and Chemistry of Solids is one of the first textbooks to discuss the physics, chemistry and materials aspects of solids from a unified viewpoint. Coverage includes both fundamental principles along with the very latest developments, such as combinatorial library synthesis, mesoporous materials, fullerenes and nanotubules, optical localization and the experimental observation of fractional electronic charge. Lucidly written and richly illustrated, this book will appeal to physicists, chemists, material scientists and engineers studying the solid state. The Physics and Chemistry of Solids features:
…this is an excellent book. Dr Paul Monk, Manchester Metropolitan University. There has been a real need for a text to cover this area. I must admit my deepest admiration for the way the author has put the text together. Dr Mike Morris, University College Cork. …this promises to be an excellent text. Dr Anthony Powell, Heriot-Watt University.
This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of the material within each chapter. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. The basic techniques that all chapters rely on are collected into a second chapter to avoid unnecessary repetition later. Remaining chapters in the "Fundamentals" part deal with the major areas of solid-state NMR which all solid-state NMR spectroscopists should know about. Each begins with an overview of the topic that puts the chapter in context. The basic principles upon which the techniques in the chapter rely are explained in a separate section. Each of these chapters exemplifies the principles and techniques with the applications most commonly found in current practice. The "Further Applications" section contains a series of shorter chapters which describe the NMR techniques used in other, more specific areas. The basic principles upon which these techniques rely will be expounded only if not already in the Fundamentals part.
Nanocomposite Structures and Dispersions deals with the preparation of gelled, branched and crosslinked nanostructured polymers in the solution free radical polymerization and controlled/living radical polymerization and polymer and composite nanoparticles and nanostructures in disperse systems, the kinetics of direct and inverse disperse polymerizations (microemulsion, miniemulsion, emulsion, dispersion and suspension polymerization), the bottom-up approach building of functionalized nanoparticles, modelling of radical microemulsion polymerization, the characterization of traditional and non-traditional polymer dispersions, the collective properties of nanomaterials and their (bio)applications. This book is designed to bridge that gap and offers several unique features. First, it is written as an introduction to and survey of nanomaterials with a careful balance between basics and advanced topics. Thus, it is suitable for both beginners and experts, including graduate and upper-level undergraduate students. Second, it strives to balance the colloidal aspects of nanomaterials with physical principles. Third, the book highlights nanomaterial based architectures including composite or hybrid conjugates rather than only isolated nanoparticles. A number of ligands have been utilized to biodecorate the polymer and composite nanocarriers. Finally, the book provides an in depth discussion of important examples of reaction mechanisms of bottom-up building of functionalized nanoparticles, or potential applications of nanoarchitectures, ranging from physical to chemical and biological systems. |
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