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Books > Science & Mathematics > Chemistry > Analytical chemistry
This volume is devoted to the physics, instrumentation and analytical methods of secondary ion mass spectroscopy (SIMS) in relation to solid surfaces. It describes modern models of secondary ion formation and the factors influencing sensitivity of measurements and the range of applications. All the main parts of SIMS instruments are discussed in detail. Emphasising practical applications the book also considers the methods and analytical procedures for constitutional analysis of solids --- including metals, semiconductors, organic and biological samples. Methods of depth profiling, spatially multidimensional analysis and study of processes at the surface, such as adsorption, catalysis and oxidation, are given along with the application of SIMS in combination with other methods of surface analysis.
The book describes the theoretical principles of nonstatistical methods of data analysis but without going deep into complex mathematics. The emphasis is laid on presentation of solved examples of real data either from authors' laboratories or from open literature. The examples cover wide range of applications such as quality assurance and quality control, critical analysis of experimental data, comparison of data samples from various sources, robust linear and nonlinear regression as well as various tasks from financial analysis. The examples are useful primarily for chemical engineers including analytical/quality laboratories in industry, designers of chemical and biological processes. Features: Exclusive title on Mathematical Gnostics with multidisciplinary applications, and specific focus on chemical engineering. Clarifies the role of data space metrics including the right way of aggregation of uncertain data. Brings a new look on the data probability, information, entropy and thermodynamics of data uncertainty. Enables design of probability distributions for all real data samples including smaller ones. Includes data for examples with solutions with exercises in R or Python. The book is aimed for Senior Undergraduate Students, Researchers, and Professionals in Chemical/Process Engineering, Engineering Physics, Stats, Mathematics, Materials, Geotechnical, Civil Engineering, Mining, Sales, Marketing and Service, and Finance.
This title includes a number of Open Access chapters. This collection presents a broad selection of recent research on analytical chemistry, including methods of determination and analysis as applied to plants, pharmaceuticals, foods, proteins, and more. Analytical chemistry is the study of what chemicals are present and in what amount in natural and artificial materials. Because these understandings are fundamental in just about every chemical inquiry, analytical chemistry is used to obtain information, ensure safety, and solve problems in many different chemical areas, and is essential in both theoretical and applied chemistry. Analytical chemistry is driven by new and improved instrumentation.
In recent years the availability of techniques and the asking of basic and technological questions has led to an international explosion of activity in the study of solid surfaces. Originally published in Reports in Progress in Physics, Electronic Properties of Surfaces reflects the modern knowledge in this field, presenting critical appraisals of progress in surface science. The book should be particularly valuable for researchers new to this field.
This book covers the progress of the last 10 years of studies on cocoa butter. Descriptions of several aspects, including physical characteristics such as rheology, hardness, melt profiles, etc., studied by new and advanced techniques are included. Similarly, the polymorphism of cocoa butter is reconsidered in light of studies done by synchrotron DSC, FTIR, and SAXS techniques. These data are complemented by new understandings on the cause of the crystallization and transitions of the polymorphs. Other aspects such as the effect of minor components, emulsifiers, and other fats are discussed in great detail in this book.
Focusing on the organic inventory of regions of star and planet formation in the interstellar medium of galaxies, this comprehensive overview of the molecular universe is an invaluable reference source for advanced undergraduates through to entry-level researchers. It includes an extensive discussion of microscopic physical and chemical processes in the universe; these play a role in the excitation, spectral characteristics, formation, and evolution of molecules in the gas phase and on grain surfaces. In addition, the latest developments in this area of molecular astrophysics provide a firm foundation for an in-depth understanding of the molecular phases of the interstellar medium. The physical and chemical properties of gaseous molecules, mixed molecular ices, and large polycyclic aromatic hydrocarbon molecules and fullerenes and their role in the interstellar medium are highlighted. For those with an interest in the molecular universe, this advanced textbook bridges the gap between molecular physics, astronomy, and physical chemistry.
This book provides up-to-date discussion of modern polarographic methods, with examples and experimental details. It is designed for the practicing analyst and a factor in bringing the reincarnated area of analytical chemistry into a new and healthy maturity.
Provides clear instructions and step-by-step exercises to make learning the material easier for students. Emphasizes fundamental laboratory skills which prepare a student for the industry. Builds students' skills through an organized and systematic presentation of materials, procedures, and tasks. Updates reflect recent innovations and regulatory requirements to ensure students stay up to date. Supplies skills suitable for careers in forensic, clinical, quality control, environmental, and other testing laboratories.
The book gives an overview about all relevant electrochemical and spectroscopic methods used in corrosion research. Besides the correct use and interpretation, the methods are correlated with industrial test methods for organic coatings and conversion layers.
This volume is an essential handbook for anyone interested in performing the most accurate spectrophotometric or other optical property of materials measurements. The chapter authors were chosen from the leading experts in their respective fields and provide their wisdom and experience in measurements of reflectance, transmittance, absorptance, emittance, diffuse scattering, color, and fluorescence. The book provides the reader with the theoretical underpinning to the methods, the practical issues encountered in real measurements, and numerous examples of important applications. Written by the leading international experts from industry, government, and academiaWritten as a handbook, with in depth discussion of the topicsFocus on making the most accurate and reproducible measurementsMany practical applications and examples
This informative book offers a wide range of knowledge on the technologies and applications of the cutting-edge field of high-resolution mass spectrometry (HRMS) in different areas of analysis. HRMS has changed the nature of experimentation and investigation in so many analytical realms. Determining exact mass determination, high resolution, and specificity-via the special features provided by HRMS instruments-is now possible for determining the composition of the analyte of interest, both qualitatively and quantitatively. High-Resolution Mass Spectrometry and Its Diverse Applications: Cutting-Edge Techniques and Instrumentation begins with an overview of the basic instrumentation techniques and goes on to present research on diverse new uses of HRMS in clinical testing, such as for therapeutic drug designing, discovery, and development; in forensic studies and investigations; in quality management systems; for analysis of pesticides; for analysis of single cells; in analysis of fossil fuels; for use in space and planetary science; and more. Chapters relay how HRMS plays an important role in the structure elucidation and unknown determination in many fields and is a great measure to be used for quantitative analyses. The book considers how these properties make the technique a strong aid in many areas. This volume highlights how HRMS can be a useful tool for scientists and researchers, faculty and students, and industry professionals in many scientific areas of study.
The second edition of "Internal Photoemission Spectroscopy" thoroughly updates this vital, practical guide to internal photoemission (IPE) phenomena and measurements. The book's discussion of fundamental physical and technical aspects of IPE spectroscopic applications is supplemented by an extended overview of recent experimental results in swiftly advancing research fields. These include the development of insulating materials for advanced SiMOS technology, metal gate materials, development of heterostructures based on high-mobility semiconductors, and more. Recent results concerning the band structure of important interfaces in novel materials are covered as well. Internal photoemission involves the physics of charge carrier
photoemission from one solid to another, and different
spectroscopic applications of this phenomenon to solid state
heterojunctions. This technique complements conventional external
photoemission spectroscopy by analyzing interfaces separated from
the sample surface by a layer of a different solid or liquid.
Internal photoemission provides the most straightforward, reliable
information regarding the energy spectrum of electron states at
interfaces. At the same time, the method enables the analysis of
heterostructures relevant to modern micro- and nano-electronic
devices as well as new materials involved in their design and
fabrication.
The present work is an introductory text in statistics, addressed to researchers and students in the field of material science. It aims to give the readers basic knowledge on how statistical reasoning is exploitable in this field, improving their knowledge of statistical tools and helping them to carry out statistical analyses and to interpret the results. It also focuses on establishing a consistent multivariate workflow starting from a correct design of experiment followed by a multivariate analysis process.
This volume will capture transformational changes in both the chemistry and engineering side of solvent extraction, creating new directions and deepening our understanding of the structure and dynamics of liquid-liquid systems from the molecular- to nano- to meso- to bulk-scale. Reviews will cover advances in microfluidics, new tools for understanding the structure and dynamics of the liquid-liquid interface, ionic liquids in liquid-liquid extraction, molecular dynamics to visualize interactions in the solvent phase, liquid-liquid electrochemistry to interrogate the energetics of interfacial transport and complexation, design of new extractants, and the streamlining of process applications.
This title provides comprehensive coverage of modern gas
chromatography including theory, instrumentation, columns, and
applications addressing the needs of advanced students and
professional scientists in industry and government laboratories.
Chapters are written by recognized experts on each topic. Each
chapter offers a complete picture with respect to its topic so
researchers can move straight to the information they need without
reading through a lot of background information.
Nuclear magnetic resonance (NMR) is an analytical tool used by
chemists and physicists to study the structure and dynamics of
molecules. In recent years, no other technique has gained such
significance as NMR spectroscopy. It is used in all branches of
science in which precise structural determination is required and
in which the nature of interactions and reactions in solution is
being studied. "Annual Reports on NMR Spectroscopy" has established
itself as a premier means for the specialist and non-specialist
alike to become familiar with new techniques and applications of
NMR spectroscopy. Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. "Annual Reports on NMR Spectroscopy" has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.
A classic in the area of organic synthesis, " Strategies and
Tactics in Organic Synthesis" provides a forum for investigators to
discuss their approach to the science and art of organic synthesis.
Rather than a simple presentation of data or a second-hand
analysis, this book vividly demonstrates through first hand
accounts how synthesis is really done and how by discovering new
reactions, creating new designs and building molecules with atom
and step economies, the advancement of the science of organic
synthesis is providing solutions through function to create a
better world.
Biomedical Applications of Magnetic Particles discusses fundamental magnetic nanoparticle physics and chemistry and explores important biomedical applications and future challenges. The first section presents the fundamentals of the field by explaining the theory of magnetism, describing techniques to synthesize magnetic particles, detailing methods to characterize magnetic particles, and quantitatively describing the applied magnetic forces, torques, and the resultant particle motions. The second section describes the wide range of biomedical applications, including chemical sensors, cellular actuators, drug delivery, magnetic hyperthermia, magnetic resonance imaging contrast enhancement, and toxicity. Additional key features include: Covers both introduction to physics and characterization of magnetic nanoparticles and the state of the art in biomedical applications Authoritative reference for scientists and engineers for all new or old to the field Describes how the size of magnetic nanoparticles affects their magnetic properties, colloidal properties, and biological properties. Written by a team of internationally respected experts, this book provides an up-to-date authoritative reference for scientists and engineers.
High-Throughput Mass Spectrometry in Drug Discovery Apply mass spectrometry to every phase of new drug discovery with this cutting-edge guide Mass spectrometry is a technique that identifies and characterizes compounds based on their mass — the fundamental molecular characteristic. It has become an invaluable analytical tool in various disciplines, industries, and research fields. It has become particularly central to new drug discovery and development, which broadly deploys mass spectrometry at every phase. The pharmaceutical industry has become one of the main drivers of technological development in mass spectrometry. High-Throughput Mass Spectrometry in Drug Discovery offers a comprehensive introduction to mass spectrometry and its applications in pharmaceutical discovery. It covers the foundational principles and science of mass spectrometry before moving to specific experimental methods and their applications at various stages of drug discovery. Its thorough treatment and detailed guidance make it an invaluable tool for pharmaceutical research and development. High-Throughput Mass Spectrometry in Drug Discovery readers will also find: Detailed analysis of techniques, including label-free screening, synthetic reaction optimization, and more An authorial team with extensive combined experience in research and industrial applications Technical strategies with the potential to accelerate quantitative bioanalysis in drug discovery High-Throughput Mass Spectrometry in Drug Discovery is essential for analytical, bioanalytical, and medicinal chemists working in the pharmaceutical industry and for any researchers and graduate students interested in drug discovery and development.
The presence of concentrations of organic substances and cations in sea water is a matter of increasing concern to the water industry, environmentalists and the general public alike. There is a threat of possible health hazards to both human, fish and crustacea. Occurrence, Toxicity and Analysis of Marine Biota discusses bioaccumulation in biota as well as occurrence and analysis of toxicants in biota. The main thrust of this book will be a review of the levels of toxicants found in the tissues of fish and invertebrates at various sites throughout the world. In addition, results will be reported on the levels of toxicants found in marine biota enabling ill health or death to occur. This will involve a discussion of toxicity index LC50 and percentile S95 concentration of toxicants and their implications on animal health and mortality, also that of humans who eat these sea creatures. The book will be a complete logical survey of this topic.
This book addresses how to estimate substance use and thereby evaluate policies intended to reduce the harms caused by drugs and other substances. Wastewater analysis (WWA) can provide efficient, affordable, fine-grained and objective data on population substance use trends on a very large scale. The authors discuss the potential implications of WWA as a new method for understanding substance use in a variety of settings and ignite a discourse with policy makers, criminologists, epidemiologists and other disciplines about the need for collaboration with WWA scientists. The book also features an explanation of the costs and harms of substance use with academic literature from criminological and epidemiological sources and reports from lead agencies. Additional features include: Details on the origin of wastewater analysis in environmental science Description of analytical chemistry methods for tracing a wide variety of substances, including illicit drugs, alcohol, tobacco and other chemicals Exploration of the major empirical problems in estimating population consumption of alcohol, tobacco and drugs at the international and national level Examination of the principles of human research ethics and their application to wastewater analysis Wastewater Analysis for Substance Abuse Monitoring and Policy Development is a valuable tool for analytical chemists, wastewater scientists and criminologists, as well as researchers and policy makers across disciplines who work in drug sectors.
The Springer Handbook of Odor is the definitive guide to all aspects related to the study of smell and their impact on human life. For the first time, this handbook aligns the senso-chemo-analytical characterization of everyday smells encountered by mankind, with the elucidation of perceptual, hedonic, behavioral and physiological responses of humans to such odors. From birth onwards we learn to interact with our environment using our sense of smell. Moreover, evolutionary processes have engendered a multi-faceted communication that is supported - even dominated - by olfaction. This compilation examines the responses of humans to odors at different stages of life, thereby building a foundation for a widely overseen area of research with broader ramifications for human life. The expert international authors and editor align aspects, concepts, methodologies and perspectives from a broad range of different disciplines related to the science of smell. These include chemistry, physiology, psychology, material sciences, technology but also disciplines related to linguistics, culture, art and design. This handbook, edited by an internationally renowned aroma scientist with the support of an outstanding team of over 60 authors, is an authoritative reference for researchers in the field of odors both in academia and in industry and is also a useful reference for newcomers to the area.
The book covers the fundamental concepts of phases, phase diagrams and their applications. Stress is on understanding and not on memorization. The book has descriptive passages and diagrams (cooling curves) that help students gain a solid foundation in subject. This text will help them learn phase rule faster. It also contains numerous phase diagrams. Note: T& F does not sell or distribute the Hardback in India, Pakistan, Nepal, Bhutan, Bangladesh and Sri Lanka.
Researchers in chemistry, chemical engineering, pharmaceutical science, forensics, and environmental science make routine use of chemical analysis, but the information these researchers need is often scattered in different sources and difficult to access. The CRC Handbook of Basic Tables for Chemical Analysis: Data-Driven Methods and Interpretation, Fourth Edition is a one-stop reference that presents updated data in a handy format specifically designed for use when reaching a decision point in designing an analysis or interpreting results. This new edition offers expanded coverage of calibration and uncertainty, and continues to include the critical information scientists rely on to perform accurate analysis. Enhancements to the Fourth Edition: Compiles a huge array of useful and important data into a single, convenient source Explanatory text provides context for data and guidelines on applications Coalesces information from several different fields Provides information on the most useful "wet" chemistry methods as well as instrumental techniques, with an expanded discussion of laboratory safety Contains information of historical importance necessary to interpret the literature and understand current methodology. Unmatched in its coverage of the range of information scientists need in the lab, this resource will be referred to again and again by practitioners who need quick, easy access to the data that forms the basis for experimentation and analysis.
Laboratory Experiments in Trace Environmental Quantitative Analysis is a collection of student-tested experiments that introduce important principles that underlie various laboratory techniques in the field of trace environmental organics and inorganics quantitative analysis. It crosses the more traditional academic disciplines of environmental science and analytical chemistry. The text is organized to begin with minimally rigorous session/experiments and increase in rigor as each session/experiment unfolds. Each experiment features learning objectives, expected student outcomes, and suggestions for further study. Additional features include: Students are introduced to the principles and laboratory practice of instrumental analysis (determinative techniques) that are clearly presented. Students are carefully taken through various ways to prepare samples for trace quantitative analysis (sample prep techniques). Safety warnings are listed within each experiment. Students are introduced to all three types of instrument calibration: external, internal and standard addition. Instructors who are responsible for laboratory courses in analytical chemistry with potential application to environmental sample matrices will find this textbook of value. Graduate programs in environmental science and engineering will also greatly benefit from the content. |
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