Annual Reports on NMR Spectroscopy, Volume 107, the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy, includes a variety of updated chapters covering NMR Diffusion Studies, Recent Advances in Understanding of Nucleus Contributions to NMR Nuclear Shieldings, and more.

Carbon Nanomaterials-Based Sensors: Emerging Research Trends in Devices and Applications covers the most recent research and design trends for carbon nanomaterials-based sensors for a variety of applications, including clinical and environmental uses, and more. Carbon nanomaterials-based sensors can be used with high sensitivity, stability and accuracy compared to other techniques. Written by experts in their given fields from around the world, this book helps researchers solve the particular challenges they face when developing new types of sensors. It instructs how to make sensitive, selective, robust, fast-response and stable carbon nanomaterial-based sensors, as well as how to utilize them in real life.

Scaling Up of Microbial Electrochemical Systems: From Reality to Scalability is the first book of its kind to focus on scaling up of microbial electrochemical systems (MES) and the unique challenges faced when moving towards practical applications using this technology. This book emphasizes an understanding of the current limitations of MES technology and suggests a way forward towards onsite applications of MES for practical use. It includes the basics of MES as well as success stories and case studies of MES in the direction of practical applications. This book will give a new direction to energy researchers, scientists and policymakers working on field applications of microbial electrochemical systems-microbial fuel cells, microbial electrolysis cells, microbial electrosynthesis cells, and more.

Essentials in Modern HPLC Separations, Second Edition discusses the role of separation in high performance liquid chromatography (HPLC). This new and updated edition systematically presents basic concepts as well as new developments in HPLC. Starting with a description of basic concepts, it provides important guidance for the practical utilization of various HPLC procedures, such as the selection of the HPLC type, proper choice of the chromatographic column, selection of mobile phase and selection of the method of detection, all of which are in correlation with the physico-chemical characteristics of the compounds separated. Every chapter has been carefully reviewed, with several new sections added to bring the book completely up-to-date. Hence, it is a valuable reference for students and professors in chemistry.

Wearable Physical, Chemical and Biological Sensors introduces readers of all backgrounds-chemistry, electronics, photonics, biology, microfluidics, materials, and more-to the fundamental principles needed to develop wearable sensors for a host of different applications. The capability to continuously monitor organ-related biomarkers, environmental exposure, movement disorders, and other health conditions using miniaturized devices that operate in real time provides numerous benefits, such as avoiding or delaying the onset of disease, saving resources allocated to public health, and making better decisions on medical diagnostics or treatment. Worn like glasses, masks, wristwatches, fitness bands, tattoo-like devices, or patches, wearables are being boosted by the Internet of Things in combination with smart mobile devices. Besides, wearables for smart agriculture are also covered. Written by experts in their respective fields, Wearable Physical, Chemical and Biological Sensors provides insights on how to design, fabricate, and operate these sensors.

SERS for Point-of-care and Clinical Applications focuses on the use of Surface-Enhanced Raman Spectroscopy (also known as Surface-Enhanced Raman Scattering) techniques in clinical and point-of-care settings. Sections provide an overview of SERS biomedical applications, providing in-depth information about point-of-care and clinical applications of SERS using specific examples from current literature. These applications are not always immediately evident to newcomers in the field, as Raman and SERS are often introduced as analytical methods for chemical analysis. This book offers a concise introduction to the biomedical applications of SERS for graduate students, scientists and researchers in all related fields.

Particle Separation Techniques: Fundamentals, Instrumentation, and Selected Applications presents the latest research in the field of particle separation methods. This edited book authored by subject specialists is logically organized in sections, grouping the separation techniques according to their preparative or analytical purposes and the particle type. Along with the traditional and classical separation methods suitable for micronic particles, an update survey of techniques appropriate for nanoparticle characterization is presented. This book fills the gap in the literature of particle suspension analysis of a synthetic but comprehensive manual, helping the reader to identify and apply selected techniques. It provides an overview of the techniques available to a reader who is not an expert on particle separation yet about to enter the field, design an experiment, or buy an instrument for his/her new lab.

ICP-MS and Trace Element Analysis as Tools for Better Understanding Medical Conditions, Volume 97 discusses trace elements and how they play an important role in biological functions and metabolism in the human body. Chapters cover Biomedical analysis by ICP-MS: A focus on single cell, Advanced statistical tools and machine learning applied to trace element analysis associated with medical conditions, ICP-MS as a tool to understand trace element homeostasis in neurological disorders, High-precision isotopic analysis of essential mineral elements - possibilities for medical diagnosis and prognosis, Exploring ICP-MS as a versatile technique: From imaging to chemical speciation, and more.

Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation-and limitations-of applying vapor generation techniques to everyday analytical problems facing the trace element analyst.

Annual Reports on NMR Spectroscopy, Volume 106 highlights new advances in the field, with this new volume presenting interesting chapters. Each chapter is written by an international board of authors.

Annual Reports on NMR Spectroscopy, Volume 105, the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy includes a variety of updated chapters covering Recent advances in dynamic nuclear polarization-enhanced NMR spectroscopy for organic polymers and Functional and structural characterization of membrane-binding proteins using NMR.

Separations of Water Pollutants with Nanotechnology, the latest volume in the Separation Science and Technology series, offers new solutions for remediating water pollution utilizing nanomaterials with separation methods. Current water purification methods are unsuitable, inconvenient or expensive, so there is a need for new and better processes and techniques. Nanomaterials can purify water by removing pollutants such as heavy metals, pathogens, organic compounds, inorganic compounds, pharmaceuticals, and chemicals of emerging concern. These can effectively replace membrane-based methods if the right expertise is developed-this book helps separation scientists do just that. Existing water treatment problems can be solved by applying a nanotechnology-based processes: antimicrobial nanotechnology, zero-valent iron nanoparticles, nanoadsorbents, nano-enhanced membranes, nanometal oxides, and nano photocatalysts. The current literature places emphasis on materials chemistry rather than the separation methods used for water purification. This new volume presents a collection of chapters that deal with remediation based on separation chemistry.

UV-Visible Spectrophotometry of Waters and Soils, Third Edition presents the latest information on the use of UV spectrophotometry for environmental quality monitoring. Using practical examples, the book illustrates how this technique can be a source of new methods of characterization and measurement. Easy and fast to run, this simple and robust analytical technique is one of the best ways to obtain a quantitative estimation of specific or aggregate parameters (e.g., Nitrate, TOC) and simultaneously qualitative information on the global composition of waters and soils. This third edition presents current methods and applications for water quality monitoring, including recent works and developments. Writing from years of experience in the development and applications of UV systems and from scientific and technical works, the book's authors provide several useful examples that show the great interest of UV spectrophotometry for water and soil monitoring. At the end of the book, the UV spectra library of previous editions is updated with new chemicals of interest.

Heteropolyacids as Highly Efficient and Green Catalysts Applied in Organic Transformations introduces heteropolyacids (HPAs) as promising candidates for use as green catalysts. This book initially presents an overview of chemistry of HPAs, including the history of their discovery and applications, systematic classifications, solubility, coordination and binding chemistry, isomerization, stability, redox activity, acidic properties, basicity, skeleton structure, structure types, self-assemblage, surface area, electrochemical behavior, methods of investigation, and characterization. Other sections present and compare the applications of HPAs as homogeneous and heterogeneous catalysts. The book provides readers with a basic-to-advanced range of knowledge on how useful and green HPAs can be used for use as catalysts in organic transformations and even the synthesis of complex organic molecules.

Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents.

Functionalized Nanomaterial-Based Electrochemical Sensors: Principles, Fabrication Methods, and Applications provides a comprehensive overview of materials, functionalized interfaces, fabrication strategies and application areas. Special attention is given to the remaining challenges and opportunities for commercial realization of functionalized nanomaterial-based electrochemical sensors. An assortment of nanomaterials has been investigated for their incorporation into electrochemical sensors. For example, carbon- based nanomaterials (carbon nanotube, graphene and carbon fiber), noble metals (Au, Ag and Pt), polymers (nafion, polypyrrole) and non-noble metal oxides (Fe2O3, NiO, and Co3O4). The most relevant materials are discussed in the book with an emphasis on their evaluation of their realization in commercial applications. Application areas touched on include the environment, food and medicine industries. Health, safety and regulation considerations are touched on, along with economic and commercialization trends.

The volume has as primary focus multidimensional gas chromatography (heart-cutting systems, comprehensive 2D-GC systems and hybrid solutions) and its characteristic features for in depth investigation of complex fractions of odor-active volatiles. Contributions, from outstanding researchers in the field from Academia and industry, cover fundamentals aspects on the physiology of olfaction, the strategies to identify key-odorants from the bulk of detectable volatiles (sensomics), the principles of operation of multidimensional analytical platforms (i.e., comprehensive two-dimensional gas chromatography - GCxGC; heart-cut 2D-GC, hybrid systems), and the fundamental role of mass spectrometry in providing reliable and informative data. Insights on new systems design and configurations are also provided, including sample preparation and data processing strategies, as important steps of the whole analytical process. Real-world examples cover food volatiles, complex aroma mixtures, odors emitted from industrial plants, volatiles of interest in forensic and medical applications.

Chemometrics in Spectroscopy, Revised Second Edition provides the reader with the methodology crucial to apply chemometrics to real world data. The book allows scientists using spectroscopic instruments to find explanations and solutions to their problems when they are confronted with unexpected and unexplained results. Unlike other books on these topics, it explains the root causes of the phenomena that lead to these results. While books on NIR spectroscopy sometimes cover basic chemometrics, they do not mention many of the advanced topics this book discusses. This revised second edition has been expanded with 50% more content on advances in the field that have occurred in the last 10 years, including calibration transfer, units of measure in spectroscopy, principal components, clinical data reporting, classical least squares, regression models, spectral transfer, and more.

Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the "what and why" that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more.

Counterterrorist Detection Techniques of Explosives, Second Edition covers the most current techniques available for explosive detection. This completely revised volume describes the most updated research findings that will be used in the next generation of explosives detection technologies. New editors Drs. Avi Cagan and Jimmie Oxley have assembled in one volume a series of detection technologies written by an expert group of scientists. The book helps researchers to compare the advantages and disadvantages of all available methods in detecting explosives and, in effect, allows them to choose the correct instrumental screening technology according to the nature of the sample.

Special Distillation Processes, Second Edition focuses on the latest developments in the field, such as separation methods that may prove useful for solving problems encountered during research. Topics include extraction, membrane and adsorption distillation involving the separation principle, process design and experimental techniques. The relationship between processes and techniques are also presented. Comprehensive and easy-to-read, this book provides key information needed to understand processes. It will be a valuable reference source for chemical engineers and students wishing to branch out in chemical engineering.

CAC series highlights new advances in the field. This Volume 94 presents interesting chapters on the recent advances in the role of nanoparticles in plant biotechnology. Each chapter is written by international experts in the respective fields.

Smartphone usage has created a new means for detection, analysis, diagnosis and monitoring through the use of new apps and attachments. These breakthrough analytical methods offer ways to overcome the drawbacks of more conventional methods, such as the expensive instrumentation that is often needed, complex sample pre-treatment steps, or time-consuming procedures. Smartphone-Based Detection Devices: Emerging Trends in Analytical Techniques gathers these modern developments in smartphone analytical methods into one comprehensive source, covering recent advancements in analytical tools while paying special attention to the most accurate, highly efficient approaches. Serving as a guide not only to analytical chemists but also to environmentalists, biotechnologists, pharmacists, forensic scientists and toxicologists, Smartphone-Based Detection Devices: Emerging Trends in Analytical Techniques is an important source for researchers who require accurate analysis of their on- and off-site samples. Students in these fields at the graduate and post-graduate level will also benefit from this topical and comprehensive book.

Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an authoritative overview of theoretical knowledge and practical applications across several fields. Since the first edition of this book was published, large developments have occurred in the theoretical understanding of-and subsequent ability to assess and apply-principles of thermal analysis. Drawing on the knowledge of its expert author, this second edition provides fascinating insight for both new and experienced students, researchers, and industry professionals whose work is influenced or impacted by thermo analysis principles and tools. Part 1 provides a detailed introduction and guide to theoretical aspects of thermal analysis and the related impact of thermodynamics. Key terminology and concepts, the fundamentals of thermophysical examinations, thermostatics, equilibrium background, thermotics, reaction kinetics and models, thermokinetics and the exploitation of fractals are all discussed. Part 2 then goes on to discuss practical applications of this theoretical information to topics such as crystallization kinetics and glass states, thermodynamics in superconductor models, and climate change.