Conventional ultrasonic methods based on ultrasonic characteristics in the linear elastic region are mainly sensitive to mature defects but are much less responsive to micro-damage or incipient material degradation. Recently, nonlinear ultrasonic characteristics beyond the linear ultrasonic amplitude range have been studied as a method for overcoming this limitation, and hence, many researchers are engaged in theoretical, experimental, and various application studies. However, the nonlinear ultrasonic characteristics are quite exacting compared to the linear phenomena so that they require vast experience and high proficiency in order to obtain proper experimental data. Actually, many researchers, especially beginners including graduate students, have difficulty in reliably measuring nonlinear ultrasonic characteristics. This book provides key technological know-how from experts with years of experience in this field, which will help researchers and engineers to obtain a clear understanding and high quality data in the nonlinear ultrasonic experiments and applications.

This updated and revised edition of a classic work provides a summary of methods for numerical computation of high resolution conventional and scanning transmission electron microscope images. At the limits of resolution, image artifacts due to the instrument and the specimen interaction can complicate image interpretation. Image calculations can help the user to interpret and understand high resolution information in recorded electron micrographs. The book contains expanded sections on aberration correction, including a detailed discussion of higher order (multipole) aberrations and their effect on high resolution imaging, new imaging modes such as ABF (annular bright field), and the latest developments in parallel processing using GPUs (graphic processing units), as well as updated references. Beginning and experienced users at the advanced undergraduate or graduate level will find the book to be a unique and essential guide to the theory and methods of computation in electron microscopy.

This edited volume brings together the expertise of numerous specialists on the topic of particles - their physical, chemical, pharmacological and toxicological characteristics - when they are a component of pharmaceutical products and formulations. The book discusses in detail properties such as the composition, size, shape, surface properties and porosity of particles with respect to how they impact the formulations and products in which they are used and the effective delivery of pharmaceutical active ingredients. It considers all dosage forms of pharmaceuticals involving particles, from powders to tablets, creams to ointments, and solutions to dry-powder inhalers, also including the latest nanomedicine products. Further, it discusses examples of particle toxicity, as well as the important subject of pharmaceutical industry regulations, guidelines and legislation. The book is of interest to researchers and practitioners who work on testing and developing pharmaceutical dosage and delivery systems.

^ < p=""> This highly informative and carefully presented volume highlights the impact behavior of fibre reinforced polymer composites. It begins with a preliminary focus on FRP materials, fabrication processes, micro- and macro- mechanics to calculate FRP laminates properties, damage nodes associated with FRP composites under different loadings. It provides a simple and unified approach to cover aspects of FRP composites behavior with low velocity impact loading. This book offers a valuable guide for those who wish to develop deeper insights into weaving architectures, stacking sequences, fabrication processes, general damage modes associated with FRP composites. It is a useful volume for students, academia and industry alike. ^

This book reports on the development and application of a new uniaxial pressure apparatus that is currently generating considerable interest in the field of materials physics. The author provides practical guidelines for performing such experiments, backed up by finite element simulations. Subsequently, the book reports on two uses of the device. In the first, high pressures are used to tune to a Van Hove singularity in Sr2RuO4, while the effects on the unconventional superconductivity and the normal state properties are investigated. In the second experiment, precise and continuous strain control is used to probe symmetry breaking and novel phase formation in the vicinity of a quantum critical point in Sr3Ru2O7.

This book highlights the benefits of Non-Destructive Testing (NDT) methods and their applications on several cultural heritage sites including the Holy Selphuchre Monitoring System in Jerusalem. This book demonstrates Nondestructive sensing technologies and inspection modules as main tools for documentation, diagnosis, characterization, preservation planning, monitoring and quality of restoration, assessment and evaluation of material and preservation work.

This thesis addresses elementary dislocation processes occurring in single-crystalline alloys based on Fe-Al, and investigates correspondences between dislocation distribution inside crystals characterized by transmission electron microscopy (TEM) and surface patterns observed using atomic force microscopy (AFM). Fe-Al alloys with different degrees of ordering were prepared and deformed in compression at ambient temperature in-situ inside the AFM device. The evolution of slip line structures was captured in the sequences of AFM images and wavy slip bands, while cross slip at the tip of the slip band and homogeneous fine slip lines were also identified. Further, the thesis develops a technique for constructing 3D representations of dislocations observed by TEM without the prohibitive difficulties of tomography, and creates 3D models of dislocation structures. Generally speaking, the thesis finds good agreement between AFM and TEM observations, confirming the value of AFM as a relevant tool for studying dislocations.

This second edition of Mass Metrology: The Newly Defined Kilogram has been thoroughly revised to reflect the recent redefinition of the kilogram in terms of Planck's constant. The necessity of defining the kilogram in terms of physical constants was already underscored in the first edition. However, the kilogram can also be defined in terms of Avogadro's number, using a collection of ions of heavy elements, by the levitation method, or using voltage and watt balances. The book also addresses the concepts of gravitational, inertial and conventional mass, and describes in detail the variation of acceleration due to gravity. Further topics covered in this second edition include: the effect of gravity variations on the reading of electronic balances derived with respect to latitude, altitude and earth topography; the classification of weights by the OIML; and maximum permissible error in different categories of weights prescribed by national and international organizations. The book also discusses group weighing techniques and the use of nanotechnology for the detection of mass differences as small as 10-24 g. Last but not least, readers will find details on the XRCD method for defining the kilogram in terms of Planck's constant.

This book presents the proceedings of Fatigue Durability India 2016, which was held on September 28-30 at J N Tata Auditorium, Indian Institute of Science, Bangalore. This 2nd International Conference & Exhibition brought international industrial experts and academics together on a single platform to facilitate the exchange of ideas and advances in the field of fatigue, durability and fracture mechanics and its applications. This book comprises articles on a broad spectrum of topics from design, engineering, testing and computational evaluation of components and systems for fatigue, durability, and fracture mechanics. The topics covered include interdisciplinary discussions on working aspects related to materials testing, evaluation of damage, nondestructive testing (NDT), failure analysis, finite element modeling (FEM) analysis, fatigue and fracture, processing, performance, and reliability. The contents of this book will appeal not only to academic researchers, but also to design engineers, failure analysts, maintenance engineers, certification personnel, and R&D professionals involved in a wide variety of industries.

This book highlights the acoustical metamaterials' capability to manipulate the direction of sound propagation in solids which in turn control the scattering, diffraction and refraction, the three basic mechanisms of sound propagation in solids. This gives rise to several novel theories and applications and hence the name new acoustics. As an introduction, the book mentions that symmetry of acoustic fields is the theoretical framework of acoustical metamaterials. This is then followed by describing that acoustical metamaterials began with locally resonant sonic materials which ushered in the concept of negative acoustic parameters such as mass density and bulk modulus. This complies with form invariance of the acoustic equation of motion which again exemplifies the symmetry property of acoustic fields.

This book provides an overview of recycled polyesters, which are an important sustainable raw material in textile production. It discusses the manufacturing methods and the unique properties of recycled polyesters manufactured using the different methods. It also highlights the various test methods and identification mechanisms for recycled polyesters, which are very essential for ensuring the traceability and conformity of usage of recycled polyester in the final product.

This collection focuses on the characterization of minerals, metals, and materials as well as the application of characterization results on the processing of these materials. Papers cover topics such as clays, ceramics, composites, ferrous metals, non-ferrous metals, minerals, electronic materials, magnetic materials, environmental materials, advanced materials, and soft materials. In addition, papers covering materials extraction, materials processing, corrosion, welding, solidification, and method development are included. This book provides a current snapshot of characterization in materials science and its role in validating, informing, and driving current theories in the field of materials science. This volume will serve the dual purpose of furnishing a broad introduction of the field to novices while simultaneously serving to keep subject matter experts up-to-date.

This book highlights novel applications of innovative fabrics in the design of an interlayer between the scalp and the helmet lining of motorcycle helmets to control the temperature inside the helmet. It examines various fibre microstructure configurations and fibre treatments in terms of their ability to assist in the dissipation of heat from the scalp. The findings presented here will be of considerable benefit to motorcyclists in South East Asia and other tropical regions.

The reader is provided with information about methods of calibration of light sources and photodetectors as well as responsiveness of spectral instruments ranging from near infrared to vacuum UV spectral, 1200 - 100 nm, and radiation intensities of up to several quanta per second in absolute and arbitrary units. The author describes for the first time original methods of measurements they created and draws upon over 40 years of experience in working with light sources and detectors to provide accurate and precise measurements. This book is the first to cover these aspects of radiometry and is divided into seven chapters thatexamine information about terminology, units, light sources and detectors, methods, including author's original ones, of absolute calibration of detectors, spectral instruments responsiveness, absolute measurements of radiation intensity of photoprocesses, and original methods of their study. Of interest to researchers measuring; luminescence spectra, light intensities from IR to vacuum UV, spectral range in wide-light intensity ranges, calibrate light sources and detectors, absolute or relative quantum yields of photoprocess determination.

The book describes developments in the crystal growth of bulk II-VI semiconductor materials. A fundamental, systematic, and in-depth study of the physical vapor transport (PVT) growth process is the key to producing high-quality single crystals of semiconductors. As such, the book offers a comprehensive overview of the extensive studies on ZnSe and related II-VI wide bandgap compound semiconductors, such as CdS, CdTe, ZnTe, ZnSeTe and ZnSeS. Further, it shows the detailed steps for the growth of bulk crystals enabling optical devices which can operate in the visible spectrum for applications such as blue light emitting diodes, lasers for optical displays and in the mid-IR wavelength range, high density recording, and military communications. The book then discusses the advantages of crystallization from vapor compared to the conventional melt growth: lower processing temperatures, the purification process associated with PVT, and the improved surface morphology of the grown crystals, as well as the necessary drawbacks to the PVT process, such as the low and inconsistent growth rates and the low yield of single crystals. By presenting in-situ measurements of transport rate, partial pressures and interferometry, as well as visual observations, the book provides detailed insights into in the kinetics during the PVT process. This book is intended for graduate students and professionals in materials science as well as engineers preparing and developing optical devices with semiconductors.

This book focus on the challenges faced by cutting materials with superior mechanical and chemical characteristics, such as hardened steels, titanium alloys, super alloys, ceramics and metal matrix composites. Aspects such as costs and appropriate machining strategy are mentioned. The authors present the characteristics of the materials difficult to cut and comment on appropriate cutting tools for their machining. This book also serves as a reference tool for manufacturers working in industry.

This book addresses the current status, challenges and future directions of data-driven materials discovery and design. It presents the analysis and learning from data as a key theme in many science and cyber related applications. The challenging open questions as well as future directions in the application of data science to materials problems are sketched. Computational and experimental facilities today generate vast amounts of data at an unprecedented rate. The book gives guidance to discover new knowledge that enables materials innovation to address grand challenges in energy, environment and security, the clearer link needed between the data from these facilities and the theory and underlying science. The role of inference and optimization methods in distilling the data and constraining predictions using insights and results from theory is key to achieving the desired goals of real time analysis and feedback. Thus, the importance of this book lies in emphasizing that the full value of knowledge driven discovery using data can only be realized by integrating statistical and information sciences with materials science, which is increasingly dependent on high throughput and large scale computational and experimental data gathering efforts. This is especially the case as we enter a new era of big data in materials science with the planning of future experimental facilities such as the Linac Coherent Light Source at Stanford (LCLS-II), the European X-ray Free Electron Laser (EXFEL) and MaRIE (Matter Radiation in Extremes), the signature concept facility from Los Alamos National Laboratory. These facilities are expected to generate hundreds of terabytes to several petabytes of in situ spatially and temporally resolved data per sample. The questions that then arise include how we can learn from the data to accelerate the processing and analysis of reconstructed microstructure, rapidly map spatially resolved properties from high throughput data, devise diagnostics for pattern detection, and guide experiments towards desired targeted properties. The authors are an interdisciplinary group of leading experts who bring the excitement of the nascent and rapidly emerging field of materials informatics to the reader.

This book offers a genuinely practical introduction to the most commonly encountered optical and non-optical systems used for the metrology and characterization of surfaces, including guidance on best practice, calibration, advantages and disadvantages, and interpretation of results. It enables the user to select the best approach in a given context. Most methods in surface metrology are based upon the interaction of light or electromagnetic radiation (UV, NIR, IR), and different optical effects are utilized to get a certain optical response from the surface; some of them record only the intensity reflected or scattered by the surface, others use interference of EM waves to obtain a characteristic response from the surface. The book covers techniques ranging from microscopy (including confocal, SNOM and digital holographic microscopy) through interferometry (including white light, multi-wavelength, grazing incidence and shearing) to spectral reflectometry and ellipsometry. The non-optical methods comprise tactile methods (stylus tip, AFM) as well as capacitive and inductive methods (capacitive sensors, eddy current sensors). The book provides: Overview of the working principles Description of advantages and disadvantages Currently achievable numbers for resolutions, repeatability, and reproducibility Examples of real-world applications A final chapter discusses examples where the combination of different surface metrology techniques in a multi-sensor system can reasonably contribute to a better understanding of surface properties as well as a faster characterization of surfaces in industrial applications. The book is aimed at scientists and engineers who use such methods for the measurement and characterization of surfaces across a wide range of fields and industries, including electronics, energy, automotive and medical engineering.

This volume constitutes the state-of-the-art in active interrogation, widely recognized as indispensable methods for addressing current and future nuclear security needs. Written by a leading group of science and technology experts, this comprehensive reference presents technologies and systems in the context of the fundamental physics challenges and practical requirements. It compares the features, limitations, technologies, and impact of passive and active measurement techniques; describes radiation sources for active interrogation including electron and ion accelerators, intense lasers, and radioisotope-based sources; and it describes radiation detectors used for active interrogation. Entire chapters are devoted to data acquisition and processing systems, modeling and simulation, data interpretation and algorithms, and a survey of working active measurement systems. Active Interrogation in Nuclear Security is structured to appeal to a range of audiences, including graduate students, active researchers in the field, and policy analysts. The first book devoted entirely to active interrogation Presents a focused review of the relevant physics Surveys available technology Analyzes scientific and technology trends Provides historical and policy context Igor Jovanovic is a Professor of Nuclear Engineering and Radiological Sciences at the University of Michigan and has previously also taught at Penn State University and Purdue University. He received his Ph.D. from University of California, Berkeley and worked as physicist at Lawrence Livermore National Laboratory. Dr. Jovanovic has made numerous contributions to the science and technology of radiation detection, as well as the radiation sources for use in active interrogation in nuclear security. He has taught numerous undergraduate and graduate courses in areas that include radiation detection, nuclear physics, and nuclear security. At University of Michigan Dr. Jovanovic is the director of Neutron Science Laboratory and is also associated with the Center for Ultrafast Optical Science. Anna Erickson is an Assistant Professor in the Nuclear and Radiological Engineering Program of the G.W. Woodruff School of Mechanical Engineering at Georgia Institute of Technology. Previously, she was a postdoctoral researcher in the Advanced Detectors Group at Lawrence Livermore National Laboratory. Dr. Erickson received her PhD from Massachusetts Institute of Technology with a focus on radiation detection for active interrogation applications. Her research interests focus on nuclear non-proliferation including antineutrino analysis and non-traditional detector design and characterization. She teaches courses in advanced experimental detection for reactor and nuclear nonproliferation applications, radiation dosimetry and fast reactor analysis.

This book presents the relationships between tensile damage and fracture, fatigue hysteresis loops, stress-rupture, fatigue life and fatigue limit stress, and stochastic loading stress. Ceramic-matrix composites (CMCs) possess low material density (i.e., only 1/4 - 1/3 of high-temperature alloy) and high-temperature resistance, which can reduce cooling air and improve structure efficiency. Understanding the failure mechanisms and internal damage evolution represents an important step to ensure reliability and safety of CMCs. This book investigates damage and fracture of fiber-reinforced ceramic-matrix composites (CMCs) subjected to stochastic loading, including: (1) tensile damage and fracture of fiber-reinforced CMCs subjected to stochastic loading; (2) fatigue hysteresis loops of fiber-reinforced CMCs subjected to stochastic loading; (3) stress rupture of fiber-reinforced CMCs with stochastic loading at intermediate temperature; (4) fatigue life prediction of fiber-reinforced CMCs subjected to stochastic overloading stress at elevated temperature; and (5) fatigue limit stress prediction of fiber-reinforced CMCs with stochastic loading. This book helps the material scientists and engineering designers to understand and master the damage and fracture of ceramic-matrix composites under stochastic loading.

The present volume presents six chapters, two of them fairly brief, covering both fundamental and applied electrochemistry. The latter aspect has, of course, historical significance in the subject as well as a major technological profile in recent decades, while intimate connections between these complementary facets of the subject have always been a driving force for its earlier and continu ing development. In the Modern Aspects of Electrochemistry series we have periodically included contributions from the several schools of Russi n electrochemistry. This approach is continued in the present volume by inclusion of the chapter by Benderskii, Brodskii, Daikhin, and Velichko from the Frumkin Institute, Moscow, on phase transitions among molecules adsorbed in the double-layer interphase at electrodes. This topic has attracted attention for some years through the works of the Russian school and of Gierst and Buess-Herman. Such behavior is also related to the important phenomenon of self-assembly of molecules in films at interfaces. In Chapter 1, these authors give an account of the factors associated with two-dimensional phase transitions and associated orientation effects with polar adsorbates at electrode interfaces. The theoretical interpretation of these effects are also treated in some detail. Chapter 2, by Rusling, deals with electrochemistry and electro catalysis in microemulsions, thus connecting aspects of electrode kinetics, adsorption at electrode interfaces, and colloid chemistry."

This special anniversary book celebrates the success of this Springer book series highlighting materials modeling as the key to developing new engineering products and applications. In this 100th volume of "Advanced Structured Materials", international experts showcase the current state of the art and future trends in materials modeling, which is essential in order to fulfill the demanding requirements of next-generation engineering tasks.

This book focuses on the importance of mobile ions presented in oxide structures, what significantly affects the metal-oxide-semiconductor (MOS) properties. The reading starts with the definition of the MOS structure, its various aspects and different types of charges presented in their structure. A review on ionic transport mechanisms and techniques for measuring the mobile ions concentration in the oxides is given, special attention being attempted to the Charge Pumping (CP) technique associated with the Bias Thermal Stress (BTS) method. Theoretical approaches to determine the density of mobile ions as well as their distribution along the oxide thickness are also discussed. The content varies from general to very specific examples, helping the reader to learn more about transport in MOS structures.

This book presents the select proceedings of the International Conference on Functional Material, Manufacturing and Performances (ICFMMP) 2019. The book primarily covers recent research, theories, and practices relevant to surface engineering and processing of materials. It focuses on the lesser-known technologies and advanced manufacturing methods which may not be standardized yet but are highly beneficial to material and manufacturing industrial engineers. The book includes current advances in the field of coating, deposition, cladding, nanotechnology, surface finishing, precision machining, processing, and emerging advanced manufacturing technologies which enhance the performance of materials in terms of corrosion, wear and fatigue. The book can be a valuable reference for beginners, researchers, and professionals interested in materials processing and allied fields.

This book introduces novel developments in the field of electromagnetic non-destructive testing and evaluation (NDT/E). The topics include electromagnetic ultrasonic guided wave testing, pulsed eddy current testing, remote field eddy current testing, low frequency eddy current testing, metal magnetic memory testing, and magnetic flux leakage testing. Considering the increasing concern about the safety maintenance of critical structures in various industries and everyday life, these topics presented here will be of particular interest to the readers in the NDT/E field. This book covers both theoretical researches and the engineering applications of the electromagnetic NDT technology. It could serve as a valuable reference for college students and relevant NDT technicians. It is also a useful material for qualification training and higher learning for nondestructive testing professionals.