This book deals with the properties and behavior of carbon at high temperatures. It presents new methods and new ways to obtain the liquid phase of carbon. Melting of graphite and the properties of liquid carbon are presented under stationary heat and pulse methods. Metal like properties of molten graphite at high initial density are indicated. A new possible transition of liquid carbon from metal to nonmetal behavior much above the melting point is mentioned. Methodical questions of pulse heating, in particular the role of pinch-pressure in receiving a liquid state of carbon, are discussed. The reader finds evidence about the necessity of applying high pressure (higher than 100 bar) to melt graphite (melting temperature 4800+/-100 K). The reader can verify the advantage of volume pulse electrical heating before surface laser heating to study the physical properties of carbon, including enthalpy, heat capacity, electrical resistivity and temperature. The advantages of fast heating of graphite by pulsed electric current during a few microseconds are shown. The data obtained for the heat capacity of liquid carbon under constant pressure and constant volume were used to estimate the behavior at temperatures much higher 5000 K.

The goal of this book is to provide a general overview of the rapidly developing field of novel scanning probe microscopy (SPM) techniques for characterization of a wide range of functional materials, including complex oxides, biopolymers, and semiconductors. Many recent advances in condensed matter physics and materials science, including transport mechanisms in carbon nanostructures and the role of disorder on high temperature superconductivity, would have been impossible without SPM. The unique aspect of SPM is its potential for imaging functional properties of materials as opposed to structural characterization by electron microscopy. Examples include electrical transport and magnetic, optical, and electromechanical properties. By bringing together critical reviews by leading researchers on the application of SPM to to the nanoscale characterization of functional materials properties, this book provides insight into fundamental and technological advances and future trends in key areas of nanoscience and nanotechnology.

* Metivier is an expert in the field of pdes/math physics, with a particular emphasis on shock waves.

* New monograph focuses on mathematical methods, models, and applications of boundary layers, present in many problems of physics, engineering, fluid mechanics.

* Metivier has good Birkhauser track record: one of the main authors of "Advances in the Theory of Shock Waves" (Freistuehler/Szepessy, eds, 4187-4).

* Manuscript endorsed by N. Bellomo, MSSET series editor...should be a good sell to members of MSSET community, who by-in-large are based in Europe.

* Included are self-contained introductions to different topics such as hyperbolic boundary value problems, parabolic systems, WKB methods, construction of profiles, introduction to the theory of Evans' functions, and energy methods with Kreiss' symmetrizers.

From Charpy to Present Impact Testing contains 52 peer-reviewed papers selected from those presented at the Charpy Centenary Conference held in Poitiers, France, 2-5 October 2001.

The name of Charpy remains associated with impact testing on notched specimens. At a time when many steam engines exploded, engineers were preoccupied with studying the resistance of steels to impact loading.

The Charpy test has provided invaluable indications on the impact properties of materials. It revealed the brittle ductile transition of ferritic steels.

The Charpy test is able to provide more quantitative results by instrumenting the striker, which allows the evolution of the applied load during the impact to be determined. The Charpy test is of great importance to evaluate the embrittlement of steels by irradiation in nuclear reactors. Progress in computer programming has allowed for a computer model of the test to be developed; a difficult task in view of its dynamic, three dimensional, adiabatic nature. Together with precise observations of the processes of fracture, this opens the possibility of transferring quantitatively the results of Charpy tests to real components. This test has also been extended to materials other than steels, and is also frequently used to test polymeric materials.

Thus the Charpy test is a tool of great importance and is still at the root of a number of investigations; this is the reason why it was felt that the centenary of the Charpy test had to be celebrated. The Societe Francaise de Metallurgie et de Materiaux decided to organise an international conference which was put under the auspices of the European Society for the Integrity of Structures (ESIS).

This Charpy Centenary Conference (CCC 2001) was held in Poitiers, at Futuroscope in October 2001. More than 150 participants from 17 countries took part in the discussions and about one hundred presentations were given. An exhibition of equipment showed, not only present day testing machines, but also one of the first Charpy pendulums, brought all the way from Imperial College in London.

From Charpy to Present Impact Testing puts together a number of significant contributions. They are classified into 6 headings:

Keynote lectures,
Micromechanisms,
Polymers,
Testing procedures,
Applications,
Modelling.

"

The book is devoted to the problem of microgeometry properties and anisotropy relations in modern piezo-active composites. These materials are characterized by various electromechanical properties and remarkable abilities to convert mechanical energy into electric energy and vice versa. Advantages of the performance of the composites are discussed in the context of the orientation effects, first studied by the authors for main connectivity patterns and with due regard to a large anisotropy of effective piezoelectric coefficients and electromechanical coupling factors. The novelty of the book consists in the systematization results of orientation effects, the anisotropy of piezoelectric properties and their role in forming considerable hydrostatic piezoelectric coefficients, electromechanical coupling factors and other parameters in the composites based on either ferroelectric ceramic or relaxor-ferroelectric single crystals.

Analytical chemists and materials scientists will find this a useful addition to their armory. The contributors have sought to highlight the present state of affairs in the validation and quality assurance of fluorescence measurements, as well as the need for future standards. Methods included range from steady-state fluorometry and microfluorometry, microscopy, and micro-array technology, to time-resolved fluorescence and fluorescence depolarization imaging techniques.

This book presents and introduces ellipsometry in nanoscience and nanotechnology making a bridge between the classical and nanoscale optical behaviour of materials. It delineates the role of the non-destructive and non-invasive optical diagnostics of ellipsometry in improving science and technology of nanomaterials and related processes by illustrating its exploitation, ranging from fundamental studies of the physics and chemistry of nanostructures to the ultimate goal of turnkey manufacturing control. This book is written for a broad readership: materials scientists, researchers, engineers, as well as students and nanotechnology operators who want to deepen their knowledge about both basics and applications of ellipsometry to nanoscale phenomena. It starts as a general introduction for people curious to enter the fields of ellipsometry and polarimetry applied to nanomaterials and progresses to articles by experts on specific fields that span from plasmonics, optics, to semiconductors and flexible electronics. The core belief reflected in this book is that ellipsometry applied at the nanoscale offers new ways of addressing many current needs. The book also explores forward-looking potential applications.

The book is about calorimetry and thermal analysis methods, alone or linked to other techniques, as applied to the characterization of catalysts, supports and adsorbents, and to the study of catalytic reactions in various domains: air and wastewater treatment, clean and renewable energies, refining of hydrocarbons, green chemistry, hydrogen production and storage. The book is intended to fill the gap between the basic thermodynamic and kinetics concepts acquired by students during their academic formation, and the use of experimental techniques such as thermal analysis and calorimetry to answer practical questions. Moreover, it supplies insights into the various thermal and calorimetric methods which can be employed in studies aimed at characterizing the physico-chemical properties of solid adsorbents, supports and catalysts, and the processes related to the adsorption desorption phenomena of the reactants and/or products of catalytic reactions. The book also covers the basic concepts for physico-chemical comprehension of the relevant phenomena. Thermodynamic and kinetic aspects of the catalytic reactions can be fruitfully investigated by means of thermal analysis and calorimetric methods, in order to better understand the sequence of the elemental steps in the catalysed reaction. So the fundamental theory behind the various thermal analysis and calorimetric techniques and methods also are illustrated.

Micromechanisms of Fracture and Fatigue forms the culmination of 20 years of research in the field of fatigue and fracture. It discusses a range of topics and comments on the state of the art for each. The first part is devoted to models of deformation and fracture of perfect crystals. Using various atomistic methods, the theoretical strength of solids under simple and complex loading is calculated for a wide range of elements and compounds, and compared with experimental data. The connection between the onset of local plasticity in nanoindentation tests and the ideal shear strength is analysed using a multi-scale approach. Moreover, the nature of intrinsic brittleness or ductility of perfect crystal lattices is demonstrated by the coupling of atomistic and mesoscopic approaches, and compared with brittle/ductile behaviour of engineering materials. The second part addresses extrinsic sources of fracture toughness of engineering materials, related to their microstructure and microstructurally-induced crack tortuosity. Micromechanisms of ductile fracture are also described, in relation to the fracture strain of materials. Results of multilevel modelling, including statistical aspects of microstructure, are used to explain remarkable phenomena discovered in experiments. In the third part of the book, basic micromechanisms of fatigue cracks propagation under uniaxial and multiaxial loading are discussed on the basis of the unified mesoscopic model of crack tip shielding and closure, taking both microstructure and statistical effects into account. Applications to failure analysis are also outlined, and an attempt is made to distinguish intrinsic and extrinsic sources of materials resistance to fracture. Micromechanisms of Fracture and Fatigue provides scientists, researchers and postgraduate students with not only a deep insight into basic micromechanisms of fracture behaviour of materials, but also a number of engineering applications.

This book presents contributions on the current problems in a number of topical areas of nonlinear dynamics and physics, written by experts from Russia, Ukraine, Israel, Germany, Poland, Italy, the Netherlands, the USA, and France. The book is dedicated to Professor Leonid I. Manevitch, an outstanding scholar in the fields of Mechanics of Solids, Nonlinear Dynamics, and Polymer Physics, on the occasion of his 80th birthday.

This book presents a modern and unconventional introduction to anisotropy. The first part presents a general description of Anisotropic Elasticity theories while the second part focuses on the polar formalism: the theoretical bases and results are completely developed along with applications to design problems of laminated anisotropic structures. The book is based on lectures on anisotropy which have been held at Ecole Polytechnique in Paris.

This book covers the topic of vibration energy harvesting using piezoelectric materials. Piezoelectric materials are analyzed in the context of their electromechanical coupling, heterogeneity, microgeometry and interrelations between electromechanical properties. Piezoelectric ceramics and composites based on ferroelectrics are advanced materials that are suitable for harvesting mechanical energy from vibrations using inertial energy harvesting which relies on the resistance of a mass to acceleration and kinematic energy harvesting which couples the energy harvester to the relative movement of different parts of a source. In addition to piezoelectric materials, research efforts to develop optimization methods for complex piezoelectric energy harvesters are also reviewed. The book is important for specialists in the field of modern advanced materials and will stimulate new effective piezotechnical applications.

Li-Co-Mn-Ni oxides have been of extreme interest as potential positive electrode materials for next generation Li-ion batteries. Though many promising materials have been discovered and studied extensively, much debate remains in the literature about the structures of these materials. There is no consensus as to whether the lithium-rich layered materials are single-phase or form a layered-layered composite on the few nanometer length-scales. Much of this debate came about because no phase diagrams existed to describe these systems under the synthesis conditions used to make electrode materials. Detailed in this thesis are the complete Li-Co-Mn-O and Li-Mn-Ni-O phase diagrams generated by way of the combinatorial synthesis of mg-scale samples at over five hundred compositions characterized with X-ray diffraction. Selected bulk samples were used to confirm that the findings are relevant to synthesis conditions used commercially. The results help resolve a number of points of confusion and contradiction in the literature. Amongst other important findings, the compositions and synthesis conditions giving rise to layered-layered nano-composites are presented and electrochemical results are used to show how better electrode materials can be achieved by making samples in the single phase-layered regions.

The second edition of High Voltage Test Techniques has been completely revised. The present revision takes into account the latest international developments in High Voltage and Measurement technology, making it an essential reference for engineers in the testing field.
High Voltage Technology belongs to the traditional area of Electrical Engineering. However, this is not to say that the area has stood still. New insulating materials, computing methods and voltage levels repeatedly pose new problems or open up methods of solution; electromagnetic compatibility (EMC) or components and systems also demand increased attention. The authors hope that their experience will be of use to students of Electrical Engineering confronted with High Voltage problems in their studies, in research and development and also in the testing field.
Benefit from a completely revised edition
Brings you up-to-date with th latest international developments in High Voltage and Measurement technology
An essential reference for engineers in the testing field

Electrochemistry plays an important role in preserving our cultural heritage. For the first time this has been documented in the present volume. Coverage includes both electrochemical processes such as corrosion and electroanalytical techniques allowing to analyse micro- and nanosamples from works of art or archaeological finds. While this volume is primarily aimed at electrochemists and analytical chemists, it also contains relevant information for conservators, restorers, and archaeologists.

This book gives a brief but thorough introduction to the fascinating subject of non-Newtonian fluids, their behavior and mechanical properties. After a brief introduction of what characterizes non-Newtonian fluids in Chapter 1 some phenomena characteristic of non-Newtonian fluids are presented in Chapter 2. The basic equations in fluid mechanics are discussed in Chapter 3. Deformation kinematics, the kinematics of shear flows, viscometric flows, and extensional flows are the topics in Chapter 4. Material functions characterizing the behavior of fluids in special flows are defined in Chapter 5. Generalized Newtonian fluids are the most common types of non-Newtonian fluids and are the subject in Chapter 6. Some linearly viscoelastic fluid models are presented in Chapter 7. In Chapter 8 the concept of tensors is utilized and advanced fluid models are introduced. The book is concluded with a variety of 26 problems. Solutions to the problems are ready for instructors

This book describes thermoelastic and inelastic deformation processes in crystalline solids undergoing loading by shock compression. Constitutive models with a basis in geometrically nonlinear continuum mechanics supply these descriptions. Large deformations such as finite strains and rotations, are addressed. The book covers dominant mechanisms of nonlinear thermoelasticity, dislocation plasticity, deformation twinning, fracture, flow, and other structure changes. Rigorous derivations of theoretical results are provided, with approximately 1300 numbered equations and an extensive bibliography of over 500 historical and modern references spanning from the 1920s to the present day. Case studies contain property data, as well as analytical, and numerical solutions to shock compression problems for different materials. Such materials are metals, ceramics, and minerals, single crystalline and polycrystalline. The intended audience of this book is practicing scientists (physicists, engineers, materials scientists, and applied mathematicians) involved in advanced research on shock compression of solid materials.

This fully illustrated text explains the basic measurement techniques, describes the commercially available instruments and provides an overview of the current perception of 3-D topography analysis in the academic world and industry, and the commonly used 3-D parameters and plots for the characterizing and visualizing 3-D surface topography.
It also includes new sections providing full treatment of surface characterization, filtering technology and engineered surfaces, as well as a fully updated bibliography.

This book covers a wide range of measurement techniques broadly referred to as Optical Metrology, with emphasis on their applications to nondestructive testing. If we look separately at each of the two terms making the generic name Optical Metrology, we find a link to two of the most distinctive aspects of humans: a particularly well developed sense of vision and a desire to classify things using numbers and rules.
Of all our five senses, vision is certainly the most developed and the closest to the rational part of our brain. It can be argued that our memory is strongly dependent on images and the brain is particularly good at processing the stimuli received from these images to extract information. Measuring, sizing and counting are, on the other hand, among the fundamental building blocks of modern society. The use of abstract quantities like size, value or intensity has simplified the description of complex enquiry and is the basis of modern science and economy. Hence, it would seem natural that the combination of two such basic aspects should result in the birth of a new field of science. However, it is known that his has not been the case. Optical Metrology remains classified as a group of special techniques used mainly in niche applications. Optical Metrology may be rightly described as an ensemble of techniques in which fields such as physics, electrical and mechanical engineering, and computer science merge and blend in new ways.
This book is intended as a tribute to the career of Professor Leopold Pflug. By looking back at his lifelong commitment to the application of optical metrology to the service of engineering sciences, more particularly devoted to the observation of the real behavior of structural components, one can retrace the major revolutions that have taken place in this domain. Starting his activity in 1971 as the head of the Laboratory for Stress Analysis at the EPFL in Switzerland, he first employed photoelasticity as a tool to improve the understanding of the real behavior of complex structures. However he soon recognized the necessity of working with the real materials used to build these structures instead of on replicas made of optically birefringent materials. He then focussed on the use of moire techniques which sparked his fascination with laser-based holography and speckle-based methods. The advent of information technology led him to open up to the use of ESPI and digital image processing techniques. Finally, in the mid 1990s he became interested in the use of optical fibers as a tool for sensing deformations inside structures, not only on their surfaces as in the case of whole-field methods. It is interesting to note the parallel in the evolution of optical metrology vis a vis developments in other fields: the development of lasers led to holographic interferometry, the availability of frame-grabbers led to ESPI and the emergence of fiber optic communications opened the way to the development of fiber optic sensors. This puts in sharp perspective the strong dependence of optical metrology on the latest technology for its development. Also interesting to note is that all fields in optical metrology touched upon by Professor Pflug are still of great relevance, as shown by the contributions in this volume.
This book is, however, not intended as a commemoration, rather as an occasion to review the trends and undercurrents that are driving the field of optical metrology, with emphasis on nondestructive testing. All the authors were asked to summarize the recent achievements in their respective fields and to speculate about the future. As a result it has become apparent that it is difficult although not impossible to spot general trends in these disparate fields. Optical metrology has considerably benefited from some of the most important innovations of the recent past: lasers, computers and fiber optics communication, all of which found their direct inspiration from the developments in the world of electronics.
In recent years we have also witnessed a shift of power from states to corporations. This has created the need to produce quick results useful to industry. Optical nondestructive testing has certainly adapted to this evolution, and several contributions in this book show that the researchers in this field understand the importance of developing technology that can be used by the industry to solve specific problems. We should also not forget that optical nondestructive testing is essentially a "service technology" and should as such not only focus on serving its clients in the best possible way, but also should continually emphasize, extend and enhance its services to new users still unaware of its potential. Hopefully this book will help in spreading awareness of the potentials of optical metrology and in focusing on the challenges of the future.

Micromanufacturing and Nanotechnology is an emerging technological infrastructure and process that involves manufacturing of products and systems at the micro and nano scale levels. Development of micro and nano scale products and systems are underway due to the reason that they are faster, accurate and less expensive. Moreover, the basic functional units of such systems possesses remarkable mechanical, electronic and chemical properties compared to the macro-scale counterparts. Since this infrastructure has already become the prefered choice for the design and development of next generation products and systems it is now necessary to disseminate the conceptual and practical phenomenological know-how in a broader context. This book incorporates a selection of research and development papers. Its scope is the history and background, underlynig design methodology, application domains and recent developments.

The book drawing on the author's nearly half a century of energetic materials research experience intends to systematically review the global researches on liquid explosives. The book focuses on the study of the conception, explosion mechanism, properties and preparation of liquid explosives. It provides a combination of theoretical knowledge and practical examples in a reader-friendly style. The book is likely to be interest of university researchers and graduate students in the fields of energetic materials, blasting engineering and mining.

This book is a manual of measurement of colloids and interfaces designed especially for new researchers who have just begun research on these topics. The book is written by active researchers in the field of colloids and interfacial chemistry, based on the practical experience of the authors. In each chapter, the key points of measurement, how to analyze data correctly, points to be careful about, and merits of a particular method are concisely explained from the point of view of the readers. Not only in industries such as cosmetics and pharmaceuticals but also in academic studies of nanotechnology, correct understanding of colloid and interface phenomena is vital because the properties of these items, however small, are affected by the nature of interfaces. This book will be particularly useful for researchers who are not yet fully confident of the measurement techniques that are clearly explained here.

Ion implantation is one of the key processing steps in silicon integrated circuit technology. Some integrated circuits require up to 17 implantation steps and circuits are seldom processed with less than 10 implantation steps. Controlled doping at controlled depths is an essential feature of implantation. Ion beam processing can also be used to improve corrosion resistance, to harden surfaces, to reduce wear and, in general, to improve materials properties. This book presents the physics and materials science of ion implantation and ion beam modification of materials. It covers ion-solid interactions used to predict ion ranges, ion straggling and lattice disorder. Also treated are shallow-junction formation and slicing silicon with hydrogen ion beams. Topics important for materials modification topics, such as ion-beam mixing, stresses, and sputtering, are also described.

This text, the first of its kind, delivers a systematically organized introduction to the theory and practice of yield prediction. The book addresses the economic need for accurate yield prediction, and clarifies the important role it plays in the semiconductor industry.

This book covers the topic of eddy current nondestructive evaluation, the most commonly practiced method of electromagnetic nondestructive evaluation (NDE). It emphasizes a clear presentation of the concepts, laws and relationships of electricity and magnetism upon which eddy current inspection methods are founded. The chapters include material on signals obtained using many common eddy current probe types in various testing environments. Introductory mathematical and physical concepts in electromagnetism are introduced in sufficient detail and summarized in the Appendices for easy reference. Worked examples and simple calculations that can be done by hand are distributed throughout the text. These and more complex end-of-chapter examples and assignments are designed to impart a working knowledge of the connection between electromagnetic theory and the practical measurements described. The book is intended to equip readers with sufficient knowledge to optimize routine eddy current NDE inspections, or design new ones. It is useful for graduate engineers and scientists seeking a deeper understanding of electromagnetic methods of NDE than can be found in a guide for practitioners.