This book focuses on charged-particle optics and microscopy, as well as their applications in the materials sciences. Presenting a range of cutting-edge theoretical and methodological advances in electron microscopy and microanalysis, and examining their crucial roles in modern materials research, it offers a unique resource for all researchers who work in ultramicroscopy and/or materials research. The book addresses the growing opportunities in this field and introduces readers to the state of the art in charged-particle microscopy techniques. It showcases recent advances in scanning electron microscopy, transmission electron microscopy and helium ion microscopy, including advanced spectroscopy, spherical-corrected microscopy, focused-ion imaging and in-situ microscopy. Covering these and other essential topics, the book is intended to facilitate the development of microscopy techniques, inspire young researchers, and make a valuable contribution to the field.

This book focuses on the widely used experimental techniques available for the structural, morphological, and spectroscopic characterization of materials. Recent developments in a wide range of experimental techniques and their application to the quantification of materials properties are an essential side of this book. Moreover, it provides concise but thorough coverage of the practical and theoretical aspects of the analytical techniques used to characterize a wide variety of functional nanomaterials. The book provides an overview of widely used characterization techniques for a broad audience: from beginners and graduate students, to advanced specialists in both academia and industry.

Handbook of Materials Failure Analysis: With Case Studies from the Aerospace and Automotive Industries provides a thorough understanding of the reasons materials fail in certain situations, covering important scenarios, including material defects, mechanical failure as a result of improper design, corrosion, surface fracture, and other environmental causes. The book begins with a general overview of materials failure analysis and its importance, and then logically proceeds from a discussion of the failure analysis process, types of failure analysis, and specific tools and techniques, to chapters on analysis of materials failure from various causes. Later chapters feature a selection of newer examples of failure analysis cases in such strategic industrial sectors as aerospace, oil & gas, and chemicals.

This monograph deals with the mechanics and thermodynamics of materials with memory, including properties of the dynamical equations that describe their evolution in time under varying loads. A work in four parts, the first is an introduction to continuum mechanics, including classical fluid mechanics, linear and non-linear elasticity. The second part considers continuum thermodynamics and its use to derive constitutive equations of materials with memory, including viscoelastic solids, fluids, heat conductors and some examples of non-simple materials. In the third part, free energies for materials with linear memory constitutive relations are discussed. The concept of a minimal state is introduced. Explicit formulae are presented for the minimum and related free energies. The final part deals with existence, uniqueness, and stability results for the integrodifferential equations describing the dynamical evolution of viscoelastic materials, including a new approach based on minimal states rather than histories. There are also chapters on the controllability of thermoelastic systems with memory, the Saint-Venant problem for viscoelastic materials and on the theory of inverse problems. The second edition includes a new chapter on thermoelectromagnetism as well as recent findings on minimal states and free energies. It considers the case of minimum free energies for non-simple materials and dielectrics, together with an introduction to fractional derivative models.

This book presents the findings of experimental and theoretical (including first-principles molecular dynamics simulation) studies of nanostructured and nanocomposite metal-based materials, and nanoscale multilayer coatings fabricated by physical or chemical vapor deposition, magnetron sputtering, electrospark alloying, ionic layer absorption, contact melting, and high-current electron beam irradiation. It also discusses novel methods of nanocomposite formation, as well as the structure of the deposited films, coatings and other nanoscale materials, their elemental and phase composition, and their physical-mechanical, tribological, magnetic and electrical properties. Lastly, it explores the influence of a various surface modification methods, such as thermal annealing, pulsed laser modification, and thermomechanical and ultrasonic treatment, as well as different properties of nanostructured films.

This book introduces the peridynamic (PD) differential operator, which enables the nonlocal form of local differentiation. PD is a bridge between differentiation and integration. It provides the computational solution of complex field equations and evaluation of derivatives of smooth or scattered data in the presence of discontinuities. PD also serves as a natural filter to smooth noisy data and to recover missing data. This book starts with an overview of the PD concept, the derivation of the PD differential operator, its numerical implementation for the spatial and temporal derivatives, and the description of sources of error. The applications concern interpolation, regression, and smoothing of data, solutions to nonlinear ordinary differential equations, single- and multi-field partial differential equations and integro-differential equations. It describes the derivation of the weak form of PD Poisson's and Navier's equations for direct imposition of essential and natural boundary conditions. It also presents an alternative approach for the PD differential operator based on the least squares minimization. Peridynamic Differential Operator for Numerical Analysis is suitable for both advanced-level student and researchers, demonstrating how to construct solutions to all of the applications. Provided as supplementary material, solution algorithms for a set of selected applications are available for more details in the numerical implementation.

This book concisely illustrates the techniques of major surface analysis and their applications to a few key examples. Surfaces play crucial roles in various interfacial processes, and their electronic/geometric structures rule the physical/chemical properties. In the last several decades, various techniques for surface analysis have been developed in conjunction with advances in optics, electronics, and quantum beams. This book provides a useful resource for a wide range of scientists and engineers from students to professionals in understanding the main points of each technique, such as principles, capabilities and requirements, at a glance. It is a contemporary encyclopedia for selecting the appropriate method depending on the reader's purpose.

The series Topics in Current Chemistry Collections presents critical reviews from the journal Topics in Current Chemistry organized in topical volumes. The scope of coverage is all areas of chemical science including the interfaces with related disciplines such as biology, medicine and materials science. The goal of each thematic volume is to give the non-specialist reader, whether in academia or industry, a comprehensive insight into an area where new research is emerging which is of interest to a larger scientific audience.Each review within the volume critically surveys one aspect of that topic and places it within the context of the volume as a whole. The most significant developments of the last 5 to 10 years are presented using selected examples to illustrate the principles discussed. The coverage is not intended to be an exhaustive summary of the field or include large quantities of data, but should rather be conceptual, concentrating on the methodological thinking that will allow the non-specialist reader to understand the information presented. Contributions also offer an outlook on potential future developments in the field.

The book gathers the peer-reviewed contributions presented at the 3rd International Conference on Application of Superabsorbent Polymers (SAP) and Other New Admixtures towards Smart Concrete, held in Skukuza, South Africa, on November 25-27, 2019. It features papers focusing on the behavior of SAP in concrete (in particular the absorption behavior) as well as the effect of SAP on fresh and hardened concrete properties. It also covers topics such as other modern admixtures, in particular rheology-modifying admixtures, including the recently emerging field of bio- or waste-derived admixtures. The conference builds on the experience and summarizes the activities of the RILEM Technical Committee 260-RSC "Recommendations for Use of Superabsorbent Polymers in Concrete Construction" and addresses other prominent research activities in the field of concrete admixtures.

This book discusses several mechanical and material problems that are typical for gas turbine components. It discusses accelerated tests and other methods for increasing the reliability of gas turbine engines. Special attention is given to non-traditional methods for calculating the strength characteristics and longevity of the main components. This first volume focuses on the selection of materials, deformation and destruction mechanisms in connection with stationary and non-stationary loading, and types of material damage such as the thermal fatigue. Particular attention is paid to the issues of the properties of single crystal alloys, the relationship between structure and properties, the influence of technological factors and long-term operation. The characteristics of creep resistance, crack resistance, and resistance to cyclic deformation of different alloys are given.

This book describes technical and practical aspects of pipeline damage. It summarizes the phenomena, mechanisms and management of pipeline corrosion in-service. The topics discussed include pipelines fracture mechanics, damage mechanisms and evolution, and pipeline integrity assessment. The concept of acceptable risk is also elucidated and the future application of new knowledge management tools is considered.

This book highlights the mathematical models and solutions of the generalized dynamics of soft-matter quasicrystals (SMQ) and introduces possible applications of the theory and methods. Based on the theory of quasiperiodic symmetry and symmetry breaking, the book treats the dynamics of individual quasicrystal systems by reducing them to nonlinear partial differential equations and then provides methods for solving the initial-boundary value problems in these equations. The solutions obtained demonstrate the distribution, deformation and motion of SMQ and determine the stress, velocity and displacement fields. The interactions between phonons, phasons and fluid phonons are discussed in some fundamental materials samples. The reader benefits from a detailed comparison of the mathematical solutions for both solid and soft-matter quasicrystals, gaining a deeper understanding of the universal properties of SMQ. The second edition covers the latest research progress on quasicrystals in topics such as thermodynamic stability, three-dimensional problems and solutions, rupture theory, and the photonic band-gap and its applications. These novel chapters make the book an even more useful and comprehensive reference guide for researchers in condensed matter physics, chemistry and materials sciences.

This book addresses perovskite quantum dots, discussing their unique properties, synthesis, and applications in nanoscale optoelectronic and photonic devices, as well as the challenges and possible solutions in the context of device design and the prospects for commercial applications. It particularly focuses on the luminescent properties, which differ from those of the corresponding quantum dots materials, such as multicolor emission, fluorescence narrowing, and tunable and switchable emissions from doped nanostructures. The book first describes the characterization and fabrication of perovskite quantum dots. It also provides detailed methods for analyzing the electrical and optical properties, and demonstrates promising applications of perovskite quantum dots. Furthermore, it presents a series of optoelectronic and photonic devices based on functional perovskite quantum dots, and explains the incorporation of perovskite quantum dots in semiconductor devices and their effect of the performance. It also explores the challenges related to optoelectronic devices, as well as possible strategies to promote their commercialization. As such, this book is a valuable resource for graduate students and researchers in the field of solid-state materials and electronics wanting to gain a better understanding of the characteristics of quantum dots, and the fundamental optoelectronic properties and operation mechanisms of the latest perovskite quantum dot-based devices.

This book investigates geopolymers and geopolymer-based composites, with a focus on their preparation, geopolymerization mechanisms, microstructures, mechanical properties, and fracture behaviors. Geopolymers are inorganic materials consisting of tetrahedral units (such as [SiO4] and [AlO4]) linked by shared oxygens and forming long-range, covalently bonded and amorphous frameworks. Geopolymers have the advantages of low-temperature preparation, low cost, high heat and corrosion resistance, and being environmentally friendly. Using the preparation methods for epoxy-based composite, they can easily be formed into complex shapes or structures. Intended for researchers investigating geopolymers and their matrix composite materials, this book is also a valuable resource for engineers from various fields, such as materials, mechanical, civil and structural engineering, as well as students interested in other kinds of inorganic materials or even cementitious materials in general.

Reflection high-energy electron diffraction (RHEED) is the analytical tool of choice for characterizing thin films during growth by molecular beam epitaxy, since it is very sensitive to surface structure and morphology. This book serves as an introduction to RHEED for beginners and describes detailed experimental and theoretical treatments for experts, explaining how to analyze RHEED patterns. For beginners the principles of electron diffraction are explained and many examples of the interpretation of RHEED patterns are described. The second part of the book contains detailed descriptions of RHEED theory. The third part applies RHEED to the determination of surface structures, gives detailed descriptions of the effects of disorder, and critically reviews the mechanisms contributing to RHEED intensity oscillations. This unified and coherent account will appeal to both graduate students and researchers in the study of molecular beam epitaxial growth.

This volume gathers the latest advances, innovations, and applications in the field of accelerated pavement testing (APT), presented at the 6th International Conference on Accelerated Pavement Testing, in Nantes, France, in April 2022. Discussing APT, which involves rapid testing of full-scale pavement constructions for structural deterioration, the book covers topics such as APT facilities, APT of asphalt concrete and sustainable/innovative materials, APT for airfield pavements, testing of maintenance and rehabilitation solutions, testing of smart and multi-functional pavements, data analysis and modeling, monitoring and non-destructive testing, and efficient means of calibrating/developing pavement design methods. Featuring peer-reviewed contributions by leading international researchers and engineers, the book is a timely and highly relevant resource for materials scientists and engineers interested in determining the performance of pavement structures during their service life (10+ years) in a few weeks or months.

This book offers a comprehensive introduction to polymer rheology with a focus on the viscoelastic characterization of polymeric materials. It contains various numerical algorithms for the processing of viscoelastic data, from basic principles to advanced examples which are hard to find in the existing literature. The book takes a multidisciplinary approach to the study of the viscoelasticity of polymers, and is self-contained, including the essential mathematics, continuum mechanics, polymer science and statistical mechanics needed to understand the theories of polymer viscoelasticity. It covers recent achievements in polymer rheology, such as theoretical and experimental aspects of large amplitude oscillatory shear (LAOS), and numerical methods for linear viscoelasticity, as well as new insights into the interpretation of experimental data. Although the book is balanced between the theoretical and experimental aspects of polymer rheology, the author's particular interest in the theoretical side will not remain hidden. Aimed at readers familiar with the mathematics and physics of engineering at an undergraduate level, the multidisciplinary approach employed enables researchers with various scientific backgrounds to expand their knowledge of polymer rheology in a systematic way.

This exhaustive work in several volumes and over 2500 pages provides a thorough treatment of ultra-high temperature materials (with melting points around or over 2500 DegreesC). The first volume focuses on carbon (graphene/graphite) and refractory metals (W, Re, Os, Ta, Mo, Nb and Ir), whilst the second and third are dedicated to refractory transition metal 4-5 groups carbides. Topics included are physical (structural, thermal, electro-magnetic, optical, mechanical, nuclear) and chemical (more than 3000 binary, ternary and multi-component systems, including those used for materials design, data on solid-state diffusion, wettability, interaction with various elements and compounds in solid and liquid states, gases and chemicals in aqueous solutions) properties of these materials. It will be of interest to researchers, engineers, postgraduate, graduate and undergraduate students alike. The readers/users are provided with the full qualitative and quantitative assessment, which is based on the latest updates in the field of fundamental physics and chemistry, nanotechnology, materials science, design and engineering.

This book gathers selected, extended and revised papers presented at the 5th Iberian-Latin American Congress on Fire Safety, CILASCI 5, held on 15-17 July 2019, in Porto, Portugal. The respective chapters address experimental efforts and the computational and numerical modelling of materials (e.g. wood, concrete, and steel) and structures to assess their fire behavior and/or improve their fire resistance. In addition, they present simulation studies on fire events and findings from fire performance tests on walls. Given its scope, the book offers a valuable resource for researchers, graduate students, and practitioners whose work involves fire safety-related topics.

This textbook offers readers an introduction to fracture mechanics, equipping them to grasp the basic ideas of the presented approaches to modeling in applied mechanics In the first part, the book reviews and expands on the classical theory of elastic and elasto-plastic material behavior. A solid understanding of these two topics is the essential prerequisite to advancing to damage and fracture mechanics. Thus, the second part of this course provides an introduction to the treatment of damage and fractures in the context of applied mechanics Wherever possible, the one-dimensional case is first introduced and then generalized in a following step. This departs somewhat from the more classical approach, where first the most general case is derived and then simplified to special cases. In general, the required mathematics background is kept to a minimum Tutorials are included at the end of each chapter, presenting the major steps for the solution and offering valuable tips and tricks. The supplementary problems featured in the book

The micro- and nano-modification of infrastructure materials and the associated multi-scale characterization and simulation has the potential to open up whole new uses and classes of materials, with wide-ranging implications for society. The use of multi-scale characterization and simulation brings the ability to target changes at the very small scale that predictably effect the bulk behavior of the material and thus allowing for the optimization of material behavior and performance. The International RILEM Symposium on Multi-Scale Modeling and Characterization of Infrastructure Materials (Stockholm, June 10-12, 2013) brought together key researchers from around the world to present their findings and ongoing research in this field in a focused environment with extended discussion times. From asphalt to concrete, from chemistry to mechanics, from nano- to macro-scale: the collection of topics covered by the Symposium represents the width and depth of the currently ongoing efforts of developing more sustainable infrastructure materials. Researchers, practitioners, undergraduates and graduate students engaged in infrastructure materials or multi-scale characterization and modeling efforts can use this book as a comprehensive reference, to learn about the currently ongoing research efforts in this field or as an inspiration for new research ideas to enhance the long-term performance of infrastructure materials from a fundamental perspective. The Symposium was held under the auspices of the RILEM Technical Committee on Nanotechnology-Based Bituminous Materials 231-NBM and the Transport Research Board (TRB) Technical Committee on Characteristics of Asphalt Materials AFK20.

The book examines advanced, non-standardized techniques that have been developed for determining different properties of cement paste, mortar and concrete, and provides state-of-the-art information on methods for monitoring hydration-induced changes in cement-based materials (CBMs). These methods are often nondestructive and allow quasi-continuous monitoring covering the time span from placement of the material to formation of a fully hardened cement composite. The book also presents various applications of acoustic emission for characterizing fresh concrete, recent developments in ultrasonic methods for characterizing CBMs since placement, application of ambient response methods for measuring elastic modulus, methods for determining deformational characteristics of CBMs since setting and methods for in situ measurements of stresses in concrete elements during hardening.

This book comprehensively outlines synchrotron-based X-ray imaging technologies and their associated applications in gaining fundamental insights into the physical and chemical properties as well as reaction mechanisms of energy materials. In this book the major X-ray imaging technologies utilised, depending on research goals and sample specifications, are discussed. With X-ray imaging techniques, the morphology, phase, lattice and strain information of energy materials in both 2D and 3D can be obtained in an intuitive way. In addition, due to the high penetration of X-rays, operando/in situ experiments can be designed to track the qualitative and quantitative changes of the samples during operation. This book will broader the reader's view on X-ray imaging techniques and inspire new ideas and possibilities in energy materials research.

The second edition of High Voltage Test Techniques has been completely revised. The present revision takes into account the latest international developments in High Voltage and Measurement technology, making it an essential reference for engineers in the testing field.
High Voltage Technology belongs to the traditional area of Electrical Engineering. However, this is not to say that the area has stood still. New insulating materials, computing methods and voltage levels repeatedly pose new problems or open up methods of solution; electromagnetic compatibility (EMC) or components and systems also demand increased attention. The authors hope that their experience will be of use to students of Electrical Engineering confronted with High Voltage problems in their studies, in research and development and also in the testing field.
Benefit from a completely revised edition
Brings you up-to-date with th latest international developments in High Voltage and Measurement technology
An essential reference for engineers in the testing field

A composite sandwich panel is a hybrid material made up of constituents such as a face sheet, a core, and adhesive film for bonding the face sheet and core together. Advances in materials have provided designers with several choices for developing sandwich structures with advanced functionalities. The selection of a material in the sandwich construction is based on the cost, availability, strength requirements, ease of manufacturing, machinability, and post-manufacturing process requirements. Sandwich Composites: Fabrication and Characterization provides insights into composite sandwich panels based on the material aspects, mechanical properties, defect characterization, and secondary processes after the fabrication, such as drilling and repair. FEATURES Outlines existing fabrication methods and various materials aspects Examines composite sandwich panels made of different face sheets and core materials Covers the response of composite sandwich panels to static and dynamic loads Describes parameters governing the drilling process and repair procedures Discusses the applications of composite sandwich panels in various fields Explores the role of 3D printing in the fabrication of composite sandwich panels Due to the wide scope of the topics covered, this book is suitable for researchers and scholars in the research and development of composite sandwich panels. This book can also be used as a reference by professionals and engineers interested in understanding the factors governing the material properties, material response, and the failure behavior under various mechanical loads.