This thesis addresses elementary dislocation processes occurring in single-crystalline alloys based on Fe-Al, and investigates correspondences between dislocation distribution inside crystals characterized by transmission electron microscopy (TEM) and surface patterns observed using atomic force microscopy (AFM). Fe-Al alloys with different degrees of ordering were prepared and deformed in compression at ambient temperature in-situ inside the AFM device. The evolution of slip line structures was captured in the sequences of AFM images and wavy slip bands, while cross slip at the tip of the slip band and homogeneous fine slip lines were also identified. Further, the thesis develops a technique for constructing 3D representations of dislocations observed by TEM without the prohibitive difficulties of tomography, and creates 3D models of dislocation structures. Generally speaking, the thesis finds good agreement between AFM and TEM observations, confirming the value of AFM as a relevant tool for studying dislocations.

The 3rd International Multidisciplinary Microscopy Congress (InterM2015), held from 19 to 23 October 2015, focused on the latest developments concerning applications of microscopy in the biological, physical and chemical sciences at all dimensional scales, advances in instrumentation, techniques in and educational materials on microscopy. These proceedings gather 17 peer-reviewed technical papers submitted by leading academic and research institutions from nine countries and representing some of the most cutting-edge research available.

This book examines in detail key aspects of sustainability in the textile industry, especially environmental, social and economic sustainability in the textiles and clothing sector. It highlights the various faces and facets of sustainability and their implications for textiles and the clothing sector.

This second edition provides comprehensive information on electromagnetic acoustic transducers (EMATs), from the theory and physical principles of EMATs to the construction of systems and their applications to scientific and industrial ultrasonic measurements on materials. The original version has been complemented with selected ideas on ultrasonic measurement that have emerged since the first edition was released. The book is divided into four parts: PART I offers a self-contained description of the basic elements of coupling mechanisms along with the practical designing of EMATs for various purposes. Several implementations to compensate for EMATs' low transfer efficiency are provided, along with useful tips on how to make an EMAT. PART II describes the principle of electromagnetic acoustic resonance (EMAR), which makes the most of EMATs' contactless nature and is the most successful amplification mechanism for precise measurements of velocity and attenuation. PART III applies EMAR to studying physical acoustics. New measurements have emerged with regard to four major subjects: in situ monitoring of dislocation behavior, determination of anisotropic elastic constants, pointwise elasticity mapping (RUM), and acoustic nonlinearity evolution. PART IV deals with a variety of individual issues encountered in industrial applications, for which the EMATs are believed to be the best solutions. This is proven by a number of field applications.

This book offers an essential introduction to the linear and non-linear behavior of solid materials, and to the concepts of deformation, displacement and stress, within the context of continuum mechanics and thermodynamics. To illustrate the fundamental principles, the book starts with an overview of solid mechanics, experimental methods, classes of material behaviors, and the thermodynamic modeling framework. It then explores linear elastic behavior, thermoelasticity, plasticity, viscoplasticity, fracture mechanics and damage behavior. The last part of the book is devoted to conventional and magnetic shape memory alloys, which may be used as actuators or sensors in adaptive structures. Given its range of coverage, the book will be especially valuable for students of engineering courses in Mechanics. Further, it includes a wealth of examples and exercises, making it accessible to the widest possible audience.

This book is a comprehensive, theoretical, practical, and thorough guide to XAFS spectroscopy. The book addresses XAFS fundamentals such as experiments, theory and data analysis, advanced XAFS methods such as operando XAFS, time-resolved XAFS, spatially resolved XAFS, total-reflection XAFS, high energy resolution XAFS, and practical applications to a variety of catalysts, nanomaterials and surfaces. This book is accessible to a broad audience in academia and industry, and will be a useful guide for researchers entering the subject and graduate students in a wide variety of disciplines.

This book is intended to provide a course of infrared spectroscopy for quantitative analysis, covering both bulk matter and surface/interface analyses. Although the technology of Fourier transform infrared (FT-IR) spectroscopy was established many years ago, the full potential of infrared spectroscopy has not been properly recognized, and its intrinsic potential is still put aside. FT-IR has outstandingly useful characteristics, however, represented by the high sensitivity for monolayer analysis, highly reliable quantitativity, and reproducibility, which are quite suitable for surface and interface analysis. Because infrared spectroscopy provides rich chemical information-for example, hydrogen bonding, molecular conformation, orientation, aggregation, and crystallinity-FT-IR should be the first choice of chemical analysis in a laboratory. In this book, various analytical techniques and basic knowledge of infrared spectroscopy are described in a uniform manner. In particular, techniques for quantitative understanding are particularly focused for the reader's convenience.

Sensors and Instrumentation, Volume 5. Proceedings of the 35th IMAC, A Conference and Exposition on Structural Dynamics, 2017, the fifth volume of ten from the Conference brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on fundamental and applied aspects of Sensors and Instrumentation, including papers on: Sensor Applications Accelerometer Design Accelerometer Calibration Sensor Technology

This interdisciplinary work on condensed matter physics, the continuum mechanics of novel materials, and partial differential equations, discusses the mathematical theory of elasticity and hydrodynamics of quasicrystals, as well as its applications. By establishing new partial differential equations of higher order and their solutions under complicated boundary value and initial value conditions, the theories developed here dramatically simplify the solution of complex elasticity problems. Comprehensive and detailed mathematical derivations guide readers through the work. By combining theoretical analysis and experimental data, mathematical studies and practical applications, readers will gain a systematic, comprehensive and in-depth understanding of condensed matter physics, new continuum mechanics and applied mathematics. This new edition covers the latest developments in quasicrystal studies. In particular, it pays special attention to the hydrodynamics, soft-matter quasicrystals, and the Poisson bracket method and its application in deriving hydrodynamic equations. These new sections make the book an even more useful and comprehensive reference guide for researchers working in Condensed Matter Physics, Chemistry and Materials Science.

This volume features fundamental research and applications in the field of the design and application of engineering materials, predominantly within the context of mechanical engineering applications. This includes a wide range of materials engineering and technology, including metals, e.g., polymers, composites, and ceramics. Advanced applications would include manufacturing in the new or newer materials, testing methods, multi-scale experimental and computational aspects. This book features fundamental research and applications in the design of engineering materials, predominantly within the context of mechanical engineering applications such as automobile, railway, marine, aerospace, biomedical, pressure vessel technology, and turbine technology. It covers a wide range of materials, including metals, polymers, composites, and ceramics. Advanced applications include the manufacturing of new materials, testing methods, multi-scale experimental and computational aspects. p>

This book presents selected contributions to the Symposium of Aeronautical and Aerospace Processes, Materials and Industrial Applications of the XXV International Materials Research Congress (IMRC). Each chapter addresses scientific principles behind processing and production of materials for aerospace/aeronautical applications. The chapter deals with microstructural characterization including composites materials and metals. The second chapter deals with corrosion in aerospace components is a large and expensive problema for aerospace industry. Finally, the last chapter covers modeling and simulation of different processes to evaluate and optimize the forming process. This book is meant to be useful to academics and professionals.

This monograph analyses in detail the physical aspects of the elastic waves radiation during deformation or fracture of materials. It presents the methodological bases for the practical use of acoustic emission device, and describes the results of theoretical and experimental researches of evaluation of the crack growth resistance of materials, selection of the useful AE signals. The efficiency of this methodology is shown through the diagnostics of various-purpose industrial objects. The authors obtain results of experimental researches with the help of the new methods and facilities.

A handbook on syntheses and properties, production processes, and applications of maleic anhydride and maleic anhydride derived products - all in one text. This handbook provides a comprehensive overview of maleic anhydride chemistry and applications from the professional perspective. With chapters written by leading R&D scientists from the chemical industry, and edited by the Vice President and ASI Technology Chief at Ashland Specialty Ingredients (ASI), Dr. Osama M. Musa, readers will find a unique perspective and summary of the latest advancements in the field of maleic anhydride science. Maleic anhydride is produced industrially on large scale (10E3 kt/annum). Its rich chemistry makes it an important raw material for numerous products and processes (e.g. for applications in polymers and coatings), many of which are covered in this handbook for the first time in a comprehensive manner. The broad scope spans topics ranging from production techniques (including topics such as processes, catalysis, trouble-shooting), synthesis and properties of small and polymeric maleic anhydride based compounds (focusing on industrially relevant compounds as well as emerging areas of importance) and in-depth and broad discussions of commercial maleic anhydride based applications.

The second edition of this textbook includes a refined presentation of concepts in each chapter, additional examples; new problems and sections, such as conformal mapping and mechanical behavior of wood; while retaining all the features of the original book. The material included in this book is based upon the development of analytical and numerical procedures pertinent to particular fields of linear elastic fracture mechanics (LEFM) and plastic fracture mechanics (PFM), including mixed-mode-loading interaction. The mathematical approach undertaken herein is coupled with a brief review of several fracture theories available in cited references, along with many color images and figures. Dynamic fracture mechanics is included through the field of fatigue and Charpy impact testing.

Challenges in Mechanics of Time-Dependent Materials, Volume 2 of the Proceedings of the 2016 SEM Annual Conference& Exposition on Experimental and Applied Mechanics, the second volume of ten from the Conference, brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on fundamental and applied aspects of Experimental Mechanics, including papers in the following general technical research areas: Extreme Environments & Environmental Effects Structure-Function of Performance of PE Effects of Inhomogeneities & Interfaces Characterization Across Scales Mechanics of Energy & Energetic Materials Metallic Materials Viscoelasticity & Viscoplasticity

This collection covers a variety of materials science topics and has contributions from leading scientists and engineers representing 8 countries and 9 international materials, metals, and minerals societies. Papers are organized into the following sections:Advanced BiomaterialsAdvanced ManufacturingMaterials for Green Energy Materials for Infrastructure Materials for the Oil and Gas Industry Materials for Transportation and LightweightingMinerals Extraction and ProcessingNanocrystalline and Ultra-fine Grain Materials and Bulk Metallic Glasses Steels

This SpringerBrief discusses the determination and classification of the ambient temperature corrosion and stress corrosion properties of aerospace structural alloys, with emphasis on (1) aluminium alloys, modern (3rd generation) aluminium-lithium alloys, stainless steels and titanium alloys and (2) some of the issues involved. Standard /reference data on environmental properties, including corrosion and stress corrosion, are mandatory for the qualification and certification of materials for aerospace vehicles, and also for the design of actual structures and components. Recommendations for further testing and evaluation are given at appropriate points in the text. The book concludes with a summary of the main topics.

The research and its outcomes presented here is devoted to the use of x-ray scattering to study correlated electron systems and magnetism. Different x-ray based methods are provided to analyze three dimensional electron systems and the structure of transition-metal oxides. Finally the observation of multipole orderings with x-ray diffraction is shown.

This collection presents papers from a symposium on extraction of rare metals as well as rare extraction processing techniques used in metal production. Topics include the extraction and processing of elements like antimony, arsenic, gold, indium, palladium, platinum, rare earth metals including yttrium and neodymium, titanium, tungsten, and vanadium. Rare processing techniques are covered, including direct extraction processes for rare-earth recovery, biosorption of precious metals, fluorination behavior of uranium and zirconium mixture of fuel debris treatment, and recovery of valuable components of commodity metals such as zinc, nickel, and metals from slag.

This book summarizes the preparation, characterization and applications of rubber based nano blends. Rubbers from natural and synthetic polymers and their blends are discussed in the individual chapters, including nitrile, polyurethane, chlorosulphonated, polybutadiene, styrene butadiene, polychloroprene rubbers. In each chapter, contributors from academia and industry describe the preparation and characterization of the rubber blends. Therefore, a variety of characterization methods like tensile testing, differential scanning calorimetry, dynamical mechanical analysis, thermogravimetric analysis, electron microscopy, scattering and diffraction techniques, and rheology measurements are utilized. The authors evaluate the properties of the different materials and discuss numerous fields of application, ranging from biomedicine, packaging, coatings and automobile to aerospace.

This book summarizes the advanced manufacturing technology of original innovations in hot stamping of lightweight car body. A detailed description of the technical system and basic knowledge of sheet metal forming is given, which helps readers quickly understand the relevant knowledge in the field. Emphasis has been placed on the independently developed hot stamping process and equipment, which help describe the theoretical and experimental research on key problems involving stress field, thermal field and phase transformation field in hot stamping process. Also, a description of the formability at elevated temperature and the numerical simulation algorithms for high strength steel hot stamping is given in combination with the experiments. Finally, the book presents some application cases of hot stamping technology such as the lightweight car body design using hot stamping components and gradient hardness components, and the cooling design of the stamping tool. This book is intended for researchers, engineers and graduate students in vehicle engineering, mechanical engineering, especially in the field of advanced manufacturing technology. The book also provides a useful reference for other new technology related temperature and phase transformation, such as aluminum-magnesium alloy hot stamping.

This book presents the theory of continuum mechanics for mechanical, thermodynamical, and electrodynamical systems. It shows how to obtain governing equations and it applies them by computing the reality. It uses only open-source codes developed under the FEniCS project and includes codes for 20 engineering applications from mechanics, fluid dynamics, applied thermodynamics, and electromagnetism. Moreover, it derives and utilizes the constitutive equations including coupling terms, which allow to compute multiphysics problems by incorporating interactions between primitive variables, namely, motion, temperature, and electromagnetic fields. An engineering system is described by the primitive variables satisfying field equations that are partial differential equations in space and time. The field equations are mostly coupled and nonlinear, in other words, difficult to solve. In order to solve the coupled, nonlinear system of partial differential equations, the book uses a novel collection of open-source packages developed under the FEniCS project. All primitive variables are solved at once in a fully coupled fashion by using finite difference method in time and finite element method in space.

This book covers various aspects of characterization of materials in the areas of metals, alloys, steels, welding, nanomaterials, intermetallic, and surface coatings. These materials are obtained by different methods and techniques like spray, mechanical milling, sol-gel, casting, biosynthesis, and chemical reduction among others. Some of these materials are classified according to application such as materials for medical application, materials for industrial applications, materials used in the oil industry and materials used like coatings. The authors provide a comprehensive overview of structural characterization techniques including scanning electron microscopy (SEM), X-ray diffraction (XRD), transmission electron microscopy (TEM), Raman spectroscopy, image analysis, finite element method (FEM), optical microscopy (OM), energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), differential thermal analysis (DTA), differential scanning calorimetry (DSC), ultraviolet-visible spectroscopy (UV-Vis), infrared photo-thermal radiometry (IPTR), electrochemical impedance spectroscopy (EIS), thermogravimetry analysis (TGA), thermo luminescence (TL), photoluminescence (PL), high resolution transmission electron microscopy (HRTEM), and radio frequency (RF). The book includes theoretical models and illustrations of characterization properties-both structural and chemical.

These proceedings collect the papers presented at the 30th International Symposium on Shock Waves (ISSW30), which was held in Tel-Aviv Israel from July 19 to July 24, 2015. The Symposium was organized by Ortra Ltd. The ISSW30 focused on the state of knowledge of the following areas: Nozzle Flow, Supersonic and Hypersonic Flows with Shocks, Supersonic Jets, Chemical Kinetics, Chemical Reacting Flows, Detonation, Combustion, Ignition, Shock Wave Reflection and Interaction, Shock Wave Interaction with Obstacles, Shock Wave Interaction with Porous Media, Shock Wave Interaction with Granular Media, Shock Wave Interaction with Dusty Media, Plasma, Magnetohyrdrodynamics, Re-entry to Earth Atmosphere, Shock Waves in Rarefied Gases, Shock Waves in Condensed Matter (Solids and Liquids), Shock Waves in Dense Gases, Shock Wave Focusing, Richtmyer-Meshkov Instability, Shock Boundary Layer Interaction, Multiphase Flow, Blast Waves, Facilities, Flow Visualization, and Numerical Methods. The two volumes serve as a reference for the participants of the ISSW30 and anyone interested in these fields.

This book presents a systematic and comprehensive exposition of the theory of measurement accuracy and provides solutions that fill significant and long-standing gaps in the classical theory. It eliminates the shortcomings of the classical theory by including methods for estimating accuracy of single measurements, the most common type of measurement. The book also develops methods of reduction and enumeration for indirect measurements, which do not require Taylor series and produce a precise solution to this problem. It produces grounded methods and recommendations for summation of errors. The monograph also analyzes and critiques two foundation metrological documents, the International Vocabulary of Metrology (VIM) and the Guide to the Expression of Uncertainty in Measurement (GUM), and discusses directions for their revision. This new edition adds a step-by-step guide on how to evaluate measurement accuracy and recommendations on how to calculate systematic error of multiple measurements. There is also an extended section on the method of reduction, which provides an alternative to the least-square method and the method of enumeration. Many sections are also rewritten to improve the structure and usability of the material. The 3rd edition reflects the latest developments in metrology and offers new results, and it is designed to be accessible to readers at various levels and positions, including scientists, engineers, and undergraduate and graduate students. By presenting material from a practical perspective and offering solutions and recommendations for problems that arise in conducting real-life measurements, author Semyon Rabinovich offers an invaluable resource for scientists in any field.