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Books > Science & Mathematics > Chemistry > Analytical chemistry > Qualitative analytical chemistry
This first book on load-pull systems is intended for readers with a broad knowledge of high frequency transistor device characterization, nonlinear and linear microwave measurements, RF power amplifiers and transmitters. Load-Pull Techniques with Applications to Power Amplifier Design fulfills the demands of users, designers, and researchers both from industry and academia who have felt the need of a book on this topic. It presents a comprehensive reference spanning different load-pull measurement systems, waveform measurement and engineering systems, and associated calibration procedures for accurate large signal characterization. Besides, this book also provides in-depth practical considerations required in the realization and usage of load-pull and waveform engineering systems. In addition, it also provides procedure to design application specific load-pull setup and includes several case studies where the user can customize architecture of load-pull setups to meet any specific measurement requirements. Furthermore, the materials covered in this book can be part of a full semester graduate course on microwave device characterization and power amplifier design.
Dipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strasso and Anders B. Nielsen.- Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. C. Chan.- Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S. Ulrich.- Probing Quadrupolar Nuclei by Solid-State NMR Spectroscopy: Recent Advances, by Christian Fernandez and Marek Pruski.- Solid State NMR of Porous Materials Zeolites and Related Materials, by Hubert Koller and Mark Weiss.- Solid-State NMR of Inorganic Semiconductors, by James P. Yesinowski.-"
In this thesis Matthew Simpson reportstwo areas of work in gas ion spectroscopy, each investigation in itself worthy of a PhD.The first study uses tunable vacuum-ultraviolet radiation from a synchrotron to identify negative ions from twenty four photoexcited polyatomic molecules in the gas phase. From these experiments, Matthew collects a vast amount of data and summarises and reviews ion-pair formation from polyatomic molecules. The second study is on selected ion flow tube mass spectrometry. Matthew investigates the reactions of cations and anions with ethene, monofluoroethene, 1,1-difluoroethene and tetrafluoroethene. In this study Matthew tries to explain why certain products are formed preferentially over other products at a microscopic level of understanding. The data recorded in this thesis form the most comprehensive collection of information about anion formation and are the basis of a review and numerous articles in specialist journals."
"Electronic Devices for Analog Signal Processing" is intended for engineers and post graduates and considers electronic devices applied to process analog signals in instrument making, automation, measurements, and other branches of technology. They perform various transformations of electrical signals: scaling, integration, logarithming, etc. The need in their deeper study is caused, on the one hand, by the extension of the forms of the input signal and increasing accuracy and performance of such devices, and on the other hand, new devices constantly emerge and are already widely used in practice, but no information about them are written in books on electronics. The basic approach of presenting the material in "Electronic Devices for Analog Signal Processing"can be formulated as follows: the study with help from self-education. While divided into seven chapters, each chapter contains theoretical material, examples of practical problems, questions and tests. The most difficult questions are marked bya diamondand can be given to advanced readers. Paragraphs marked by/// are very important for the understanding of the studied material and together they can serve a brief summary of a section. The text marked by italic indicates new or non-traditional concepts. Calculated examples are indicated by >. The main goal of "Electronic Devices for Analog Signal Processing" is not only to give some knowledge on modern electronic devices, but also to inspire readers on the more detailed study of these devices, understanding of their operation, ability to analyze circuits, synthesize new devices, and assess the possibilities of their application for solution of particular practical problems."
Methods of nuclear magnetic resonance (NMR) are increasingly applied in engineering sciences. The book summarizes research in the field of chemical and process engineering performed at the Karlsruhe Institute of Technology (KIT). Fundamentals of the methods are exposed for readers with an engineering background. Applications cover the fields of mechanical process engineering (filtration, solid-liquid separation, powder mixing, rheometry), chemical process engineering (trickle-bed reactor, ceramic sponges), bioprocess engineering (biofilm growth), and food process engineering (microwave heating, emulsions). Magnetic Resonance Imaging (MRI) as well as low-field NMR are covered with notes on hardware. Emphasis is placed on quantitative data analysis and image processing.
This book mainly focuses on the study of the high-temperature superconductor Bi2Sr2CaCu2O8 by vacuum, ultra-violet, laser-based, angle-resolved photoemission spectroscopy (ARPES). A new form of electron coupling has been identified in Bi2212, which occurs in the superconducting state. For the first time, the Bogoliubov quasiparticle dispersion with a clear band back-bending has been observed with two peaks in the momentum distribution curve in the superconducting state at a low temperature. Readers will find useful information about the technique of angle-resolved photoemission and the study of high-temperature superconductors using this technique. Dr. Wentao Zhang received his PhD from the Institute of Physics at the Chinese Academy of Sciences.
Density functional theory (DFT) has become the standard
workhorse for quantum mechanical simulations as it offers a good
compromise between accuracy and computational cost.
The high time-resolution radio sky represents unexplored astronomical territory. This thesis presents a study of the transient radio sky, focussing on millisecond scales. As such, the work is concerned primarily with neutron stars. In particular this research concentrates on a recently identified group of neutron stars, known as RRATs, which exhibit radio bursts every few minutes to every few hours. After analysing neutron star birthrates, a re-analysis of the Parkes Multibeam Pulsar Survey is described which has resulted in the discovery of 19 new transient radio sources. Of these, 12 have been seen to repeat and a follow-up campaign of observations has been undertaken. These studies have greatly increased our knowledge of the rotational properties of RRATs and enable us to conclude that they are pulsars with extreme nulling and/or pulse-to-pulse modulation. Although the evolution of neutron stars post-supernova is not yet understood, it seems that RRATs fit into the emerging picture in which pulsar magnetospheres switch between stable configurations.
The field of single charge tunneling comprises of phenomena where the tunneling of a microscopic charge, usually carried by an electron or a Cooper pair, leads to macro scopically observable effects. The first conference entirely devoted to this new field was the NATO Advanced Study Institute on Single Charge Tunneling held in Les Hauches, France, March 5-15, 1991. This book contains a series of tutorial articles based on lectures presented at the meeting. It was intended to provide both an introduction for nonexperts and a valuable reference summarizing the state of the art of single charge tun neling. A complementary publication with contributions by participants of the NATO Advanced Study Institute is the Special Issue on Single Charge Tunneling of Zeitschrift fur Physik B, Vol. 85, pp. 317-468 (1991 ). That issue with original papers provides a snapshot af the leading edge of current research in the field. The success of the meeting and the publicatian of this volume was made possible through the generaus support af the NATO Scientific A: ffairs Division, Brussels, Belgium. The Centre de Physique des Hauches has provided a superbly situated conference site and took care af many lacal arrangements. Both far the preparation of the conference and the handling af some manuscripts the suppart af the Centre d 'Etudes de Saclay was essential. The editing of the proceedings volume would not have been passible without the dedicated efforts of Dr. G. -1. Ingald, who tailared a 1\."
Electron energy loss spectroscopy has become an indispensable tool in surface analysis. Although the basic physics of this technique is well understood, instrument design has previously largely been left to intuition. This book is the first to provide a comprehensive treatment of the electron optics involved in the production of intense monochromatic beams and the detection of scattered electrons. It includes a full three-dimensional analysis of the electron optical properties of electron emission systems, monochromators and lens systems, placing particular emphasis on the procedures for matching the various components. The description is kept mathematically simple and focuses on practical aspects, with many hints for writing computer codes to calculate and optimize electrostatic lens elements.
The technological means now exists for approaching the fundamentallimiting scales of solid state electronics in which a single carrier can, in principle, represent a single bit in an information flow. In this light, the prospect of chemically, or biologically, engineered molccular-scale structures which might support information processing functions has enticed workers for many years. The one common factor in all suggested molecular switches, ranging from the experimentally feasible proton-tunneling structure, to natural systems such as the micro-tubule, is that each proposed structure deals with individual information carrying entities. Whereas this future molecular electronics faces enormous technical challenges, the same Iimit is already appearing in existing semiconducting quantum wires and small tunneling structures, both superconducting and normal meta! devices, in which the motion of a single eh arge through the tunneling barrier can produce a sufficient voltage change to cut-off further tunneling current. We may compare the above situation with today's Si microelectronics, where each bit is encoded as a very !arge number, not necessarily fixed, of electrons within acharge pulse. The associated reservoirs and sinks of charge carriers may be profitably tapped and manipulated to proviele macro-currents which can be readily amplified or curtailed. On the other band, modern semiconductor ULSI has progressed by adopting a linear scaling principle to the down-sizing of individual semiconductor devices.
This book provides tools well suited for the quantitative
investigation of semiconductor electron microscopy. These tools
allow for the accurate determination of the composition of ternary
semiconductor nanostructures with a spatial resolution at near
atomic scales. The book focuses on new methods including strain
state analysis as well as evaluation of the composition via the
lattice fringe analysis (CELFA) technique. The basics of these
procedures as well as their advantages, drawbacks and sources of
error are all discussed. The techniques are applied to quantum
wells and dots in order to give insight into kinetic growth effects
such as segregation and migration. In the first part of the book
the fundamentals of transmission electron microscopy are provided.
These are needed for an understanding of the digital image analysis
techniques described in the second part of the book. There the
reader will find information on different methods of
The PUILS series delivers up-to-date reviews of progress in Ultrafast Intense Laser Science, a newly emerging interdisciplinary research field spanning atomic and molecular physics, molecular science and optical science which has been stimulated by the recent developments in ultrafast laser technologies. Each volume compiles peer-reviewed articles authored by researchers at the forefront of each their own subfields of UILS. Every chapter opens with an overview of the topics to be discussed, so that researchers unfamiliar to the subfield as well as graduate students can grasp the importance and attractions of the research topic at hand. These are followed by reports of cutting-edge discoveries. This eighth volume covers a broad range of topics from this interdisciplinary research field, focusing on molecules interacting with ultrashort and intense laser fields, advanced technologies for the characterization of ultrashort laser pulses and their applications, laser plasma formation and laser acceleration.
Chemical relaxation spectrometry involves the application of several different relaxation techniques to investigate the kinetics and mechanisms of fast chemical reactions and also dynamic molecul 10 ar processes that occur in liquids in the time range 1 - 10- secs. These methods have been used widely in several disciplines of the natural sciences including molecular biology, biochemistry, organic stereochemistry, detergent chemistry and inorganic chemistry. The purpose of the Advanced Study Institute was to provide a forum for scientists to discuss the role, scope and limitations of the various applications of chemical relaxation methods in order to stimulate discussion and interaction between workers in these different fields. The papers described in this volume are a summary of the contributions that were discussed at the meeting. The brief given to the authors was to attempt to prepare an article contain ing a good supply of references so that the book can be used not only by those starting in the field, but also by the specialist and research worker. These contributions cover a varied range of topics summarizing the achievements, the current state of knowledge and possible application in many disciplines. It is to be hoped that this volume will help to point out some new directions towards which research efforts are required and to attract new researchers with fresh points of view."
This monograph examines the principles and applications of head-space analysis--a new and rapidly developing independent field in gas chromatographic analysis based on the use of "out of column" phase equilibria and partition coefficients in gas-liquid states. Different variations of quantitative analysis, including techniques for increasing analytical sensitivity and the calibration of chromatographs, are also presented. The advantages of analytical and physicochemical applications are illustrated by such examples as the determination of volatile organic impurities in natural and industrial discharge waters, polymers, and air, and also by examples in medical, biological, food, agricultural, and other types of research. Also included are discussions of the automatic instruments and technical equipment needed to conduct these analyses. A basic knowledge of the principles of gas chromatography and physical chemistry (an understanding of phase equilibria) is assumed. The book, therefore, can be used by a wide circle of readers, from teachers and students in advanced courses dealing with analytical chemistry and gas chromatography, to workers at testing and analytical laboratories. The book will also prove valuable to individuals involved in medicinal, sanitation and forensic chemistry, environmental protection, ecology and criminology.
Sputtering, the ejection of atoms or groups of atoms from the surface of a solid bombarded by energetic particles, is a widely observed phenomenon that has many applications in today's experimental physics and technology. This is the third and final volume of a comprehensive review on sputtering. Whereas the first two volumes deal primarily with physical aspects such as the theory of sputtering, experimentally observed sputtering yields and surface topography changes, this volume is devoted to the characteristic properties of the sputtered particles and technological applications of sputtering. The particles are characterized by their energy, mass, and angular distributions, along with their charge and excitation states, while the applications described in- clude surface and depth analysis, micromachining, and the production of surface coatings and thin films. As in the previous two volumes, the various chapters have been written by the main authorities in the field. The book addresses a broad audience: scientists active in the field will find the overview and background information they have long been seeking, while students and new comers to surface science and materials science will find a readable introduction to sputtering.
Extinction and standardization corrections to infrared measurements are of the utmost importance in astronomy. Various views on these concepts and problems of implementation in infrared photometry are discussed thoroughly and recommendations are presented. Among these are: the adoption of narrower broad-band "Johnson" filters that are better centered in the atmospheric water windows than is currently the case; the measurements of atmospheric water vapor content concurrent with the astronomical measurements; the use of appropriate atmospheric models to treat the extinction adequately; and the publication of complete details of the systemic passbands and their transformability to other systems. To conclude the volume, R. Bell summarizes and comments on the contributions to the symposium, and the editor adds a concluding postscript on post-meeting developments and perspectives. |
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