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Organic Structure Determination Using 2-D NMR Spectroscopy - A Problem-Based Approach (Paperback, 2nd edition)
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Organic Structure Determination Using 2-D NMR Spectroscopy - A Problem-Based Approach (Paperback, 2nd edition)
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Organic Structure Determination Using 2-D NMR Spectroscopy: A
Problem-Based Approach, Second Edition, is a primary text for a
course in two-dimensional (2-D) nuclear magnetic resonance (NMR)
techniques, with the goal to learn to identify organic molecular
structure. It presents strategies for assigning resonances to known
structures and for deducing structures of unknown organic molecules
based on their NMR spectra. The book begins with a discussion of
the NMR technique, while subsequent chapters cover instrumental
considerations; data collection, processing, and plotting; chemical
shifts; symmetry and topicity; through-bond effects; and
through-space effects. The book also covers molecular dynamics;
strategies for assigning resonances to atoms within a molecule;
strategies for elucidating unknown molecular structures; simple and
complex assignment problems; and simple and complex unknown
problems. Each chapter includes problems that will enable readers
to test their understanding of the material discussed. The book
contains 30 known and 30 unknown structure determination problems.
It also features a supporting website from which instructors can
download the structures of the unknowns in selected chapters,
digital versions of all figures, and raw data sets for processing.
This book will stand as a single source to which instructors and
students can go to obtain a comprehensive compendium of NMR
problems of varying difficulty.
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