In the process industry, shutdown and turnaround costs are responsible for an excessive amount of maintenance expenses. Process Plants: Shutdown and Turnaround Management explores various types of shutdowns, presents recommendations for better management, and offers feasible solutions to help reduce overheads. Because turnaround management is the largest maintenance activity, plant turnaround is the focal point of this text. The book details a plan to lengthen the interval between turnarounds, and curtail costs in process production management by at least 30 percent. This practical guidebook provides a thorough study of shutdown management, discusses different types of shutdown and managing events (emergency, unplanned, planned, and turnaround), and covers all aspects of plant turnaround management including startup, shutdown, and maintenance. It describes the five phases of shutdown management-initiating, planning, executing, controlling, and closing. It contains specific principles and precautions for successful shutdown planning, and highlights many aspects including turnaround philosophy, planning and scheduling, estimation, contractor management, execution, safety management, managing human resources, and post shut down review. Process Plants: Shutdown and Turnaround Management also includes topical information that readers can successfully apply to future shutdown projects. It is suitable for industry professionals and graduate students.

For more than three decades the Electroanalytical Chemistry Series has delivered the most in-depth and critical research related to issues in electrochemistry. Volume 24 continues this gold-standard with practical reviews of recent applications as well as innovative contributions from internationally respected specialists who highlight the emergence of new technologies and trends in the field.

A review of the nation's new coverages serves as a ready reminder that drinking water safety is more than regional of local concern. In recent times, the print media alone has drawn attention to barium, bacteria, heavy metals, and increasingly organic contaminants, in public water supplies located in Florida, Rhode Island, Texas, Oregon, Illinois, Minnesota, North Carolina, Michigan, and California, to name a few. In an effort to address one of the major issues confronting the future of the nation's drinking water supplies, chemical contamination, the Drinking Water Research Foundation and the American Chemical Society presented the symposium, "Safe Drinking Water: the Impact of Chemicals on a Limited Resource." To add balance to the total presentation, two papers were included that were not part of the symposium. Many questions as to the public significance of hundreds of organic chemicals known to be present in the national drinking water supply are waiting to be answered. In some areas of the country, aid rain-induced alterations of the natural leaching process represent an unexplored potential source of toxic pollutants. Finding workable ways to clean up the water supply will be an ongoing task. Addressing these questions, as well as investigating how other countries are responding to these problems, the alternate sources available, such as bottled water, and point of use devices, the presenters in this symposium have attempted to explain the problems, situation, and alternatives. As progress is made in one area, setbacks will occur in another. As we eliminate problems thought chemical technology, we often create others, such as contamination of our waters. While all the situations, problems, and alternatives are not discussed in these proceedings, it is hoped that some attention will be brought to the public, government, and private sectors so that future work will be done to assure the nation of safe drinking water resources.

Coulson and Richardson's Chemical Engineering: Volume 3A: Chemical and Biochemical Reactors and Reaction Engineering, Fourth Edition, covers reactor design, flow modelling, gas-liquid and gas-solid reactions and reactors.

Experimental Methods and Instrumentation for Chemical Engineers, Second Edition, touches many aspects of engineering practice, research, and statistics. The principles of unit operations, transport phenomena, and plant design constitute the focus of chemical engineering in the latter years of the curricula. Experimental methods and instrumentation is the precursor to these subjects. This resource integrates these concepts with statistics and uncertainty analysis to define what is necessary to measure and to control, how precisely and how often. The completely updated second edition is divided into several themes related to data: metrology, notions of statistics, and design of experiments. The book then covers basic principles of sensing devices, with a brand new chapter covering force and mass, followed by pressure, temperature, flow rate, and physico-chemical properties. It continues with chapters that describe how to measure gas and liquid concentrations, how to characterize solids, and finally a new chapter on spectroscopic techniques such as UV/Vis, IR, XRD, XPS, NMR, and XAS. Throughout the book, the author integrates the concepts of uncertainty, along with a historical context and practical examples. A problem solutions manual is available from the author upon request.

This unique approach to the basic concepts of adsorption is written for students, engineers, scientists, and others who need a clear presentation of adsorption processes. Unlike other texts on this subject, which are written for the specialist and rely heavily on advanced mathematics, this unique book helps you solve everyday problems in applications of adsorption, without complex mathematics or computers. The author, a recognized expert in the field, gives you a quick introduction to the underlying physics of absorption and explains how to apply adsorption to solve analytical and design problems. Rich with practical examples and enhanced by illustrations that support the text, this refreshingly straightforward presentation helps you cut through the complexities of adsorption to find fast answers to pressing real-world questions.

Coulson and Richardson's Chemical Engineering: Volume 3B: Process Control, Fourth Edition, covers reactor design, flow modeling, and gas-liquid and gas-solid reactions and reactors.

Over the past four decades, notable advancements in the theory and application of ion exchange science uncovered a wealth of knowledge that fueled new scientific pursuits and created synergies with myriad scientific endeavors. Today, pioneers continue to break new ground by synthesizing novel materials and merging the interdisciplinary fields of science and engineering. Now in its 20th volume, Ion Exchange and Solvent Extraction: A Series of Advances chronicles the ongoing changes that drive innovation in this important field. Beginning with a review of research studies that show how functionalized ion exchange polymers serve as supports to stabilize metal nanoparticles (MNPs) without forming larger than nano aggregates, the book describes the sorption of different gases from the air by ion exchange resins and fibrous ion exchangers and discusses the selective ion exchange technology capable of removing and recovering perchlorate quantitatively through stable isotope ratio analysis of chlorine and oxygen atoms, allowing for the forensic analysis of perchlorate origin in contaminated water. Later chapters demonstrate how numerical simulations coupled with small-scale bench-top experiments can help tailor particle size distribution and enhance the efficiency of each application, review dual-temperature ion exchange processes in which sorption and desorption are carried out solely by varying temperature, and present the preparation and characterization of a new composite material in which microparticles of clinoptilolite are embedded in a matrix of cross-linked chitosan, opening new opportunities for the natural biopolymer. The book concludes with the preparation, characterization, and field-level experience of an emerging class of "hybrid ion exchangers" that enhance the application opportunities of ion exchange resins. Highlighting the latest and most pivotal discoveries, the 20th volume of a field standard codifies the current state-of-the-art and lays the groundwork for the next generation of growth and expansion in the field of ion exchange.

Sustainable Design through Process Integration: Fundamentals and Applications to Industrial Pollution Prevention, Resource Conservation, and Profitability Enhancement, Second Edition, is an important textbook that provides authoritative, comprehensive, and easy-to-follow coverage of the fundamental concepts and practical techniques on the use of process integration to maximize the efficiency and sustainability of industrial processes. The book is ideal for adoption in process design and sustainability courses. It is also a valuable guidebook to process, chemical, and environmental engineers who need to improve the design, operation, performance, and sustainability of industrial plants. The book covers pressing and high growth topics, including benchmarking process performance, identifying root causes of problems and opportunities for improvement, designing integrated solutions, enhancing profitability, conserving natural resources, and preventing pollution. Written by one of the world's foremost authorities on integrated process design and sustainability, the new edition contains new chapters and updated materials on various aspects of process integration and sustainable design. The new edition is also packed with numerous new examples and industrial applications.

Characterization of Liquids, Dispersions, Emulsions and Porous Materials Using Ultrasound, Third Edition, presents a scientific background for novel methods of characterizing homogeneous and heterogeneous liquids (dispersions, emulsions, and gels) as well as porous materials. Homogeneous liquids are characterized in rheological terms, whereas particle-size distribution and zeta potential are parameters of heterogeneous liquids. For porous materials, porosity, pore size, and zeta potential are output characteristics. These methods are based on ultrasound, which opens an opportunity for simplifying the sample preparation by eliminating dilution. This in turn, makes measurements faster, easier, precise, suitable for accurate quality control, PAT, and formulation of complex systems. This book provides theoretical background of acoustics, rheology, colloid science, electrochemistry, and other relevant scientific fields, describing principles of existing instrumentation and, in particular, commercially available instruments. Finally, the book features an extensive list of existing applications.

A reflection of the explosion of research and development in this field, OMICS: Biomedical Perspectives and Applications explores applications of omics in bioinformatics, cancer research and therapy, diabetes research, plant science, molecular biology, and neurosciences. A select editorial panel of experts discusses their cutting edge omics research and novel technologies, supplying a basic platform of methods and applications and a resource for enhanced cross-pollination in a multiomics approach to future endeavors in the fertile fields of omics research. After an introduction on the omics universe, the book presents modern omics and its applications in nanotechnology, genomics, proteomics, metagenomics, toxicogenomics, immunomics, nutrigenomics, diabetes, neurology, cardiology, and cancer to name just a few. The book begins with an overview of omics and omic technologies such as cellomics, glycomics, and lipidomics. It also discusses bioinformatics, demonstrating how it can be a tool in omics, and examines the various approaches of omics technology in toxicology research and applications in biomedical sciences. While there are a long list of omics books available, most focus narrowly on one area. Presenting a wide view of the current status of integrative omics, this resource contains complete coverage of omics in research and therapy, ranging from neuroscience to cardiology. It collates recent developments in the field into a state-of-the-art framework for this discipline.

Refiners' efforts to conform to increasingly stringent laws and a preference for fuels derived from renewable sources have mandated changes in fluid cracking catalyst technology. Advances in Fluid Catalytic Cracking: Testing, Characterization, and Environmental Regulations explores recent advances and innovations in this important component of petroleum refining technology and evaluates how the industry has been changed by environmental regulations worldwide. Measurement, testing, and improvement Modern spectroscopic techniques continue to be essential to the understanding of catalyst performance and feedstock properties. The book contains a detailed review of the use of adsorption microcalorimetry to measure acidity, acid site density, and the strength of the strongest acid sites in heterogenous catalysts. It also discusses the use of 1H-NMR to characterize the properties of a FCCU feedstock. In addition, the book dedicates several chapters to pilot plant testing of catalysts and nontraditional feedstocks, maximizing and improving LCO (heating oil) production and quality, and improving FCCU operations. Complying with the EPA The EPA has identified the petroleum refining industry as a targeted enforcement area for the Clean Air Act (CAA) passed in 1970 and the CAA Amendments of 1990. The final chapters of the book examine the evolution of the EPA's attempts to encourage the refining industry to enter into voluntary consent decrees to comply with the CAA and the 1990 amendments. The book describes consent decree negotiations as well as FCC emissions (SOx, NOx, CO, PM) reduction technologies through consent decree implementations. Containing contributions from a panel of worldwide experts, the book demonstrates how the global shift toward environmentalism has engineered significant changes in the petroleum refining industry at a critical level.

Chemical Engineering Process Simulation is ideal for students, early career researchers, and practitioners, as it guides you through chemical processes and unit operations using the main simulation softwares that are used in the industrial sector. This book will help you predict the characteristics of a process using mathematical models and computer-aided process simulation tools, as well as model and simulate process performance before detailed process design takes place. Content coverage includes steady and dynamic simulations, the similarities and differences between process simulators, an introduction to operating units, and convergence tips and tricks. You will also learn about the use of simulation for risk studies to enhance process resilience, fault finding in abnormal situations, and for training operators to control the process in difficult situations. This experienced author team combines industry knowledge with effective teaching methods to make an accessible and clear comprehensive guide to process simulation.

Surface thermodynamics forms the foundation of any meaningful study of capillarity and wetting phenomena. The second edition of Applied Surface Thermodynamics offers a comprehensive state-of-the-art treatment of this critical topic. It provides students and researchers with fundamental knowledge and practical guidelines in solving real-world problems related to the measurement and interpretation of interfacial properties. Containing 40 percent new material and reorganized content, this second edition begins by presenting a generalized Gibbs theory of capillarity, including discussions of highly curved interfaces. Concentrating on drop-shape techniques, the book discusses liquid-fluid interfacial tension and its measurement. Next, the authors focus on contact angles with chapters on experimental procedures, thermodynamic models, and the interpretation of contact angles in terms of solid surface tension. The book discusses theoretical approaches to determining solid surface tension as well as interfacial tensions of particles and their manifestations. It concludes by discussing drop size dependence of contact angles and line tension. What's New in the Second Edition: Recent progress in Axisymmetric Drop Shape Analysis (ADSA) Image processing methods for drop shape analysis Advanced applications and generalizations of ADSA Recent studies of contact angle hysteresis Contact angles on inert fluoropolymers Update on line tension and the drop size dependence of contact angles Exploring a range of different aspects of surface science and its applications, the book logically progresses so that knowledge of previous chapters enhances the understanding of subsequent material, yet each chapter is freestanding so that experienced researchers can quickly refer to topics of particular interest.

What role will biofuels play in the scientific portfolio that might bring energy independence and security, revitalize rural infrastructures, and wean us off of our addiction to oil? The shifting energy landscape of the 21st century, with its increased demand for renewable energy technology, poses a worrying challenge. Discussing the multidisciplinary study of bioenergy and its potential for replacing fossil fuels in the coming decades, Introduction to Biofuels provides a roadmap for understanding the broad sweep of technological, sociological, and energy policy issues that intermingle and intertwine. Copiously illustrated and with numerous examples, this book explores key technologies, including biotechnology, bioprocessing, and genetic reprogramming of microorganisms. The author examines the future of biofuels from a broader perspective, addressing the economic, social, and environmental issues crucial for studying the sustainable development of bioenergy. Each chapter begins with questions and provides the answers later in the chapter as key informational points. Embedded Science, Technology, Engineering, and Math (STEM) sections provide detailed derivations and equations for a subset of topics that can be found easily as buzzwords in popular media and on web sites. Together, the STEM topics form a thread of essential technologies and a guide to how researchers have established quantitative parameters that are crucial to the ever-growing biofuels database. With so much information scattered throughout the literature, it is often difficult to make sense of what is real and what is an optimistic selling of ideas with no scientific credibility. This book does an excellent job of filtering through volumes of data, providing a historical perspective on which to anchor the information, and outlining the strengths and constraints of the different biofuels.

The rise and rationalization of the industrial phosphates industry have gone hand in hand with the development and maturation of technologies to purify phosphoric acid. In the 1960s and 70s, driven by the exponential sales growth of the detergent-builder sodium tripolyphosphate, chemical producers raced to develop processes that would provide a sufficiently pure phosphoric acid feedstock for manufacture to undercut thermal phosphoric acid made from phosphorus. As environmental and political pressure led to a collapse in demand for sodium tripolyphosphate in the 1990s, the commercial pressures to rationalize at plant and corporate levels rose such that only the fittest survived. Phosphoric Acid: Purification, Uses, Technology, and Economics, the first and only book of its kind to be written on this topic, covers the development of purification technologies for phosphoric acid, especially solvent extraction, describing the more successful processes and setting this period in the historical context of the last 350 years. Individual chapters are devoted to the key derivative products which are still undergoing active development, as well as to sustainability and how to approach the commissioning of these plants. The text is aimed at students of chemistry, chemical engineering, business, and industrial history, and to new entrants to the industry.

Discusses the modeling and analysis of nanoparticles. Covers all fundamental aspects of particle and droplet flows. Includes heat and mass transfer processes. Features new and updated sections throughout the text. Includes chapter exercises.

The first edition of Asbestos: Risk Assessment, Epidemiology, and Health Effects received critical acclaim due to the interdisciplinary nature of its content. Editors Ronald Dodson and Samuel Hammar have carefully kept this popular focus while updating and expanding the topics covered in the first edition with the help of internationally known experts. While there are hundreds of books available on many different aspects of asbestos, none contain the encyclopedic, comprehensive coverage you will find here. See What's New in the Second Edition: Definitions of asbestos by different methodologies and the potential impact that those forms have on health Internationally accepted sampling/analytical schemes Findings of major asbestos-related diseases that continue to increase in most industrialized countries where asbestos is widely used Information on asbestos-induced diseases in biological systems Expanded regulations chapter Copiously illustrated with diagrams, tables, and photographs, including some in color, the book remains an interdisciplinary resource on the major issues in asbestos exposure and human health, with coverage that spans history, pathology, and epidemiology as well as sampling, analysis, and regulatory issues. The editors' expertise and careful updating set this book apart, making it a comprehensive resource that interlinks diverse specialties. They provide an updated and expanded state-of-the-art discussion of important interdisciplinary factors associated with asbestos-related issues in an easy-to-use reference.

In recent years, the area dealing with the physical chemistry of materials has become an emerging discipline in materials science that emphasizes the study of materials for chemical, sustainable energy, and pollution abatement applications. Written by an active researcher in this field, Physical Chemistry of Materials: Energy and Environmental Applications presents methods for synthesizing and characterizing adsorbents, ion exchangers, ionic conductors, heterogeneous catalysts, and permeable porous and dense materials. It also discusses their properties and applications. The book explores various examples of these important materials, including perovskites, zeolites, mesoporous molecular sieves, silica, alumina, active carbons, carbon nanotubes, titanium dioxide, magnesium oxide, clays, pillared clays, hydrotalcites, alkali metal titanates, titanium silicates, polymers, and coordination polymers. It shows how the materials are used in adsorption, ion conduction, ion exchange, gas separation, membrane reactors, catalysts, catalysts supports, sensors, pollution abatement, detergency, animal nourishment, agriculture, and sustainable energy applications. Rising pollution levels and the need for sustainable energy have necessitated new ways of using certain materials to combat these problems. Focusing on this emerging discipline, Physical Chemistry of Materials describes the methods of syntheses and characterization of adsorbents, ion exchangers, ionic conductors, catalysts, and permeable materials. It tackles key issues in materials science and physical chemistry.

The novel properties of multifunctional polymer nanocomposites make them useful for a broad range of applications in fields as diverse as space exploration, bioengineering, car manufacturing, and organic solar cell development, just to name a few. Presenting an overview of polymer nanocomposites, how they compare with traditional composites, and their increasing commercial importance, Multifunctional Polymer Nanocomposites conveys the significance and various uses of this new technology for a wide audience with different needs and levels of understanding. Exploring definitions, architectures, applications, and fundamental principles of various functions of multifunctional polymeric smart materials-from bulk to nano-this book covers the use of multifunctional polymer nanocomposites in: Carbon nanotubes Electroactive and shape memory polymers Magnetic polymers Biomedical and bioinformation applications Fire-resistance treatments Coating technologies for aeronautical applications Ocean engineering A practical analysis of functional polymers, nanoscience, and technology, this book integrates coverage of fundamentals, research and development, and the resulting diversity of uses for multifunctional polymers and their nanocomposites. Quite possibly the first reference of its kind to explore the progress of polymer nanocomposites in terms of their multifunctionality, it covers both theory and experimental results regarding the relationships between the effective properties of polymer composites and those of polymer matrices and reinforcements. This book is a powerful informational resource that illustrates the importance of polymer nanomaterials, examining their applications in various sectors to promote new, novel research and development in those areas. It will be a welcome addition to the libraries of not only engineering researchers, but senior and graduate students in relevant fields.

Although nosocomial, or hospital-acquired, infections have been well cataloged and are fairly well understood, traditional solutions have failed to completely eliminate the problem. Even the most modern hospitals find themselves stymied by the persistence of these pathogens in hospital wards and operating rooms. The degree to which most of these infections are airborne is not known, but a growing body of evidence indicates that airborne transmission plays a role in many hospital-acquired infections. Addressing one of the most important topics in health care, Hospital Airborne Infection Control is the first book to deal with the control of airborne nosocomial infections in detail. It identifies all pathogens known or suspected to be airborne, along with their sources in hospital environments. It also summarizes all epidemiological evidence for airborne transmission. The text addresses respiratory, surgical site, burn wound, immunocompromised, pediatric, nursing home, and non-respiratory infections. In each category, an extensive number of examples show that inhalation is not the only airborne route by which infections may be transmitted. Noting that airborne transmission and surface contamination are virtually inseparable, the author emphasizes that both air and surface disinfection, including hand hygiene, are important factors in controlling the transmission of airborne disease. He also proposes a variety of new solutions and technologies, including ultraviolet, ionization, ozone, plasma, and vegetative air cleaning systems. A compendium of scientific and medical information, this book helps hospitals control nosocomial infections and outbreaks spread by the airborne route as well as by direct contact and contact with fomites or contaminated equipment.

The Concise Encyclopedia of Self-Propagating High-Temperature Synthesis: History, Theory, Technology, and Products helps students and scientists understand the fundamental concepts behind self-propagating high-temperature synthesis (SHS). SHS-based technologies provide valuable alterations to traditional methods of material fabrication, such as powder metallurgy, conventional and force sintering, casting, extrusion, high isostatic pressure sintering, and others. The book captures the whole spectrum of the chemistry, physics, reactions, materials, and processes of self-propagating high-temperature synthesis. This book is an indispensable resource not only to scientists working in the field of SHS, but also to researchers in multidisciplinary fields such as chemical engineering, metallurgy, material science, combustion, explosion, and the chemistry of solids.

Pretreatment for Reverse Osmosis Desalination is a comprehensive reference on all existing and emerging seawater pretreatment technologies used for desalination. The book focuses on reverse osmosis membrane desalination, which at present is the most widely applied technology for the production of fresh drinking water from highly saline water sources (brackish water and seawater). Each chapter contains examples illustrating various pretreatment technologies and their practical implementation.

Although batch processing has existed for a long time, designing these processes and unit operations has been considered an onerous task that required computational efforts. Design of these processes is made more complex because of the time dependent nature of the process and the allowable flexibility. More often than not, every unit encounters optimal control problems. Therefore, traditional design books have not covered batch processing in detail. Filling this void, Batch Processing: Modeling and Design describes various unit operations in batch and bio-processing as well as design methods for these units. Topics include: Batch distillation operating modes and configurations Batch absorption operations based on the solubility difference Batch adsorption based on differential affinity of various soluble molecules to solid absorbents Batch chromatography for measuring a wide variety of thermodynamic, kinetic, and physico-chemical properties Batch crystallization where a phase is used to find the supersaturation at which point material crystallizes Batch drying that stresses the phase diagram of water to describe this operation Batch filtration using a porous medium or screen to separate solids from liquids Batch centrifugation where centrifugal force is used for separation Batch processes are widely used in pharmaceutical, food, and specialty chemicals where high value, low volume products are manufactured. Recent developments in bio-based manufacturing also favor batch processes because feed variations can be easily handled in batch processes. Further, the emerging area of nanomaterials manufacturing currently uses batch processes as they are low volume, high energy intensive processes. With examples, case studies, and more than 100 homework problems, this book describes the unit operations in batch and bioprocessing and gives students a thorough grounding in the numerical methods necessary to solve these design problems.

With their broad range of properties, polymer blends are widely used in adhesion, colloidal stability, the design of composite and biocompatible materials, and other areas. As the science and technology of polymer blends advances, an increasing number of polymer blend systems and applications continue to be developed. Functional Polymer Blends: Synthesis, Properties, and Performance presents the latest synthesis and characterization methodologies for generating polymer blend systems. This one-stop resource brings together both experimental and theoretical material, much of which has previously only been available in research papers. Featuring contributions by eminent international experts, the book: Reviews polymer blend systems Details miscibility enhancements in polymer blends through multiple hydrogen binding interactions Presents the component dynamics in polymer blend systems Discusses concepts of shape memory polymer blends Considers ethylene methyl acrylate (EMA) copolymer toughened polymethyl methacrylate (PMMA) blends Provides theoretical insights through molecular dynamics simulation studies for binary blend miscibility Reports on the conformation and topology of cyclic linear polymer blends (CLBs) Addresses strain hardening in polymer blends with fibril morphology Explores the modification of polymer blends by irradiation techniques Examines the directed assembly of polymer blends using nanopatterned chemical surfaces Combining background and advanced information on technologies, methods, and applications, this practical reference is a must-have for researchers and industry professionals as well as students in materials science, chemistry, and chemical and surface engineering.