Ammonia holds great promise as a carbon-neutral liquid fuel for storing intermittent renewable energy sources and power generation due to its high energy density and hydrogen content. Photo-Electrochemical Ammonia Synthesis: Nanocatalyst Discovery, Reactor Design, and Advanced Spectroscopy covers the synthesis of novel hybrid plasmonic nanomaterials and their application in photo-electrochemical systems to convert low energy molecules to high value-added molecules and looks specifically at photo-electrochemical nitrogen reduction reaction (NRR) for ammonia synthesis as an attractive alternative to the long-lasting thermochemical process. Provides an integrated scientific framework, combining materials chemistry, photo-electrochemistry, and spectroscopy to overcome the challenges associated with renewable energy storage and transport Reviews materials chemistry for the synthesis of a range of heterogeneous (photo) electrocatalysts including plasmonic and hybrid plasmonic-semiconductor nanostructures for selective and efficient conversion of N2 to NH3 Covers novel reactor design to study the redox processes in the photo-electrochemical energy conversion system and to benchmark nanocatalysts' selectivity and activity toward NRR Discusses the use of advanced spectroscopic techniques to probe the reaction mechanism for ammonia synthesis Offers techno-economic analysis and presents performance targets for the scale-up and commercialization of electrochemical ammonia synthesis This book is of value to researchers, advanced students, and industry professionals working in sustainable energy storage and conversion across the disciplines of Chemical Engineering, Mechanical Engineering, Materials Science and Engineering, Environmental Engineering, and related areas.

Updating content from the author's 2001 book Coal Desulfurization, this new title focuses on CO2 sequestration and utilization. It includes information on the theory and practical approaches to CO2 capture and recent advances in the use of sequestered CO2. Avoiding these pollutants requires either forgetting about the 250 billion tons of coal reserves the United States possesses or capturing and utilizing the pollutants in a profitable and environmentally responsible fashion. The book covers postcombustion and precombustion capture approaches for coal, and postcombustion capture can be generalized to many other fuels. Recent practical implementations at full-scale power facilities around the world are discussed. The book covers sequestering CO2 via underground, oceanic, biological, and other long-term CO2 storage methods. It also includes recent advances in utilizing CO2 for enhanced oil recovery, advances in storage with depleted oil and gas reservoirs and deep saline aquifers, and additional topics. The book also examines specific applications of pure CO2 and covers chemical conversion of CO2 to useful compounds. It answers questions like "Can we create methanol from coal?" or "Can we create ethanol from coal?" It is found that methanol and ethanol cannot be sustainably produced from coal power alone. However, oxalic acid can be created at a much lower energy cost than methanol or ethanol. Oxalic acid can be used to extract rare earths, which are not currently produced anywhere in the United States, but are typically concentrated in coal ash. Aimed at researchers and industry professionals in chemical, environmental, and energy engineering, this book provides insight and inspiration into capturing CO2 not merely as a response to regulatory pressure and climate change but as an inherently profitable and valuable venture.

Tissue Engineering Strategies for Organ Regeneration addresses the existing and future trends of tissue engineering approaches for organ/tissue regeneration or repair. This book provides a comprehensive summary of the recent improvement of biomaterials used in scaffold-based tissue engineering, and the tools and different protocols needed to design tissues and organs. The chapters in this book provide the in-depth principles for many of the supporting and enabling technologies including the applications of BioMEMS devices in tissue engineering, and the combination of organoid formation and three dimensional (3D) bioprinting. The book also highlights the advances and strategies for regeneration of three-dimensional microtissues in microcapsules, tissue reconstruction techniques, and injectable composite scaffolds for bone tissue repair and augmentation. Key Features: Addresses the current obstacles to tissue engineering applications Provides the latest improvements in the field of integrated biomaterials and fabrication techniques for scaffold-based tissue engineering Shows the influence of microenvironment towards cell-biomaterials interactions Highlights significant and recent improvements of tissue engineering applications for the artificial organ and tissue generation Describes the applications of microelectronic devices in tissue engineering Describes different current bioprinting technologies

Design of new processes that avoid the use of toxic reagents has been the focus of intense research of late. Catalysis by metals and non-metals offers diverse opportunities for the development of new organic reactions with promising range of selectivities-chemoselectivity, regioselectivity, diastereoselectivity, and enantioselectivity. Furthermore, these transformations frequently occur under mild conditions, tolerate a broad array of functional groups, and proceed with high stereoselectivity. The area of catalysis is sometimes referred to as a 'foundational pillar' of green chemistry. Catalytic reactions often reduce energy requirements and decrease separations because of increased selectivity; they are also capable of permitting the use of renewable feedstocks of less toxic reagents or minimizing the quantities of reagents needed. New catalytic organic synthesis methodologies have, thus, offered several possibilities for considerable improvement in the eco-compatibility of fine chemical production. Hence, these catalytic methodologies have emerged as powerful tools for the efficient and chemoselective synthesis of heterocyclic molecules. Key Features: Presents the synthesis of different five-membered heterocycles. Contains the most up-to-date information in this fast-moving field. Covers novel catalytic approaches used in the study and application of catalysts in synthetic organic reactions. Presents new methodologies for the synthesis of heterocycles.

Bioremediation: A Sustainable Approach to Preserving Earth's Water discusses the latest research in green chemistry practices and principles that are involved in water remediation and the quality improvement of water. The presence of heavy metals, dyes, fluoride, dissolved solids and many other pollutants are responsible for water pollution and poor water quality. The removal of these pollutants in water resources is necessary, yet challenging. Water preservation is of great importance globally and researchers are making significant progress in ensuring this precious commodity is safe and potable. This volume illustrates how bioremediation in particular is a promising green technique globally. Features: Addresses bioremediation of all the major water pollutants Approaches the chemistry of water and the concept of water as a renewable resource from a green chemistry aspect Discusses environmental chemistry and the practice of industrial ecology Explains the global concern of adequate high quality water supplies, and how bioremediation can resolve this Explores sustainable development through green engineering

The important resource that explores the twelve design principles of sustainable environmental engineering Sustainable Environmental Engineering (SEE) is to research, design, and build Environmental Engineering Infrastructure System (EEIS) in harmony with nature using life cycle cost analysis and benefit analysis and life cycle assessment and to protect human health and environments at minimal cost. The foundations of the SEE are the twelve design principles (TDPs) with three specific rules for each principle. The TDPs attempt to transform how environmental engineering could be taught by prioritizing six design hierarchies through six different dimensions. Six design hierarchies are prevention, recovery, separation, treatment, remediation, and optimization. Six dimensions are integrated system, material economy, reliability on spatial scale, resiliency on temporal scale, and cost effectiveness. In addition, the authors, two experts in the field, introduce major computer packages that are useful to solve real environmental engineering design problems. The text presents how specific environmental engineering issues could be identified and prioritized under climate change through quantification of air, water, and soil quality indexes. For water pollution control, eight innovative technologies which are critical in the paradigm shift from the conventional environmental engineering design to water resource recovery facility (WRRF) are examined in detail. These new processes include UV disinfection, membrane separation technologies, Anammox, membrane biological reactor, struvite precipitation, Fenton process, photocatalytic oxidation of organic pollutants, as well as green infrastructure. Computer tools are provided to facilitate life cycle cost and benefit analysis of WRRF. This important resource: - Includes statistical analysis of engineering design parameters using Statistical Package for the Social Sciences (SPSS) - Presents Monte Carlos simulation using Crystal ball to quantify uncertainty and sensitivity of design parameters - Contains design methods of new energy, materials, processes, products, and system to achieve energy positive WRRF that are illustrated with Matlab - Provides information on life cycle costs in terms of capital and operation for different processes using MatLab Written for senior or graduates in environmental or chemical engineering, Sustainable Environmental Engineering defines and illustrates the TDPs of SEE. Undergraduate, graduate, and engineers should find the computer codes are useful in their EEIS design. The exercise at the end of each chapter encourages students to identify EEI engineering problems in their own city and find creative solutions by applying the TDPs. For more information, please visit www.tang.fiu.edu.

This valuable book is devoted to problems of the synthesis, vulcanization, modification, and study of structure and properties of highly filled sealants based on polysulfide oligomers (PSO). The book summarizes information concerning chemistry, synthesis technology, structure, and properties of liquid thiokols and thiokol-containing polyesters. It also presents a literary survey on chemism and mechanisms for liquid thiokols vulcanization involving oxidants or through polyaddition. The book describes formulation principles of sealants, their properties, and application areas. The book provides research on vulcanization and modification of thiokol sealants involving thiokol-epoxy resin copolymers, unsaturated polyesters, and various isocyanate prepolymers. It describes studies of mechanisms underlying vulcanization of polysulphide oligomers by manganese dioxide, sodium dichromate and zinc oxide, and also of the structure and properties of sealants on the basis of a liquid thiokol and commercial " -2" polymer depending on a chemical nature and the ratio of constituent oligomers. The book gives information on the influence of filling materials on vulcanization kinetics, rheological, and physico-mechanical properties of sealants depending on the nature of PSO. The book will be of interest to research personnel of scientific institutes and centers developing reactive oligomers and their compositions and studying their structure and properties as well as engineers working in science centers or enterprises working in the area of development, production, and application of polysulfide oligomers and sealants.

One of the major areas of emphasis in the field of in chemical science and engineering technology in recent years has been interdisciplinary research, a trend that promises new insights and innovations rooted in cross-disciplinary collaboration. This volume is designed for stepping beyond traditional disciplinary boundaries and applying knowledge and insights from multiple fields. This book, Chemical Science and Engineering Technology: Perspectives on Interdisciplinary Research, provides a selection of chapters on interdisciplinary research in chemical science and engineering technology, taking a conceptual, and practical approach. The book includes case studies and supporting technologies and also explains the conceptual thinking behind current uses and potential uses not yet implemented. International experts with countless years of experience lend this volume credibility.

Many economically developing countries and nations without robust occupational hygiene (OH) educational programs endure a shortage of qualified occupational hygienists, resulting in higher rates of workplace injury, illness, and fatality. Damage to valuable infrastructure, environment, and public health also occurs without adequate support. Improving Global Worker Health and Safety Through Collaborative Capacity Building Initiatives outlines a broad variety of capacity building projects in OH. It also introduces detailed experiences of occupational hygienists working abroad and working on special global topics including a discussion of how global trade agreements influence the practice and policy within OH. It describes the special needs of informal workers who do not have a "typical" employer and special challenges of creating university curricular guidelines for OH, building competency, and increasing capacity. This book also informs experienced professionals in international OH-capacity building initiatives and directions. Features: Presents the global impact and importance of occupational hygienists Outlines knowledge and collaboration through networking Provides case studies on real world situations and problems This text will be useful for professionals and graduate students in the fields of occupational health and safety and public health.

Forever Chemicals: Environmental, Economic, and Social Equity Concerns with PFAS in the Environment provides the reader with an understanding of the complex and interwoven issues associated with per- and polyfluorinated substances (PFAS) in our environment. The chapters provide in-depth perspective into various issues, including health, regulation, detection, clean-up strategies and technologies, and more. Taken together or as the reader's interests lead them, the variety of topics covered in the book present a balanced perspective on this complex topic. It will address the current state of PFAS and where indicators are pointing for future developments. The book is also a deeper investigation of the regulatory challenges, analytical hurdles, and toxicological progress to date for the suite of PFAS chemicals. Features Explains the trends that will affect future policy and regulatory decisions Looks holistically at 4000+ PFAS chemicals Includes PFAS risk assessments at contaminated sites and biomonitoring insights Provides in-depth discussions on remediation technologies Illustrates quality and diversified content Provides a balanced perspective on this complex topic

This volume, Engineering Technology and Industrial Chemistry with Applications, brings together innovative research, new concepts, and novel developments in the application of new tools for chemical and materials engineers. It provides a collection of innovative chapters on new scientific and industrial research from chemists and chemical engineers at several prestigious institutions. It looks at recent significant research and reports on new methodologies and important applications in the fields of chemical engineering as well as provides coverage of chemical databases, bringing together theory and practical applications. Highlighting theoretical foundations, real-world cases, and future directions, this authoritative reference source will be a valuable addition for researchers, practitioners, professionals, and students of chemistry material and chemical engineering.

This book provides an important structural analysis of polymer solutions and melts, using fractal analysis. The book covers the theoretical fundamentals of macromolecules fractal analysis. It then goes on to discuss the fractal physics of polymer solutions and the fractal physics of melts. The intended audience of the book includes specialists in chemistry and physics of polymer synthesis and those in the field of polymers and polymer composites processing.

This book focuses on important aspects of materials chemistry by providing an overview of the theoretical aspects of materials chemistry, by describing the characterization and analysis methods for materials, and by explaining physical transport mechanisms in various materials. Not only does this book summarize the classical theories of materials chemistry, but also it exhibits their engineering applications in response to the current key issues. The chapters provide practical equations, figures, and references, providing suitable complement to the text. This book is designed to provide important information for scientists and engineers on experimental research in materials chemistry using modern methods. The methods and instrumentation described represent modern analytical techniques useful to researchers, product development specialists, and quality control experts in polymer synthesis and manufacturing.

Interplant Resource Integration: Optimization and Allocation presents an introduction to the planning and implementation methods for interplant resource integration. The analytic tools provided in this book can be used for the tasks of formulating mathematical programming model(s) to maximize the achievable overall savings and also for devising the "fair" distribution scheme(s) to allocate individual financial benefits among the participating plants. Offers tools for gaining economic benefit and environmental friendliness Presents methods for realistically feasible solutions Provides concrete mathematical modeling procedures Familiarizes readers with various network synthesis approaches and shows alternative viewpoints that can be adopted to model the interactions of participating members in an interplant resource integration scheme Aimed at chemical engineers, process engineers, industrial chemists, mechanical engineers in the fields of chemical processing and plant engineering.

An Introduction to Compressible Flow, Second Edition covers the material typical of a single-semester course in compressible flow. The book begins with a brief review of thermodynamics and control volume fluid dynamics, then proceeds to cover isentropic flow, normal shock waves, shock tubes, oblique shock waves, Prandtl-Meyer expansion fans, Fanno-line flow, Rayleigh-line flow, and conical shock waves. The book includes a chapter on linearized flow following chapters on oblique shocks and Prandtl-Meyer flows to appropriately ground students in this approximate method. It includes detailed appendices to support problem solutions and covers new oblique shock tables, which allow for quick and accurate solutions of flows with concave corners. The book is intended for senior undergraduate engineering students studying thermal-fluids and practicing engineers in the areas of aerospace or energy conversion. This book is also useful in providing supplemental coverage of compressible flow material in gas turbine and aerodynamics courses.

Nanomaterials are becoming ubiquitous; microbes similarly are everywhere. This book focuses on various ways the diverse nanomaterials interact with microbial communities and implications of such interactions. Both toxicity and beneficial effects of nanomaterial-microbe interactions have been covered. This includes areas such as fate and bioavailability of nanomaterials in environments, microbial synthesis of nanomaterials and antimicrobial action of nanomaterials. Fairly comprehensive but with narrow focus, the book provides useful insights into these interactions which need to be factored in while designing nanoscience based new technologies.

Non-thermal operations in food processing are an alternative to thermal operations and similarly aimed at retaining the quality and organoleptic properties of food products. This volume covers different non-thermal processing technologies such as high-pressure processing, ultrasound, ohmic heating, pulse electric field, pulse light, membrane processing, cryogenic freezing, nanofiltration, and cold plasma processing technologies. The book focuses both on fundamentals and on recent advances in non-thermal food processing technologies. It also provides information with the description and results of research into new emerging technologies for both the academy and industry. Key features: Presents engineering focus on non-thermal food processing technologies. Discusses sub-classification for recent trends and relevant industry information/examples. Different current research-oriented results are included as a key parameter. Covers high-pressure processing, pulse electric field, pulse light technology, irradiation, and ultrasonic techniques. Includes mathematical modeling and numerical simulations. Food Processing: Advances in Non-Thermal Technologies is aimed at graduate students, professionals in food engineering, food technology, and biological systems engineering.

Textiles and Their Use in Microbial Protection: Focus on COVID-19 and Other Viruses provides readers with vital information about disinfection mechanisms used in textile applications in the fight against dangerous microbes and viruses. KEY FEATURES: Introduces the basics of textile materials used for medical applications Features key information on virology, characterization, indication, and passivation of COVID-19 Describes UV, photocatalysis, photooxidation, application of TiO2, copper-based viral inhibition, and activated carbon Discusses antiviral finishes for the protection against SARS-CoV-2, particle penetration in dense cotton fabrics under swollen state, and the impact of moisture on face masks and their designs Aimed at textile and materials engineers as well as readers in medical fields, this text offers a comprehensive view of fundamentals and solutions in the use of textiles for microbial protection.

Pullulan is a polysaccharide produced by the fungus Aureobasidium pullulans and possesses some distinct properties such as excellent transparent film-forming ability, moisture absorptivity, water solubility, non-toxicity, and adhesivity. These properties allow pullulan to find potential applications in various industries such as pharmaceuticals, cosmetics, food, and health care. This book presents the chemistry and properties of pullulan, along with the method of its production at the laboratory level. It discusses the structural engineering, processing methods, and versatile applications of pullulan, as well as highlights the challenges that still have to be overcome for its large-scale production. This unique book comprehensively summarizes many of the recent research findings on pullulan, contributed by leading experts in this research domain. It is a useful reference book for scientists, academicians, researchers, chemists, technologists, graduate and postgraduate students, and general readers who are interested in pullulan.

Subcritical water is a green extraction solvent compared to conventional extraction solvents. While experimental results on subcritical water extraction (SWE) technology have been published piecemeal, there has been no comprehensive review of the state of the art. Green Extraction in Separation Technology fills that gap, serving to cover extracting with subcritical water as an environmentally friendly solvent. FEATURES Presents new technologies for extracting natural compounds from plants and compares the advantages and disadvantages versus SWE Explains research on SWE over the last 15 years Offers an overview of the solubility of different compounds in SWE and related theoretical content Discusses modeling of SWE and describes the development of a new model for this process This monograph is aimed at researchers and advanced students in chemical and biochemical engineering.

For over 80 years, the National Society of Professional Engineers (NSPE) has been a leader in the promotion of ethical practice within the field of engineering. One of the Society's greatest contributions is the formation and adoption of the NSPE Code of Ethics. But the code, with its six "Fundamental Canons," is only truly instructive if engineers can bridge the gap between principles and action. Here there is no substitute for personal reflection on the ethical and philosophical issues that underlie the code. If done well, such reflection provides an indispensable basis for moral problem solving. Beyond the Code: A Philosophical Guide to Engineering Ethics is designed to complement the NSPE Code of Ethics by helping readers "go beyond" in their understanding of the philosophical issues bound up in the code. Each chapter addresses one of the Fundamental Canons of the NSPE code, and provides a philosophical analysis of the various parts of each canon by employing contemporary and classical texts. This unique approach to engineering ethics guides students and professionals in their readings of the appended selections to refine their understanding of the code in order to apply it to the practical challenges of today's engineers. Key Features: Is the first introduction to engineering ethics that helps students understand and apply the NSPE Code of Ethics to engineering practice Includes a Preface from Arthur E. Schwartz, NSPE Deputy Executive Director and General Counsel, and NAFE Executive Director As a hybrid text, includes primary philosophical texts with extensive introductions and guided reading questions from the book's three authors Offers case studies from the NSPE Board of Ethical Review, allowing students to see a direct connection between the issues discussed in the text and real-world engineering practice Includes the following pedagogical aids: "Key Terms and Concepts" for each chapter "Preparing to Read" sections before each primary source reading "Guided Reading Questions" after each primary source reading "Going Beyond-Our Questions for a Deep Dive" after each case study.

The aim of this text is to provide a comprehensive set of calculations relating to mass and energy balances for an entire process plant. An ammonia synthesis plant will be taken as a calculation model to develop the relevant mass and energy balances necessary for the design and subsequent production, as the production of ammonia synthesis gas is an internationally used process. Instead of teaching the basics of mass and energy balances, the text aims to give a detailed series of process integrated and illustrated calculations to help readers develop and design a process plant. * Details complete mass and energy calculations related to a manufacturing plant and includes stepwise procedures for mass and energy balances * Demonstrates how the series of integrated calculations will lead to the production of a specified amount of final product * Features "teaching" appendices that lay out applications of prior-assumed knowledge, which can be used in conjunction with the main text where more detailed explanation may be needed * Contains problems linked to various manufacturing sections covered in the text to help readers consolidate their knowledge This book will serve undergraduate Chemical Engineering students as a teaching aid in capstone design and related courses and gives useful insights to advanced students, researchers, and industry personnel within the Chemical Engineering field.

The aim of this text is to provide a comprehensive set of calculations relating to mass and energy balances for an entire process plant. An ammonia synthesis plant will be taken as a calculation model to develop the relevant mass and energy balances necessary for the design and subsequent production, as the production of ammonia synthesis gas is an internationally used process. Instead of teaching the basics of mass and energy balances, the text aims to give a detailed series of process integrated and illustrated calculations to help readers develop and design a process plant. * Details complete mass and energy calculations related to a manufacturing plant and includes stepwise procedures for mass and energy balances * Demonstrates how the series of integrated calculations will lead to the production of a specified amount of final product * Features "teaching" appendices that lay out applications of prior-assumed knowledge, which can be used in conjunction with the main text where more detailed explanation may be needed * Contains problems linked to various manufacturing sections covered in the text to help readers consolidate their knowledge This book will serve undergraduate Chemical Engineering students as a teaching aid in capstone design and related courses and gives useful insights to advanced students, researchers, and industry personnel within the Chemical Engineering field.

Membrane Contactors: Fundamentals, Applications and Potentialities, Volume 11 covers new operations that could be efficiently used to improve the performance of a variety of industrial production cycles in applications ranging from biotechnology to agrofood. This book focuses on the basic "principles of work": required membrane materials and properties; major operating parameters; the importance of module configuration and design and; the performance of membrane contactors in specific processes. The authors dynamic approach to this subject makes Membrane Contactors: Fundamentals, Applications and Potentialities, Volume 11 the most comprehensive book currently available on all aspects related to the 'membrane contactor world.
* Describes new unit operations in process engineering
* Covers a wide variety of industrial applications, from biotechnology to agrofood
* Applicable to process intensification and sustainable growth strategies

Functionalized polymers are macromolecules to which chemically bound functional groups are attached which can be used as catalysts, reagents, protective groups, etc. Functionalized polymers have low cost, ease of processing and attractive features for functional organic molecules. Chemical reactions for the introduction of functional groups in polymers and the conversion of functional groups in polymers depend on different properties. Such properties are of great importance for functionalization reactions for possible applications of reactive polymers. This book deals with the synthesis and design of various functional polymers, the modification of preformed polymer backbones and their various applications.