As a stand alone volume, Advances in NMR, comprehensively highlights the rapid progress of nuclear magnetic resonance over the last five years.

• Features 66 articles on the latest major advances in NMR
• Written by over 80 internationally recognised experts

Including these outstanding articles:
- Double-Quantum NMR Spectroscopy of Dipolar Coupled Spins Under Fast Magic Angle Spinning (H W Spiess)
- Pulse Sequence Design using Rotor and Spin Symmetry ( M Levitt)
- Indirect Nuclear Spin-Spin Coupling Tensors (R E Wasylishen)
- Weakly Aligned Biomolecules in Liquid Crystals (A Bax)
- Multiple-Resonance, Multi-dimensional Solid-state NMR of Proteins (S J Opella)
- Dynamics of Hydrogen Transfer in Liquids and Solids (H Limbach)
- Optically Pumped NMR of Semiconductors and Two-dimensional Electron Systems (R Tycko/S E Barrett)

"The list of contributors looks like a Who's Who of the subject"
The Times Higher Education Supplement

Planned and organised by an eminent international editorial board and reviewed by a distinguished advisory board, articles are written by pioneers and key NMR innovators in the field.

The eight volume Encyclopedia of Nuclear Magnetic Resonance published in 1996 has established itself as the professional modern reference work on NMR. Since publication, a number of the key areas covered in the original work have seen extensive developments. With the addition of the 9th volume, this brings the Encyclopedia completely up-to-date, offering the most complete coverage of NMR available.

This book presents a collection of chapters on modern bioelectrochemistry focusing on new materials for biodevice, bioelectrosynthesis and bioenergy. The chapters cover protein engineering, semiconductors, biorecognition, graphene-based bioelectronics, bioelectrosynthesis, biofuel cells, bioinspired batteries and biophotovoltaics.

This handbook is aimed to deliver an up-to-date account of some of the recently developed experimental and theoretical methods in EPR, as well as a complete up-to-date listing of the experimentally determined values of multifrequency transition-ion spin Hamiltonian parameters by Sushil Misra, reported in the past 20 years, extending such a listing published by him in the Handbook on Electron Spin Resonance, volume 2. This extensive data tabulation makes up roughly 60% of the books content. It is complemented by the first full compilation of hyperfine splittings and g-factors for aminoxyl (nitroxide) radicals since 197 by Larry Berliner, a world expert on spin labeling, helping to identify and interpret substances and processes by means of EPR techniques. The book also includes coverage of the recently developed experimental technique of rapid-scan EPR by Sandra Eaton and Gareth Eaton, and a thorough review of computational modeling in EPR by Stefan Stoll, author of Easy Spin.

It is clear that electron transfer chemisty is now one of the most active areas of chemical study. "Advances in Electron Transfer Chemistry" has been designed to allow scientists who are developing new knowledge in this rapidly expanding area to describe their most recent research findings. This volume will serve those interested in learning about current breakthroughs in this rapidly expanding area of chemical research.

"Direct Alcohol Fuel Cells: Materials, Performance, Durability and Applications "begins with an introductory overview of direct alcohol fuel cells (DAFC); it focuses on the main goals and challenges in the areas of materials development, performance, and commercialization. The preparation and the properties of the anodic catalysts used for the oxidation of methanol, higher alcohols, and alcohol tolerant cathodes are then described. The membranes used as proton conductors in DAFC are examined, as well as alkaline membranes, focusing on the electrical conductivity and alcohol permeability.The use of different kinds of carbon materials as catalyst supports, gas diffusion layers, and current collectors in DAFC is also discussed. State of the art of the modeling is used to estimate performance and durability. The closing chapter reviews the use of DAFC in portable equipment and mobile devices and features a detailed discussion on the mechanisms of component degradation which limits their durability.

This book is written to facilitate the understanding of DAFC technology, applications, and future challenges. It is an excellent introduction for electrochemical and material engineers interested in small fuel cells as portable energy sources, scientists focused on materials science for energy production and storage, as well as policy-makers in the area of renewable energies."

This book focuses on the design, fabrication and applications of carbon-based materials for lithium-sulfur (Li-S) batteries. It provides insights into the localized electrochemical transition of the "solid-solid" reaction instead of the "sulfur-polysulfides-lithium sulfides" reaction through the desolvation effect in subnanometer pores; demonstrates that the dissolution/diffusion of polysulfide anions in electrolyte can be greatly reduced by the strong binding of sulfur to the oxygen-containing groups on reduced graphene oxide; manifests that graphene foam can be used as a 3D current collector for high sulfur loading and high sulfur content cathodes; and presents the design of a unique sandwich structure with pure sulfur between two graphene membranes as a very simple but effective approach to the fabrication of Li-S batteries with ultrafast charge/discharge rates and long service lives. The book offers an invaluable resource for researchers, scientists, and engineers in the field of energy storage, providing essential insights, useful methods, and practical ideas that can be considered for the industrial production and future application of Li-S batteries.

The first international symposium on the subject "The Physics and Chemistry of Si02 and the Si-Si02 Interface," organized in association with the Electrochemical Society, Inc. , was held in Atlanta, Georgia on May 15- 20, 1988. This symposium contained sixty papers and was so successful that the sponsoring divisions decided to schedule it on a regular basis every four years. Thus, the second symposium on "The Physics and Chemistry of Si02 and the Si02 Interface was held May 18-21, 1992 in St. Louis, Missouri, again sponsored by the Electronics and Dielectrics Science and Technology Divisions of The Electrochemical Society. This volume contains manuscripts of most of the fifty nine papers presented at the 1992 symposium, and is divided into eight chapters - approximating the organization of the symposium. Each chapter is preceded with an introduction by the session organizers. It is appropriate to provide a general assessment of the current status and understanding of the physics and chemistry of Si02 and the Si02 interface before proceeding with a brief overview of the individual chapters. Semiconductor devices have continued to scale down in both horizontal and vertical dimensions. This has resulted in thinner gate and field oxides as well as much closer spacing of individual device features. As a result, surface condition, native oxide composition, and cleaning and impurity effects now provide a much more significant contribution to the properties of oxides and their interfaces.

In its second volume, this book aims to link the academic research with development in the real world and provide a historical and institutional background that can enrich more formal research. The first section will include an assessment of the evolution and the state of the nascent second-generation biofuel as well as a perspective on the evolution of corn ethanol and sugarcane ethanol in Brazil. It will also include a historical and institutional background on the biofuel industry in Brazil that has global lessons, and later, provide a technical overview of major analytical tools used to assess the economic, land use and greenhouse gas implications of biofuel policies at a regional and global level. Additionally, the book analyzes the various drivers for land use change both at a micro-economic level and at a macro-economic level. It presents studies that apply regional and global economic models to examine the effects of biofuel policies in the US, EU and Brazil on regional and global land use, on food and fuel prices and greenhouse gas emissions. These papers illustrate the use of partial and general equilibrium modeling approaches to simulate the effects of various biofuel policies, and includes studies showing the effects of risk aversion, time preferences and liquidity constraints on farmers decision to grow energy crops for biofuel production. By presenting the tools of lifecycle analysis for assessing the direct greenhouse gas intensity of biofuels, this handbook investigates the types of indirect or market mediated effects that can offset or strengthen these direct effects. It will include tools to assess the direct and indirect effects of biofuel production on greenhouse gas emissions in the US and Brazil, and ultimately provide a comprehensive background to understand the state of biofuel in the present and how to analyze their implication.

This second, completely updated edition of a classic textbook provides a concise introduction to the fundamental principles of modern electrochemistry, with an emphasis on applications in energy technology. The renowned and experienced scientist authors present the material in a didactically skilful and lucid manner.

They cover the physical-chemical fundamentals as well as such modern methods of investigation as spectroelectrochemistry and mass spectrometry, electrochemical analysis and production methods, as well as fuel cells and micro- and nanotechnology.

The result is a must-have for advanced chemistry students as well as those studying chemical engineering, materials science and physics.

This book encompasses select proceedings of NSEST-2020 and ECSIRM-2020. The volume covers advances in major areas of electrochemical science and technology and surface engineering. It covers all aspects of electrochemistry with more emphasis on corrosion. The corrosion topics include self-healing sol-gel based corrosion resistant coatings, nitric acid corrosion of stainless steel, stress corrosion cracking, etc. Few chapters are focused on electrodeposition and new materials for oxygen evolution catalysts, fuel cells and batteries. The chapters on molecularly imprinted polymer sensor for dual analytes, electrochemical sensors for lead ions and dopamine, etc., are of interest. Some papers are related to the green synthesis of nanosized oxides and superhydrophobic coatings. This book will be handy and beneficial to researchers, students, and professionals working in areas related to electrochemistry and surface engineering.

Specialist Periodical Reports provide systematic and detailed review coverage of progress in the major areas of chemical research. Written by experts in their specialist fields the series creates a unique service for the active research chemist, supplying regular critical in-depth accounts of progress in particular areas of chemistry. For over 80 years the Royal Society of Chemistry and its predecessor, the Chemical Society, have been publishing reports charting developments in chemistry, which originally took the form of Annual Reports. However, by 1967 the whole spectrum of chemistry could no longer be contained within one volume and the series Specialist Periodical Reports was born. The Annual Reports themselves still existed but were divided into two, and subsequently three, volumes covering Inorganic, Organic and Physical Chemistry. For more general coverage of the highlights in chemistry they remain a 'must'. Since that time the SPR series has altered according to the fluctuating degree of activity in various fields of chemistry. Some titles have remained unchanged, while others have altered their emphasis along with their titles; some have been combined under a new name whereas others have had to be discontinued.

This book documents the proceedings of the symposium "Fundamentals and Applications of Anion Separations" held during American Chemical Society National Meeting in Chicago, Illinois, August 25-30, 200I. Nearly 40 papers devoted to discussions on anion separation related to fundamental research and applications were presented. The symposium, sponsored by Osram Sylvania, BetzDearbom, and the Separation Science & Technology Subdivision of the Industrial & Engineering Chemistry Division of the American Chemical Society was organized by Bruce A. Moyer, Chemical Sciences Division, Oak Ridge National Laboratory, P.O. Box 2008, Building. 4500S, Oak Ridge, TN 37831-6119, and Raj P. Singh, Chemicals and Powders R&D, Osram Sylvania, Chemical and Metallurgical Products Division, Towanda, PA 18848. It drew presenters from Australia, the Czech Republic, France, Germany, Japan, South Africa, Thailand, the United Kingdom, and the United States. Separations constitute an integral part of chemical industry. Chemical products typically originate in resources that must be concentrated and purified, chemically transformed, and subjected to fmal purification. Effluent streams from the processes must be treated to recycle reusable components and to remove environmentally harmful species. Some industrial processes are devoted to environmental cleanup after pollution has occurred. In addition, many analytical methods require a separation for preconcentration, or a separation may be an inherent part of the analysis itself. Micro separations occurring at membranes or interfaces are also related phenomena employed for ion sensing. Many species targeted for separation are naturally anionic. Although the standard separations techniques ofextraction, ion exchange, adsorption, precipitation, etc.

This book is intended to be a working guide to the operation of capillary electrophoresis (CE) instrumentation. Since CE is still a rap idly maturing technique, detailed validated protocols are not widely established. Therefore, extensive experimental procedures are not pro vided for individual analyses. The intention is to provide general guide lines on the principles and practice of CE and to give an overview of the specific technologies and important application areas. Part I provides operating instructions for standard commercially available instruments. Guidelines are included for activities such as changing capillaries, method development, quantitative procedures, optimization of precision and sensitivity, and the validation of meth ods, fraction collection, and troubleshooting, as well as a quick guide to running a separation. The application range of CE is possibly the most diverse of all analytical techniques and ranges from large, complex macromolecules, such as proteins and nucleic acids, to small solutes, such as organic drugs and inorganic anions and cations."

The series Topics in Current Chemistry Collections presents critical reviews from the journal Topics in Current Chemistry organized in topical volumes. The scope of coverage is all areas of chemical science including the interfaces with related disciplines such as biology, medicine and materials science. The goal of each thematic volume is to give the non-specialist reader, whether in academia or industry, a comprehensive insight into an area where new research is emerging which is of interest to a larger scientific audience. Each review within the volume critically surveys one aspect of that topic and places it within the context of the volume as a whole. The most significant developments of the last 5 to 10 years are presented using selected examples to illustrate the principles discussed. The coverage is not intended to be an exhaustive summary of the field or include large quantities of data, but should rather be conceptual, concentrating on the methodological thinking that will allow the non-specialist reader to understand the information presented. Contributions also offer an outlook on potential future developments in the field.

This volume discusses both the latest experimental research in bioelectrosynthesis and current applications. Beginning with an introduction into the "electrification of biotechnology" as well as the underlying fundamentals, the volume then discusses a wide range of topics based on the interfacing of biotechnological and electrochemical reaction steps. It includes contributions on the different aspects of bioelectrochemical applications for synthesis purposes, i.e. the production of fine and platform chemicals based on enzymatically or microbially catalyzed reactions driven by electric energy. The volume finishes with a summary and outlook chapter which gives an overview of the current status of the field and future perspectives. Edited by experts in the field, and authored by a wide range of international researchers, this volume assesses how research from today's lab bench can be developed into industrial applications, and is of interest to researchers in academia and industry.

This book highlights the state of the art in solid electrolytes, with particular emphasis on lithium garnets, electrolyte-electrode interfaces and all-solid-state batteries based on lithium garnets. Written by an international group of renowned experts, the book addresses how garnet-type solid electrolytes are contributing to the development of safe high energy density Li batteries. Unlike the flammable organic liquid electrolyte used in existing rechargeable Li batteries, garnet-type solid electrolytes are intrinsically chemically stable in contact with metallic lithium and potential positive electrodes, while offering reasonable Li conductivity. The book's respective chapters cover a broad spectrum of topics related to solid electrolytes, including interfacial engineering to resolve the electrolyte-electrode interfaces, the latest developments in the processing of thin and ultrathin lithium garnet membranes, and fabrication strategies for the high-performance solid-state batteries.This highly informative and intriguing book will appeal to postgraduate students and researchers at academic and industrial laboratories with an interest in the advancement of high energy-density lithium metal batteries

Based on a university course, this book provides an exposition of a large spectrum of geological, geochemical and geophysical problems that are amenable to thermodynamic analysis. It also includes selected problems in planetary sciences, relationships between thermodynamics and microscopic properties, particle size effects, methods of approximation of thermodynamic properties of minerals, and some kinetic ramifications of entropy production. The textbook will enable graduate students and researchers alike to develop an appreciation of the fundamental principles of thermodynamics, and their wide ranging applications to natural processes and systems.

The IUTAM Symposium on "Combustion in Supersonic Flows" was held in Poitiers at Ecole Nationale Superieure de Mecanique et d'Aerotechnique (ENSMA) from 2 to 6 october 1995. The Symposium was hosted by the Laboratoire de Combustion et de Detonique (UPR - CNRS 9028) and was attended by 60 delegates from 10 countries. The formal presentations and invited lectures were focused on four main topics, related to combustion in supersonic streams and practical issues relative to the development of new propulsion system: fundamental studies on premixed and unpremixed combustion, fluid dynamic aspects of supersonic combustion, practical system including Scramjet, Ramaccelerators and Pulsed Detonation Engines, application of detonation to propulsion. Invited lectures presenting the state of the art on these topics as well as available data base were delivered by professors Paul A. Libby from University of California at San Diego, Vladimir Sabel'nikov from TsAGI (Russia), Paul Clavin from IRPHE (Marseille, France) and Drs Shmuel Eidelman from SAlC (USA), Gunter Smeets from the French-German Institut of Saint-Louis and Bruno Deshaies from LCD (poi tiers, France).

Volume 41 of the prominent series Modern Aspects of Electrochemistry covers a range of topics in Electrochemistry and Electrochemical Engineering. The topics include the second chapter on the survey of experimental techniques and devices of solid state electrochemistry begun by Professor Joachim Maier in Volume 39. Chapter two contains a review of synthesis and characterization of nanoporous carbons and their electrochemical applications. The next chapter reviews and discusses the use of graphs in the study of chemical reaction network. The book also reviews and discusses mathematical models of three dimensional electrode structures.

This important review series began in 1954 at Academic Press. The latest volume deals with scanning tunneling microscopy, the nickel oxide electrode, radioactive labeling as an in situ method of characterization of solid/liquid interfaces, metallic glasses, reaction kinetics and mechanisms, and DC r