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Books > Science & Mathematics > Science: general issues > Scientific standards
The continuous evolution and development of experimental techniques is at the basis of any fundamental achievement in modern physics. Strongly correlated systems (SCS), more than any other, need to be investigated through the greatest variety of experimental techniques in order to unveil and crosscheck the numerous and puzzling anomalous behaviors characterizing them. The study of SCS fostered the improvement of many old experimental techniques, but also the advent of many new ones just invented in order to analyze the complex behaviors of these systems. Many novel materials, with functional properties emerging from macroscopic quantum behaviors at the frontier of modern research in physics, chemistry and materials science, belong to this class of systems. The volume presents a representative collection of the modern experimental techniques specifically tailored for the analysis of strongly correlated systems. Any technique is presented in great detail by its own inventor or by one of the world-wide recognized main contributors. The exposition has a clear pedagogical cut and fully reports on the most relevant case study where the specific technique showed to be very successful in describing and enlightening the puzzling physics of a particular strongly correlated system. The book is intended for advanced graduate students and post-docs in the field as textbook and/or main reference, but also for any other researcher in the field who appreciates consulting a single, but comprehensive, source or wishes to get acquainted, in a as painless as possible way, with the working details of a specific technique.
This book highlights the latest advances and trends in advanced signal processing (such as wavelet theory, time-frequency analysis, empirical mode decomposition, compressive sensing and sparse representation, and stochastic resonance) for structural health monitoring (SHM). Its primary focus is on the utilization of advanced signal processing techniques to help monitor the health status of critical structures and machines encountered in our daily lives: wind turbines, gas turbines, machine tools, etc. As such, it offers a key reference guide for researchers, graduate students, and industry professionals who work in the field of SHM.
This book presents in a concise way the Mie theory and its current applications. It begins with an overview of current theories, computational methods, experimental techniques, and applications of optics of small particles. There is also some biographic information on Gustav Mie, who published his famous paper on the colour of Gold colloids in 1908. The Mie solution for the light scattering of small spherical particles set the basis for more advanced scattering theories and today there are many methods to calculate light scattering and absorption for practically any shape and composition of particles. The optics of small particles is of interest in industrial, atmospheric, astronomic and other research. The book covers the latest developments in divers fields in scattering theory such as plasmon resonance, multiple scattering and optical force.
Tests of the current understanding of physics at the highest energies achievable in man-made experiments are performed at CERN's Large Hadron Collider. In the theory of the strong force within the Standard Model of particle physics - Quantum ChromoDynamics or QCD - confined quarks and gluons from the proton-proton scattering manifest themselves as groups of collimated particles. These particles are clustered into physically measurable objects called hadronic jets. As jets are widely produced at hadron colliders, they are the key physics objects for an early "rediscovery of QCD". This thesis presents the first jet measurement from the ATLAS Collaboration at the LHC and confronts the experimental challenges of precision measurements. Inclusive jet cross section data are then used to improve the knowledge of the momentum distribution of quarks and gluons within the proton and of the magnitude of the strong force.
This book on astronomical measurement takes a fresh approach to
teaching the subject. After discussing some general principles, it
follows the chain of measurement through atmosphere, imaging,
detection, spectroscopy, timing, and hypothesis testing. The
various wavelength regimes are covered in each section, emphasising
what is the same, and what is different. The author concentrates on
the physics of detection and the principles of measurement, aiming
to make this logically coherent.
This research monograph presents the latest results related to the characterization of low dimensional systems. Low-angle polarized neutron scattering and X-ray scattering at grazing incidence are used as the two main techniques to explore various physical phenomena of these systems. Special focus is put on systems like thin film transition metal and rare-earth layers, oxide heterostructures, hybrid systems, self-assembled nanostructures and self-diffusion. Readers will gain in-depth knowledge about the usage of specular scattering and off-specular scattering techniques. Investigation of in-plane and out-of-plane structures and magnetism with vector magnetometric information is illustrated comprehensively. The book caters to a wide audience working in the field of nano-dimensional magnetic systems and the neutron and X-ray reflectometry community in particular.
PART I - APPARATUS AND PRINCIPLES USED IN MICRODIFFUSION ANALYSIS - II. A STANDARD MICRO DIFFUSION APPARATUS OR 'UNIT' - III. FACTORS INFLUENCING THE ABSORPTION RATE FROM OUTER TO INNER CHAMBER WITH SPECIAL REFERENCE TO AMMONIA - IV. GENERAL PRINCIPLES GOVERNING THE ABSORPTION TIME IN MICRO DIFFUSION ANALYSIS - V. PIPETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND THEIR DELIVERY ERRORS - VI. MICRO-BURETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND ERRORS INVOLVED IN THEIR USE - VII. THE MICRODIFFUSION METHOD WITH END-POINT VOLUMES AROUND 20 CUBIC MILLIMETRES - VII. COLORIMETRY IN THE MICRODIFFUSION METHODS - PART II - DESCRIPTION OF METHODS WITH THE STANDARD UNITS - IX. AMMONIA. GENERAL METHOD USING STANDARD ACID AS ABSORBENT - X. AMMONIA. GENERAL METHOD (USING THE BORIC-HCL PROCEDURE) - XI. SPECIAL FACTORS INFLUENCING THE RATE OF AMMONIA ABSORPTION - XII. OTHER METHODS FOR DETERMINING THE ABSORBED AMMONIA IN THE MICRO DIFFUSION PROCEDURE - XIII. AMMONIA. BIOLOGICAL DETERMINATIONS - XIV. TOTAL NITROGEN XVII. UREA (BLOOD AND URINE) - XIX. ADENOSINETRIPHOSPHORIC ACID, ADENYLIC ACID, ADENOSINE, ETC. - XX. NITRATE, NITRITE AND AMIDE NITROGEN - XXII. MONOAMINE OXIDASE AND HISTAMINASE IN TISSUES - XXIII. DETERMINATION OF VOLATILE AMINES - XXIV. CARBONATES AND BICARBONATE - XXV. BLOOD GLUCOSE AND FERMENTABLE SUGAR IN NORMAL URINE - XXVI. DETERMINATION OF CARBONIC ANHYDRASE - XXVII. OXIDATION RATES OF ORGANIC SUBSTANCES WITH A STANDARD OXIDANT WITH APPLICATION TO DETERMINATION OF MINUTE AMOUNTS OF CALCIUM AS OXALATE - XXVIII. ACETIC ACID AND OTHER LOWER FATTY ACIDS - XXIX. ASSAY OF ACETYLCHOLINESTERASE - XXX. CYANIDE, AZIDE, SULPHIDE, PHENOLS - XXXI. METHANOL AND ISOPROPANOL GROUP - XXXII. ETHANOL - XXXIII. ETHANOL FROM URETHANE - XXXIV. FORMALDEHYDE - XXXV. FORMALDEHYDOGENIC STEROIDS (PERIODIC ACID AS OXIDANT) - XXXVI. FORMALDEHYDOGENIC STEROIDS (SODIUM BISMUTHATE AS OXIDANT) - XXXVII. GLYCINE (FORMALDEHYDE PRODUCED BY NINHYDRIN OXIDATION) - XXXVIII. ACETALDEHYDE (SEMICARBAZIDE ABSORPTION) - XXXIX. ACETALDEHYDE FROM LACTIC ACID AND THREONINE WITH BISULPHITE ABSORPTION - XL. ACETONE (INCLUDING A RAPID CLINICAL METHOD USING THE NESSLER SOLUTION) - XLI. THE HALOGENS (INTRODUCTORY) - XLII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO IODIDE) - XLIII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO FAST GREEN) - XLIV. BROMIDE - XLV. IODIDES AND HALOGEN MIXTURES - XLVI. SERIAL DETERMINATION OF ORGANICALLY BOUND HALOGEN - XLVII. VOLATILE HALOGENATED HYDROCARBONS (CHLOROFORM, TRICHLORETHYLENE AND CARBON TETRACHLORIDE) - XLVIII. CARBON MONOXIDE - XLIX. A RAPID CLINICAL METHOD FOR CARBON MONOXIDE DETERMINATION - LI. TOTAL MOLECULAR CONCENTRATION IN FLUID SAMPLES OF ABOUT 3-4 MILLIGRAMS - LII. SEPARATION OF CRYSTALS AND' GUMS' BY MICRODIFFUSION - QUALITATIVE MICRO-DIFFUSION ANALYSIS - LIII. SOME CONSIDERATIONS ON QUALITATIVE MICRO-DIFFUSION ANALYSIS - PART III - THE ERROR OF VOLUMETRIC TITRATION - LIV. INTRODUCTORY - LV. THE VARIABLE GLASS ERROR - LVI. THE TOTAL VARIABLE GLASS ERROR AND ITS CONTROL - LVII. THE VARIABLE CHEMICAL ERROR IN TITRATION - LVIII. THE RATIONALE OF MICRO TITRATION - LIX. THE CONSTANT GLASS ERROR - LX. THE CONSTANT CHEMICAL ERROR - LXI. VOLUMETRIC ERROR IN KJELDAHL NITROGEN ANALYSES - LXIII. UREA EXCRETION AS RENAL FUNCTION TEST - Full TOC available on website
In this book on Fundamentals of Mass Determination, the definition and dissemination of units of mass is explained, starting with an introduction to metrology and mass determination. Establishing a mass scale requires corresponding mass standards and mass comparators. The metrological requirements for weighing instruments, weight pieces, and measuring conditions are explained and discussed based on international directives and applicable legal regulations. International directives and institutions are striving towards the worldwide uniform implementation of these requirements. Processes used to determine density and volume are described to the extent that they apply to mass determination. Calculating measurement uncertainty entails taking into consideration the effect of influence variables on mass determination. An overview of this topic is provided to make it easier to determine and specify measurement uncertainty in practice, while additional information in the form of tables, illustrations, and literature references allow the reader to study mass metrology further.
Interferometry, the most precise measurement technique known today, exploits the wave-like nature of the atoms or photons in the interferometer. As expected from the laws of quantum mechanics, the granular, particle-like features of the individually independent atoms or photons are responsible for the precision limit, the shot noise limit. However this "classical" bound is not fundamental and it is the aim of quantum metrology to overcome it by employing entanglement among the particles. This work reports on the realization of spin-squeezed states suitable for atom interferometry. Spin squeezing was generated on the basis of motional and spin degrees of freedom, whereby the latter allowed the implementation of a full interferometer with quantum-enhanced precision.
Advances in the synthesis of new materials with often complex, nano-scaled structures require increasingly sophisticated experimental techniques that can probe the electronic states, the atomic magnetic moments and the magnetic microstructures responsible for the properties of these materials. At the same time, progress in synchrotron radiation techniques has ensured that these light sources remain a key tool of investigation, e.g. synchrotron radiation sources of the third generation are able to support magnetic imaging on a sub-micrometer scale. With the Sixth Mittelwihr School on Magnetism and Synchrotron Radiation the tradition of teaching the state-of-the-art on modern research developments continues and is expressed through the present set of extensive lectures provided in this volume. While primarily aimed at postgraduate students and newcomers to the field, this volume will also benefit researchers and lecturers actively working in the field.
Accurate fluid level measurement in dynamic environments can be assessed using a Support Vector Machine (SVM) approach. SVM is a supervised learning model that analyzes and recognizes patterns. It is a signal classification technique which has far greater accuracy than conventional signal averaging methods. Ultrasonic Fluid Quantity Measurement in Dynamic Vehicular Applications: A Support Vector Machine Approach describes the research and development of a fluid level measurement system for dynamic environments. The measurement system is based on a single ultrasonic sensor. A Support Vector Machines (SVM) based signal characterization and processing system has been developed to compensate for the effects of slosh and temperature variation in fluid level measurement systems used in dynamic environments including automotive applications. It has been demonstrated that a simple -SVM model with Radial Basis Function (RBF) Kernel with the inclusion of a Moving Median filter could be used to achieve the high levels of accuracy required for fluid level measurement in dynamic environments. Aimed toward graduate and postgraduate students, researchers, and engineers studying applications of artificial intelligence, readers will learn about a measurement system that is based on a single ultrasonic sensor which can achieve the high levels of accuracy required for fluid level measurement in dynamic environments.
The work presented in this book is a major step towards understanding and eventually suppressing background in the direct search for dark matter particles scattering off germanium detectors. Although the flux of cosmic muons is reduced by many orders of magnitude in underground laboratories, the remaining energetic muons induce neutrons through various processes, neutrons that can potentially mimic a dark matter signal. This thesis describes the measurement of muon-induced neutrons over more than 3 years in the Modane underground laboratory. The data are complemented by a thorough modeling of the neutron signal using the GEANT4 simulation package, demonstrating the appropriateness of this tool to model these rare processes. As a result, a precise neutron production yield can be presented. Thus, future underground experiments will be able to reliably model the expected rate of muon-induced neutrons, making it possible to develop the necessary shielding concept to suppress this background component.
This book focuses on the issues of integrating large-scale renewable power generation into existing grids. The issues covered in this book include different types of renewable power generation along with their transmission and distribution, storage and protection. It also contains the development of medium voltage converters for step-up-transformer-less direct grid integration of renewable generation units, grid codes and resiliency analysis for large-scale renewable power generation, active power and frequency control and HVDC transmission. The emerging SMES technology for controlling and integrating large-scale renewable power systems is also discussed.Since the protection issues with large-scale distributed renewable power systems are different compared to the existing protection system for one way power flow, this book includes a new protection technique for renewable generators along with the inclusion of current status of smart grid. This book is a good reference for the researchers who are working the area of renewable power generation and smart grids."
In this thesis, the author has developed a high-resolution spin-resolved photoemission spectrometer that achieves the world-best energy resolution of 8 meV. The author has designed a new, highly efficient mini Mott detector that has a large electron acceptance angle and an atomically flat gold target to enhance the efficiency of detecting scattered electrons. The author measured the electron and spin structure of Bi thin film grown on a Si(111) surface to study the Rashba effect. Unlike the conventional Rashba splitting, an asymmetric in-plane spin polarization and a tremendous out-of-plane spin component were observed. Moreover, the author found that the spin polarization of Rashba surface states is reduced by decreasing the film thickness, which indicates the considerable interaction of Rashba spin-split states between the surface and Bi/Si interface.
This book covers the diagnosis and assessment of the various faults which can occur in a three phase induction motor, namely rotor broken-bar faults, rotor-mass unbalance faults, stator winding faults, single phasing faults and crawling. Following a brief introduction, the second chapter describes the construction and operation of an induction motor, then reviews the range of known motor faults, some existing techniques for fault analysis, and some useful signal processing techniques. It includes an extensive literature survey to establish the research trends in induction motor fault analysis. Chapters three to seven describe the assessment of each of the five primary fault types. In the third chapter the rotor broken-bar fault is discussed and then two methods of diagnosis are described; (i) diagnosis of the fault through Radar analysis of stator current Concordia and (ii) diagnosis through envelope analysis of motor startup current using Hilbert and Wavelet Transforms. In chapter four, rotor-mass unbalance faults are assessed, and diagnosis of both transient and steady state stator current has been analyzed using different techniques. If both rotor broken-bar and rotor-mass unbalance faults occur simultaneously then for identification an algorithm is provided in this chapter. Chapter five considers stator winding faults and five different analysis techniques, chapter six covers diagnosis of single phasing faults, and chapter seven describes crawling and its diagnosis. Finally, chapter eight focuses on fault assessment, and presents a summary of the book together with a discussion of prospects for future research on fault diagnosis.
Stars are born and die in clouds of gas and dust, opaque to most types of radiation, but transparent in the infrared. Requiring complex detectors, space missions and cooled telescopes, infrared astronomy is the last branch of this discipline to come of age. After a very successful sky survey performed in the eighties by the IRAS satellite, the Infrared Space Observatory, in the nineties, brought spectacular advances in the understanding of the processes giving rise to powerful infrared emission by a great variety of celestial sources. Outstanding results have been obtained on the bright comet Hale-Bopp, and in particular of its water spectrum, as well as on the formation, chemistry and dynamics of planetary objects in the solar system. Ideas on the early stages of stellar formation and on the stellar initial mass function have been clarified. ISO is the first facility in space able to provide a systematic diagnosis of the physical phenomena and the chemistry in the close environment of pre-main sequence stars, in the interstellar medium, and in the final stages of stellar life, using, among other indicators, molecular hydrogen, ubiquitous crystalline silicates, water and ices. ISO has dramatically increased our ability to investigate the power production, excitation and fuelling mechanism of galaxies of every type, and has discovered a new very cold dust component in galaxies. ISO has demonstrated that luminous infrared galaxies were brighter and much more numerous in the past, and that they played a dominant role in shaping present day galaxies and in producing the cosmic infrared background.
As the focus in materials science shifts towards designing materials at the sub-micron scale - the "nanotechnology" revolution - it becomes increasingly important to characterize the mechanical properties of thin films and small volumes of material. The development of of nanoscale probes and ultrasensitive transducers for force and depth has made such measurements possible. "Nanoindentation" testing is becoming increasingly used in a wide variety of research and manufacturing areas, ranging from the testing of silicon wafers in the electronics industry to the characterization of hard coatings and other surface treatments for cutting tools, dental restoratives and other biomedical implants, and optical components.This book presents a comprehensive and detailed overview of the field of nanoindentation. The underlying theory behind the extraction of elastic modulus, hardness and other properties from the load-displacement data is discussed along with the various systematic and materials-related corrections involved. Also covered are the various methods of testing, details of an international standard for depth-sensing indentation testing, the significance of surface forces and adhesion details of commercially available instruments, and sample applications of the technique. Self-contained, the treatment is aimed at those entering the field, but by bringing together material scattered widely throughout the research literature the book will also be a useful reference for the more experienced researcher.
This volume will define the direction of eddy-current technology in nondestructive evaluation (NDE) in the twenty-first century. It describes the natural marriage of the computer to eddy-current NDE, and its publication was encouraged by favorable responses from workers in the nuclear-power and aerospace industries. It will be used by advanced students and practitioners in the fields of computational electromagnetics, electromagnetic inverse-scattering theory, nondestructive evaluation, materials evaluation and biomedical imaging, among others, and will be based on our experience in applying the subject of computational electromagnetics to these areas, as manifested by our recent research and publications. Finally, it will be a reference to future monographs on advanced NDE that are being contemplated by our colleagues and others. Its importance lies in the fact that it will be the first book to show that advanced computational methods can be used to solve practical, but difficult, problems in eddy-current NDE. In fact, in many cases these methods are the only things available for solving the problems. The book will cover the topic of computational electromagnetics in eddy-current nondestructive evaluation (NDE) by emphasizing three distinct topics: (a) fundamental mathematical principles of volume-integral equations as a subset of computational electromagnetics, (b) mathematical algorithms applied to signal-processing and inverse scattering problems, and (c) applications of these two topics to problems in which real and model data are used. This will make the book more than an academic exercise; we expect it to be valuable to users of eddy-current NDE technology in industries as varied as nuclear power, aerospace, materials characterization and biomedical imaging. We know of no other book on the market that covers this material in the manner in which we will present it, nor are there any books, to our knowledge, that apply this material to actual test situations that are of importance to the industries cited. It will be the first book to actually define the modern technology of eddy-current NDE, by showing how mathematics and the computer will solve problems more effectively than current analog practice.
This book is dedicated to the adoption of broadband microwave reflectometry (BMR)-based methods for diagnostics and monitoring applications. This electromagnetic technique has established as a powerful tool for monitoring purposes; in fact, it can balance several contrasting requirements, such as the versatility of the system, low implementation cost, real-time response, possibility of remote control, reliability, and adequate measurement accuracy. Starting from an extensive survey of the state of the art and from a clear and concise overview of the theoretical background, throughout the book, the different approaches of BMR are considered (i.e., time domain reflectometry - TDR, frequency domain reflectometry - FDR, and the TDR/FDR combined approach) and several applications are thoroughly investigated. The applications considered herein are very diverse from each other and cover different fields. In all the described procedures and methods, the ultimate goal is to endow them with a significant performance enhancement in terms of measurement accuracy, low cost, versatility, and practical implementation possibility, so as to unlock the strong potential of BMR.
In this book, leading scientists share their vision on the Kolsky-Hopkinson bar technique, which is a well-established experimental technique widely used to characterize materials and structures under dynamic, impact and explosion loads. Indeed, the Kolsky-Hopkinson bar machine is not a simple experimental device. It is rather a philosophical approach to solve the problem of measuring impact events. The split Hopkinson pressure bar conventional device is mainly limited to test homogeneous ductile non-soft materials under uni-axial compression. Extending the use of this device to more versatile applications faces several challenges such as controlling the stress state within the specimen and mastering the measurement of forces and velocities at the specimen-bar interfaces and then the material properties. Thus, the topics discussed in this book mainly focused on the loading and processing parts.
Large mass bolometers are used in particle physics experiments
to search for rare processes, like neutrinoless double beta decay
and dark matter interactions.
This book presents high-quality papers from the 2019 International Conference on Optoelectronics and Measurement (ICOM2019) which was held on November 28-30, 2019, in Hangzhou, China. It focuses on the latest developments in the fields of optics, photonics, optoelectronics, sensors, and related measurement technology. Being closely related to either the key device technology or the important commercial applications, topics of fiber optics, photodetectors, sensors, and measurement technology are of particular interest for the readers. The book contains the illustrations of advanced device technologies, measurement principles, as well as scientific and technological conclusions of the great reference value. The readers will gain deep insight into the latest development in the related fields, obtain important technical data and scientific conclusions, and inspire new ideas for their research.
These two volumes present the proceedings of the International Conference on Technology and Instrumentation in Particle Physics 2017 (TIPP2017), which was held in Beijing, China from 22 to 26 May 2017. Gathering selected articles on the basis of their quality and originality, it highlights the latest developments and research trends in detectors and instrumentation for all branches of particle physics, particle astrophysics and closely related fields. This is the second volume, and focuses on the main themes Astrophysics and space instrumentation, Front-end electronics and fast data transmission, Trigger and data acquisition systems, Machine detectors, Interfaces and beam instrumentation, Backend readout structures and embedded systems, Medical imaging, and Security & other applications. The TIPP2017 is the fourth in a series of international conferences on detectors and instrumentation, held under the auspices of the International Union of Pure and Applied Physics (IUPAP). The event brings together experts from the scientific and industrial communities to discuss their current efforts and plan for the future. The conference's aim is to provide a stimulating atmosphere for scientists and engineers from around the world.
In this book, the author describes the development of the experimental diffraction setup and structural analysis of non-crystalline particles from material science and biology. Recent advances in X-ray free electron laser (XFEL)-coherent X-ray diffraction imaging (CXDI) experiments allow for the structural analysis of non-crystalline particles to a resolution of 7 nm, and to a resolution of 20 nm for biological materials. Now XFEL-CXDI marks the dawn of a new era in structural analys of non-crystalline particles with dimensions larger than 100 nm, which was quite impossible in the 20th century. To conduct CXDI experiments in both synchrotron and XFEL facilities, the author has developed apparatuses, named KOTOBUKI-1 and TAKASAGO-6 for cryogenic diffraction experiments on frozen-hydrated non-crystalline particles at around 66 K. At the synchrotron facility, cryogenic diffraction experiments dramatically reduce radiation damage of specimen particles and allow tomography CXDI experiments. In addition, in XFEL experiments, non-crystalline particles scattered on thin support membranes and flash-cooled can be used to efficiently increase the rate of XFEL pulses. The rate, which depends on the number density of scattered particles and the size of X-ray beams, is currently 20-90%, probably the world record in XFEL-CXDI experiments. The experiment setups and results are introduced in this book. The author has also developed software suitable for efficiently processing of diffraction patterns and retrieving electron density maps of specimen particles based on the diffraction theory used in CXDI.
This thesis describes a high-quality, high-precision method for the data analysis of an interesting elementary particle reaction. The data was collected at the Japanese B-meson factory KEKB with the Belle detector, one of the most successful large-scale experiments worldwide. CP violation is a subtle quantum effect that makes the world look different when simultaneously left and right and matter and antimatter are exchanged. This being a prerequisite for our own world to have developed from the big bang, there are only a few experimental indications of such effects, and their detection requires very intricate techniques. The discovery of CP violation in B meson decays garnered Kobayashi and Maskawa, who had predicted these findings as early as 1973, the 2008 Nobel prize in physics. This thesis describes in great detail what are by far the best measurements of branching ratios and CP violation parameters in two special reactions with two charm mesons in the final state. It presents an in-depth but accessible overview of the theory, phenomenology, experimental setup, data collection, Monte Carlo simulations, (blind) statistical data analysis, and systematic uncertainty studies. |
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