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Books > Science & Mathematics > Chemistry > Analytical chemistry
This book is an introduction to the field of multi--way analysis for chemists and chemometricians. Its emphasis is on the ideas behind the method and its pratical applications. Sufficient mathematical background is given to provide a solid understanding of the ideas behind the method. There are currently no other books on the market which deal with this method from the viewpoint of its applications in chemistry. * Applicable in many areas of chemistry.* No comparable volume currently available.* The field is becoming increasingly important.
The book explains fundamental and advanced topics related to the field of membrane science including extensive coverage of material selection, preparation, characterization and applications of various membranes. Explores both preparation and wide range of applications for all possible membranes, contains an exclusive chapter on functionalized membranes and incorporation of stimuli responsive membranes in each type and includes exercise problems after each chapter It also discusses new membrane operations as membrane reactors and membrane contactors
The second edition defines the tools used in QA/QC, especially the application of statistical tools during analytical data treatment. Clearly written and logically organized, it takes a generic approach applicable to any field of analysis. The authors begin with the theory behind quality control systems, then detail validation parameter measurements, the use of statistical tests, counting the margin of error, uncertainty estimation, traceability, reference materials, proficiency tests, and method validation. New chapters cover internal quality control and equivalence method, changes in the regulatory environment are reflected throughout, and many new examples have been added to the second edition.
Contributed by multiple experts, the book covers the scientific and engineering aspects of membrane processes and systems. It aims to cover basic concepts of novel membrane processes including membrane bioreactors, microbial fuel cell, forward osmosis, electro-dialysis and membrane contactors. Maintains a pragmatic approach involving design, operation and cost analysis of pilot plants as well as scaled-up counterparts
This book covers theoretical aspects of adsorption, followed by an introduction to molecular simulations and other numerical techniques that have become extremely useful as an engineering tool in recent times to understand the interplay of different mechanistic steps of adsorption. Further, the book provides brief experimental methodologies to use, test, and evaluate different types of adsorbents for water pollutants. Through different chapters contributed by accomplished researchers working in the broad area of adsorption, this book provides the necessary fundamental background required for an academician, industrial scientist or engineer to initiate studies in this area. Key Features Explores fundamentals of adsorption-based separation Provides physical insight into aqueous phase adsorption Includes theory, molecular and mesoscopic level simulation techniques and experiments Describes molecular simulations and lattice-Boltzmann method based models for aqueous phase adsorption Presents state-of-art experimental works particularly addressing removal of "emerging pollutants" from aqueous phase
Statistical techniques have assumed an integral role in both the
interpretation and quality assessment of analytical results. In
this book the range of statistical methods available for such tasks
are described in detail, with the advantages and disadvantages of
each technique clarified by use of examples. With a focus on the
essential practical application of these techniques the book also
includes sufficient theory to facilitate understanding of the
statistical principles involved.
"Statistical Treatment of Analytical Data" is written for professional analytical chemists in industry, government and research institutions who require a practical understanding of the application of statistics in day to day activities in the analytical laboratory. It is also for students who require further and detailed information that may not be available directly in a typical undergraduate course.
Mass spectrometric techniques have developed over recent years to offer ever increasing solutions to solving problems in food processing and packaging. Even the smallest amount of contamination in food can cause a problem for food production companies, thus they are keen to find speedy and efficient quality control methods. This book outlines how ingredients and their interrelationship with processing and packaging have developed with the exploitation of mass spectrometry and gives practical protocols to stake holders showing the flexibility of this technique. With huge relevance worldwide, this book will appeal to food packaging scientists and mass spectrometry practitioners alike.
This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually 'work'. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR.Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra.How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields.A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation.The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition "For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book" - "Chemistry World" ..".I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools" - "Magnetic Resonance in Chemistry"
The issue of quality assurance in the analytical chemistry laboratory has become of great importance in recent years. "Quality Assurance in Analytical Chemistry" introduces the reader to the whole concept of quality assurance. It discusses how all aspects of chemical analysis, from sampling and method selection to choice of equipment and the taking and reporting of measurements affect the quality of analytical data. Finally, the implementation and use of quality systems are covered.
Annual Reports in Computational Chemistry, Volume 15, provides timely and critical reviews of important topics in computational chemistry. Topics covered in this series include quantum chemistry, molecular mechanics, force fields, chemical education, and applications in academic and industrial settings. Focusing on the most recent literature and advances in the field, each article covers a specific topic of importance to computational chemists.
Chemical Analysis for Forensic Evidence provides readers with the fundamental framework of forensic analytical chemistry, describing the entire process, from crime scene investigation to evidence sampling, laboratory analysis, quality aspects, and reporting and testifying in court. In doing so, important principles and aspects are demonstrated through the various forensic expertise areas in which analytical chemistry plays a key role, including illicit drugs, explosives, toxicology, fire debris analysis and microtraces such as gunshot residues, glass and fibers. This book illuminates the underlying practical framework that governs how analytical chemistry is used in practice by forensic experts to solve crime. Arian van Asten utilizes a hands-on approach with numerous questions, examples, exercises and illustrations to help solidify key concepts and teach them in an engaging way.
A Century of Separation Science presents an extensive overview of the critical developments in separation science since 1900, covering recent advances in chromatography, electrophoresis, field-flow fractionation, countercurrent chromatography, and supercritical fluid chromatography for high-speed and high-throughput analysis.
Fundamentals and Applications of Fourier Transform Mass Spectrometry is the first book to delve into the underlying principles on the topic and their linkage to industrial applications. Drs. Schmitt-Kopplin and Kanawati have brought together a team of leading experts in their respective fields to present this technique from many different perspectives, describing, at length, the pros and cons of FT-ICR and Orbitrap. Numerous examples help researchers decide which instruments to use for their particular scientific problem and which data analysis methods should be applied to get the most out of their data.
Mip Synthesis, Characteristics and Analytical Application, Volume 86 in the Comprehensive Analytical Chemistry series, highlights advances in the field, with this new volume presenting interesting chapters on synthesis and polymerization techniques of molecularly imprinted polymers, Solid phase extraction technique as a general field of application of molecularly imprinted polymer materials, Advanced artificially receptor- based sorbents for solid phase extraction using molecular imprinting technology: a new trend in food analysis, Application of molecularly imprinted polymers in microextraction and solventless extraction techniques, Magnetic molecularly imprinted microspheres - analytical approach, Surface Imprinted Micro- and Nanoparticles, and much more.
BURNT HUMAN REMAINS An all-encompassing reference and guide designed for professionals involved in the forensic analysis of burnt remains Burnt Human Remains: Recovery, Analysis and Interpretation presents an in-depth multidisciplinary approach to the detection, recovery, analysis, and identification of thermally altered remains. Bridging the gap between research and practice, this invaluable one-stop reference provides detailed coverage of analytical techniques in forensic medicine and pathology, forensic anthropology, forensic odontology, and forensic chemistry and forensic biology. Contributions from a panel of expert authors review the newest findings in forensics research and discuss their applicability to forensic case work. Opening with a historical overview of the discipline, the book covers the search and recovery aspects of burnt human remains, medico-legal investigations, determination of the post mortem interval of burnt remains, structural changes of burnt bone and teeth, DNA extraction from burnt remains, and much more. Throughout the text, the authors emphasize the importance of understanding the changes undergone by bodies when subjected to fire for establishing identity, reconstructing the events leading up to incineration, and determining the cause and manner of death. Provides a systemic framework that integrates established forensic methods and state-of-the-art analytical approaches Describes different forensic analyses from the macroscopical, microscopical, biochemical, and molecular level Features international case studies of challenging individual cases as well as natural or man-made mass fatalities requiring the identification of incinerated remains Demonstrates how changes to the macro- and microstructure of burnt remains can reveal information about incineration conditions Discusses organizations and programs focused on developing standards and best practice for the recovery and analysis burnt remains Burnt Human Remains: Recovery, Analysis and Interpretation is an indispensable resource for all practitioners engaged in the interpretation of burned human tissue, including pathologists, forensic chemists, forensic biologists, forensic anthropologists, forensic odontologists, and archaeologists.
Since four decades, rapid detection and monitoring in clinical and food diagnostics and in environmental and biodefense have paved the way for the elaboration of electrochemical biosensors. Thanks to their adaptability, ease of use in relatively complex samples, and their portability, electrochemical biosensors now are one of the mainstays of analytical chemistry. In particular, electrochemistry has played a pivotal role in the development of transduction methods for biological processes and biosensors. In parallel, the explosion of activity in nanoscience and nanotechnology and their huge success have profoundly affected biosensor technology, opening new avenues of research for electrode materials and transduction. This book provides an overview of biosensors based on amperometry, conductimetry, potentiometry, square-wave voltammetry, impedance, and electrochemiluminescence and describes the use of ultramicroelectrodes for the real-time monitoring and understanding of exocytosis. Areas of particular interest are the use of silver and gold nanoparticles for signal amplification, photocurrent transduction, and aptamer design. Moreover, advanced insights in the innovative concept of self-powered biosensors derived from biofuel cells are also discussed.
Arsenic Speciation in Algae, Volume 85, addresses the most important issues to consider during arsenic speciation in algae, including new sections on Occurrence, distribution, and significance of arsenic speciation, Biogeochemistry of arsenic in aquatic environments: the role of speciation, Sampling and sampling processing: fit for purpose techniques, Separation methods applied to arsenic speciation, Detection and quantification of arsenic compounds, Analytical approaches for proteomics and lipidomics of arsenic in algae, Quality control and quality assurance issues in arsenic speciation, Arsenic speciation in algae: case studies in Europe, and more.
Quality Control and Evaluation of Herbal Drugs brings together current thinking and practices for evaluation of natural products and traditional medicines. The use of herbal medicine in therapeutics is on the rise in both developed and developing countries and this book facilitates the necessary development of quality standards for these medicines.This book elucidates on various challenges and opportunities for quality evaluation of herbal drugs with several integrated approaches including metabolomics, chemoprofiling, marker analysis, stability testing, good practices for manufacturing, clinical aspects, Ethnopharmacology and Ethnomedicine inspired drug development. Written by Prof. Pulok K Mukherjee, a leader in this field; the book highlights on various methods, techniques and approaches for evaluating the purity, quality, safety and efficacy of herbal drugs. Particular attention is paid to methods that assess these drugs' activity, the compounds responsible and their underlying mechanisms of action. The book describes the quality control parameters followed in India and other countries, including Japan, China, Bangladesh, and other Asian countries, as well as the regulatory profiles of the European Union and North America. This book will be useful in bio-prospecting of natural products and traditional medicine-inspired drug discovery and development.
Evaluating Water Quality to Prevent Future Disasters, volume 11 in the Separation Science and Technology series, covers various separation methods that can be used to avoid water catastrophes arising from climate change, arsenic, lead, algal bloom, fracking, microplastics, flooding, glyphosphates, triazines, GenX, and oil contamination. This book provides a valuable resource that will help the reader solve their potential water contamination problems and help them develop their own new approaches to monitor water contamination.
Analysis, Fate, and Toxicity of Engineered Nanomaterials in Plants, Volume 84 in the Comprehensive Analytical Chemistry series, highlights new advances in the field, with this new volume presenting interesting chapters on the Current status of environmental monitoring, Physical principles of infrared, Chemical principles of infrared, Instrumentation and hardware, Data analysis, Sampling, Applications in water, Application in soil and sediments, Applications in ecology of animals and plants, Applications in air monitoring, Applications in contamination, Applications in marine environments, Advantages and pitfalls, and more.
This book emphasizes the use of four complex plane formalisms (impedance, admittance, complex capacitance, and modulus) in a simultaneous fashion. The purpose of employing these complex planes for handling semicircular relaxation using a single set of measured impedance data (ac small-signal electrical data) is highly underscored. The current literature demonstrates the importance of template version of impedance plot whereas this book reflects the advantage of using concurrent four complex plane plots for the same data. This approach allows extraction of a meaningful equivalent circuit model attributing to possible interpretations via potential polarizations and operative mechanisms for the investigated material system. Thus, this book supersedes the limitations of the impedance plot, and intends to serve a broader community of scientific and technical professionals better for their solid and liquid systems. This book addresses the following highlighted contents for the measured data but not limited to the: - (1) Lumped Parameter/Complex Plane Analysis (LP/CPA) in conjunction with the Bode plots; (2) Equivalent circuit model (ECM) derived from the LP/CPA; (3) Underlying Operative Mechanisms along with the possible interpretations; (4) Ideal (Debye) and non-ideal (non-Debye) relaxations; and (5) Data-Handling Criteria (DHC) using Complex Nonlinear Least Squares (CNLS) fitting procedures.
"Provides comprehensive coverage of the structures, properties, and interactions of organo-clay complexes as well as their role in the origin of life. Presents current techniques in nuclear magnetic resonance, differential thermal analysis and thermogravimetry, visible spectroscopy, and infrared and thermal-infrared spectroscopy for the analysis of fine structures in organo-clay complexes."
Mass Spectrometry: Principles and Applications, Third Edition Edmond de Hoffmann, "UniversitAA(c) Catholique de Louvain, Belgium" and Vincent Stroobant, "Ludwig Institute for Cancer Research, Brussels Branch, Belgium." "Mass Spectrometry, Third Edition" provides students with a complete overview of the principles, theories and key applications of modern mass spectrometry. Extensively revised and updated, the third edition of this successful textbook focuses on recent developments in techniques and applications. All instrumental aspects of mass spectrometry are clearly and concisely described. Emphasis is placed throughout the text on practical application examples. As with previous editions, it contains numerous tables of useful data, references and a series of exercises of increasing difficulty to encourage student understanding. Provides a complete overview of the principles, theories and applications of modern mass spectrometry An extensive revision and update including: increased coverage of MALDI and ESI, resolution and mass accuracy and activation of ions New material about instruments such as linear traps, Orbitrap, TOF/TOF, hybrid instruments, and about new atmospheric ionisation techniques such as APPI, DESI, DART. The range of applications has been expanded and newer methods such as metabolome are included Contains numerous examples and exercises to encourage student understanding "Mass Spectrometry: Principles and Applications, Third Edition" will prove invaluable to undergraduates and postgraduates using this technique in departments of chemistry, biochemistry, medicine, pharmacology, agriculture, materials science and food science. It will alsoappeal to researchers looking for an overview of the latest techniques and developments.
Partial table of contents: Transport in Conducting Polymers (E. Conwell). Charge Transport in Conducting Polymers (R. Menon). Photochemical Processes of Conductive Polymers (M. Abdou & S. Holdcroft). Photorefractive Polymers (L. Yu, et al.). Electropolymerized Phthalocyanines and Their Applications (T. Guarr). Characterization and Applications of Poly(p-phenylene) and Poly(p-phenylenevinylene) (C. Kvarnström & A. Ivaska). Artificial Muscles, Electrodissolution and Redox Processes in Conducting Polymers (T. Otero). Conducting Polymers for Batteries, Supercapacitors and Optical Devices (C. Arbizzani, et al.). Photoelectric Conversion by Polymeric and Organic Materials (M. Kaneko). Index |
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